ES2069259T3 - Procedimiento para la obtencion de n,n,n',n'-tetraglicidil-3,3'-dialquil-4,4'-diaminodifenilmetanos. - Google Patents
Procedimiento para la obtencion de n,n,n',n'-tetraglicidil-3,3'-dialquil-4,4'-diaminodifenilmetanos.Info
- Publication number
- ES2069259T3 ES2069259T3 ES91810303T ES91810303T ES2069259T3 ES 2069259 T3 ES2069259 T3 ES 2069259T3 ES 91810303 T ES91810303 T ES 91810303T ES 91810303 T ES91810303 T ES 91810303T ES 2069259 T3 ES2069259 T3 ES 2069259T3
- Authority
- ES
- Spain
- Prior art keywords
- sub
- tetraglicidil
- diaminodifenilmetanos
- dialquil
- procedure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/36—Compounds containing oxirane rings with hydrocarbon radicals, substituted by nitrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/32—Epoxy compounds containing three or more epoxy groups
- C08G59/3227—Compounds containing acyclic nitrogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Epoxy Compounds (AREA)
- Epoxy Resins (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
METODO PARA LA ELABORACION DE COMPOSICIONES DE LA FORMULA I DONDE R SIGNIFICA GLICIDIL, Y R SUB 1 Y R SUB 3 INDEPENDIENTEMENTE ENTRE SI, SON C SUB 1-C SUB 6 ALQUILO Y R SUB 2 Y R SUB 4 INDEPENDIENTEMENTE ENTRE SI SON HIDROGENO O METILO, Y SE CARACTERIZA PORQUE (I) UN DIAMIN DE LA FORMULA II SE TRANSFORMA EN EPICLORIDRIN EN UNA RELACION DE MOL DE 1:12 A 1:40 A UNA TEMPERATURA DE 80 A 115 C, DONDE R SUB 1, R SUB 2, R SUB 3 Y R SUB 4 TIENEN EL MISMO SIGNIFICADO ARRIBA MENCIONADO. (II) AÑADE A UNA MEZCLA DE REACCION UN CATALIZADOR DE FASENTRANSFER, QUE SOMETE A LA EPICLORIDRIN A UNA DESTILACION DE CIRCULACION Y SE LLEVA A CABO AL MISMO TIEMPO QUE LA DEHIDROCLORIZACION AL AÑADIR UNA DISOLUCION DE (TIERRA) DE ALCALIHIDROXID, AL MISMO TIEMPO QUE SE PRODUCE LA SEPARACION DEL AGUA DESTILADA DE AZEOTROP
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH153790 | 1990-05-07 |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2069259T3 true ES2069259T3 (es) | 1995-05-01 |
Family
ID=4212742
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES91810303T Expired - Lifetime ES2069259T3 (es) | 1990-05-07 | 1991-04-23 | Procedimiento para la obtencion de n,n,n',n'-tetraglicidil-3,3'-dialquil-4,4'-diaminodifenilmetanos. |
Country Status (6)
Country | Link |
---|---|
US (1) | US5149841A (es) |
EP (1) | EP0456602B1 (es) |
JP (1) | JP3035671B2 (es) |
CA (1) | CA2041833C (es) |
DE (1) | DE59104649D1 (es) |
ES (1) | ES2069259T3 (es) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5132036B2 (ja) * | 2005-03-29 | 2013-01-30 | 日本化薬株式会社 | 液状エポキシ樹脂、エポキシ樹脂組成物及びその硬化物 |
JP5028818B2 (ja) * | 2006-02-21 | 2012-09-19 | 三菱瓦斯化学株式会社 | テトラグリシジルアミノ化合物の製造方法 |
AU2011230864B2 (en) * | 2010-03-23 | 2014-02-13 | Toray Fine Chemicals Co., Ltd. | High-purity epoxy compound and method for producing same |
CN111777741B (zh) * | 2020-08-04 | 2023-03-21 | 上海华谊树脂有限公司 | 四缩水甘油胺类环氧树脂及其制备方法 |
CN113698574A (zh) * | 2021-09-14 | 2021-11-26 | 安徽新远科技股份有限公司 | 一种四官能缩水甘油胺型环氧树脂的合成方法 |
CN114591490B (zh) * | 2022-04-24 | 2022-12-09 | 四川大学 | 一种缩水甘油胺型环氧树脂的合成方法 |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1790042A (en) * | 1926-08-03 | 1931-01-27 | Winthrop Chem Co | Substituted 1, 3-di-amino-2-propanols |
US3278561A (en) * | 1962-06-15 | 1966-10-11 | Monsanto Co | Hydrophobic diglycidylamines |
US3595882A (en) * | 1968-10-24 | 1971-07-27 | Dow Chemical Co | Process for preparing halogenated amine polyepoxides |
JPS53124226A (en) * | 1977-04-07 | 1978-10-30 | Mitsubishi Gas Chem Co Inc | Preparation of polyglycidyl compounds |
DE2947469A1 (de) * | 1979-11-24 | 1981-06-04 | Hoechst Ag, 6000 Frankfurt | Verfahren zur herstellung von glycidylaethern ein- oder mehrwertiger phenole |
JPS5770881A (en) * | 1980-10-20 | 1982-05-01 | Mitsubishi Petrochem Co Ltd | Preparation of polyepoxy compound |
GB2111977A (en) * | 1981-10-01 | 1983-07-13 | Secr Defence | Epoxy compounds containing N-diglycidyl groups |
JPS59175481A (ja) * | 1983-03-25 | 1984-10-04 | Kanegafuchi Chem Ind Co Ltd | 新規エポキシ樹脂およびその製造方法 |
EP0143075B1 (de) * | 1983-09-29 | 1987-11-19 | Ciba-Geigy Ag | Verfahren zur Herstellung von N-Glycidylverbindungen |
JPH0832697B2 (ja) * | 1987-04-03 | 1996-03-29 | 三菱瓦斯化学株式会社 | ポリグリシジルアミノ化合物の製造方法 |
US4778863A (en) * | 1987-08-13 | 1988-10-18 | The Dow Chemical Company | Preparation of epoxy resins having low undesirable halogen content |
JPH0277376A (ja) * | 1988-09-12 | 1990-03-16 | Sanyo Electric Co Ltd | 自転車用表示装置 |
-
1991
- 1991-04-23 DE DE59104649T patent/DE59104649D1/de not_active Expired - Fee Related
- 1991-04-23 EP EP91810303A patent/EP0456602B1/de not_active Expired - Lifetime
- 1991-04-23 ES ES91810303T patent/ES2069259T3/es not_active Expired - Lifetime
- 1991-05-01 US US07/694,525 patent/US5149841A/en not_active Expired - Lifetime
- 1991-05-03 CA CA002041833A patent/CA2041833C/en not_active Expired - Fee Related
- 1991-05-07 JP JP3131768A patent/JP3035671B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
JP3035671B2 (ja) | 2000-04-24 |
US5149841A (en) | 1992-09-22 |
CA2041833C (en) | 2001-11-20 |
DE59104649D1 (de) | 1995-03-30 |
EP0456602A1 (de) | 1991-11-13 |
EP0456602B1 (de) | 1995-02-22 |
CA2041833A1 (en) | 1991-11-08 |
JPH04225970A (ja) | 1992-08-14 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG2A | Definitive protection |
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