ES2083076T3 - Dimeros de cetena de cadena larga. - Google Patents

Dimeros de cetena de cadena larga.

Info

Publication number
ES2083076T3
ES2083076T3 ES92204040T ES92204040T ES2083076T3 ES 2083076 T3 ES2083076 T3 ES 2083076T3 ES 92204040 T ES92204040 T ES 92204040T ES 92204040 T ES92204040 T ES 92204040T ES 2083076 T3 ES2083076 T3 ES 2083076T3
Authority
ES
Spain
Prior art keywords
triethyl amine
recipient
rate
fed
carboxylic acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES92204040T
Other languages
English (en)
Inventor
Nils Brolund
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Akzo Nobel NV
Original Assignee
Akzo Nobel NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=8208115&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES2083076(T3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Akzo Nobel NV filed Critical Akzo Nobel NV
Application granted granted Critical
Publication of ES2083076T3 publication Critical patent/ES2083076T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/87—Preparation of ketenes or dimeric ketenes
    • C07C45/89—Preparation of ketenes or dimeric ketenes from carboxylic acids, their anhydrides, esters or halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/88—Ketenes; Dimeric ketenes
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/03—Non-macromolecular organic compounds
    • D21H17/05—Non-macromolecular organic compounds containing elements other than carbon and hydrogen only
    • D21H17/17—Ketenes, e.g. ketene dimers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Paper (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Epoxy Compounds (AREA)
  • Warehouses Or Storage Devices (AREA)
  • Forklifts And Lifting Vehicles (AREA)
  • Devices For Conveying Motion By Means Of Endless Flexible Members (AREA)
  • Steroid Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Lubricants (AREA)

Abstract

LOS DIMEROS DE CETENA DE CADENA LARGA SE PREPARAN SEGUN UN PROCESO EN QUE, EN AUSENCIA DE UN SOLVENTE ORGANICO, SE ALIMENTA CLORURO DE ACIDO CARBOXILICO, MEZCLANDO INTENSAMENTE, EN UN RECIPIENTE DE TRIETILAMINA A UNA VELOCIDAD NO SUPERIOR A 3 MOLES/HORA POR MOL DE LA TRIETILAMINA PRESENTE Y LA MEZCLA, ALIMENTACION E INTERCAMBIO DE CALOR SE LLEVAN DE UNA MANERA TAN ARMONIZADA ENTRE SI QUE LA VISCOSIDAD DE LA MEZCLA SIEMPRE ES MENOR DE 250 MPA.S, MEDIDA A 60 (GRADOS) C (VELOCIDAD DEL ESFUERZO CORTANTE SUPERIOR A 100 L/SEG) Y LA RELACION MOLAR DE LA CANTIDAD TOTAL DE ACIDO CARBOXILICO ALIMENTANDO RESPECTO A LA CANTIDAD DE AMINA EN EL RECIPIENTE ES DE 1 : 1,025 A 1 : 2 Y DESPUES DE LA CONVERSION LA MEZCLA DE REACCION SE TRATA CON UN ACIDO HIDROCLORICO ACUOSO, DILUIDO O CON UNA SOLUCION ACUOSA DE HIDROCLORURO DE TRIETILAMINA Y ACIDO HIDROCLORICO Y SE SEPARA EL DIMERO DE CETENA. LAS CETENAS SON MUY ADECUADAS PARA UTILIZARLAS EN EL DIMENSIONAMIENTO DE PAPEL.
ES92204040T 1991-12-30 1992-12-21 Dimeros de cetena de cadena larga. Expired - Lifetime ES2083076T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP91203425 1991-12-30

Publications (1)

Publication Number Publication Date
ES2083076T3 true ES2083076T3 (es) 1996-04-01

Family

ID=8208115

Family Applications (1)

Application Number Title Priority Date Filing Date
ES92204040T Expired - Lifetime ES2083076T3 (es) 1991-12-30 1992-12-21 Dimeros de cetena de cadena larga.

Country Status (9)

Country Link
US (1) US5344943A (es)
EP (1) EP0550107B1 (es)
JP (1) JP2980475B2 (es)
AT (1) ATE133648T1 (es)
CA (1) CA2086452C (es)
DE (1) DE69208071T2 (es)
ES (1) ES2083076T3 (es)
FI (1) FI106195B (es)
NO (1) NO179170C (es)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3083323B2 (ja) * 1993-02-15 2000-09-04 エカ ノーベル アクチェボラーグ セルロース反応性疎水剤中の有機溶媒の含量の低減方法
SE9300584D0 (sv) * 1993-02-22 1993-02-22 Eka Nobel Ab A process for the production of ketene dimers
SE511318C2 (sv) * 1993-02-22 1999-09-13 Eka Chemicals Ab Förfarande för framställning av ketendimerer
GB9309604D0 (en) * 1993-05-10 1993-06-23 Hercules Inc Process for the manufacture of alkyl ketene dimer
US5685815A (en) * 1994-02-07 1997-11-11 Hercules Incorporated Process of using paper containing alkaline sizing agents with improved conversion capability
DE59602419D1 (de) * 1995-05-03 1999-08-19 Basf Ag Verfahren zur Herstellung von lösungsmittelarmen Alkyldiketenen
FI104714B (fi) * 1998-12-04 2000-03-31 Neste Oyj Menetelmä alkyyliketeenidimeerien valmistamiseksi
DE10158661A1 (de) 2001-11-30 2003-06-12 Basf Ag Verfahren zur Herstellung von Alkylketendimeren
DE10222624A1 (de) * 2002-05-17 2003-11-27 Schill & Seilacher Verfahren zur Herstellung von Dialkyldiketenen
BRPI0706299A2 (pt) * 2006-01-03 2011-03-22 Hercules Inc preparação de dìmeros de alquil ceteno
CN101845030B (zh) * 2010-01-19 2012-10-17 苏州天马精细化学品股份有限公司 连续化制备akd的方法
CN102962026B (zh) 2012-12-04 2014-02-05 苏州天马精细化学品股份有限公司 连续化无溶剂制备高纯度akd的设备及方法
CN103102333B (zh) * 2013-01-25 2015-01-21 甘肃银光聚银化工有限公司 一种烷基烯酮二聚物的生产方法
CN105541760B (zh) * 2016-01-15 2018-02-13 苏州天马精细化学品股份有限公司 一种液体akd蜡的制备方法
CN112321540B (zh) * 2019-08-05 2021-09-24 丰益表面活性材料（连云港）有限公司 制备烷基烯酮二聚体的方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE748980C (de) * 1937-12-03 1944-12-19 Verfahren zur Herstellung von hoehermolekularen Ketenen
US2369919A (en) * 1938-10-13 1945-02-20 Du Pont Ketoethenones and process therefor
DE2327988A1 (de) * 1973-06-01 1975-01-02 Henkel & Cie Gmbh Verfahren zur herstellung laengerkettiger dimerer alkylketene
DE2335488A1 (de) * 1973-07-12 1975-02-06 Basf Ag Verfahren zur herstellung von fettalkyldiketenen
DE2927118C2 (de) * 1979-07-05 1981-10-15 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von Fettalkyldiketenen
DE3434212A1 (de) * 1984-09-18 1986-03-20 Schill & Seilacher GmbH & Co, 7030 Böblingen Verfahren zur herstellung von ketendimeren und deren verwendung
DE4001237A1 (de) * 1990-01-18 1991-07-25 Basf Ag Stabilisierte waessrige alkyldiketenemulsionen
JPH0436258A (ja) * 1990-05-29 1992-02-06 Nippon Oil & Fats Co Ltd アルキルケテンダイマーの製造法

Also Published As

Publication number Publication date
NO179170B (no) 1996-05-13
DE69208071D1 (de) 1996-03-14
EP0550107A1 (en) 1993-07-07
CA2086452A1 (en) 1993-07-01
CA2086452C (en) 1999-05-18
FI106195B (fi) 2000-12-15
JPH05271212A (ja) 1993-10-19
NO924984D0 (no) 1992-12-22
EP0550107B1 (en) 1996-01-31
ATE133648T1 (de) 1996-02-15
FI925950A (fi) 1993-07-01
DE69208071T2 (de) 1996-08-29
NO924984L (no) 1993-07-01
JP2980475B2 (ja) 1999-11-22
NO179170C (no) 1996-08-21
FI925950A0 (fi) 1992-12-30
US5344943A (en) 1994-09-06

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