EP3505896A1 - Diaphragme, capteur de pression utilisant le diaphragme et procédé de production de diaphragme - Google Patents

Diaphragme, capteur de pression utilisant le diaphragme et procédé de production de diaphragme Download PDF

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Publication number
EP3505896A1
EP3505896A1 EP19152399.2A EP19152399A EP3505896A1 EP 3505896 A1 EP3505896 A1 EP 3505896A1 EP 19152399 A EP19152399 A EP 19152399A EP 3505896 A1 EP3505896 A1 EP 3505896A1
Authority
EP
European Patent Office
Prior art keywords
diaphragm
pressure
pressure receiver
support member
present
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP19152399.2A
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German (de)
English (en)
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EP3505896B1 (fr
Inventor
Tomoo Kobayashi
Ryo Sugawara
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Seiko Instruments Inc
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Seiko Instruments Inc
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Filing date
Publication date
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Publication of EP3505896A1 publication Critical patent/EP3505896A1/fr
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Publication of EP3505896B1 publication Critical patent/EP3505896B1/fr
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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L9/00—Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means
    • G01L9/0041—Transmitting or indicating the displacement of flexible diaphragms
    • G01L9/0051—Transmitting or indicating the displacement of flexible diaphragms using variations in ohmic resistance
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L7/00—Measuring the steady or quasi-steady pressure of a fluid or a fluent solid material by mechanical or fluid pressure-sensitive elements
    • G01L7/02—Measuring the steady or quasi-steady pressure of a fluid or a fluent solid material by mechanical or fluid pressure-sensitive elements in the form of elastically-deformable gauges
    • G01L7/08—Measuring the steady or quasi-steady pressure of a fluid or a fluent solid material by mechanical or fluid pressure-sensitive elements in the form of elastically-deformable gauges of the flexible-diaphragm type
    • G01L7/082—Measuring the steady or quasi-steady pressure of a fluid or a fluent solid material by mechanical or fluid pressure-sensitive elements in the form of elastically-deformable gauges of the flexible-diaphragm type construction or mounting of diaphragms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K20/00—Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating
    • B23K20/02—Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating by means of a press ; Diffusion bonding
    • B23K20/023—Thermo-compression bonding
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L7/00—Measuring the steady or quasi-steady pressure of a fluid or a fluent solid material by mechanical or fluid pressure-sensitive elements
    • G01L7/02—Measuring the steady or quasi-steady pressure of a fluid or a fluent solid material by mechanical or fluid pressure-sensitive elements in the form of elastically-deformable gauges
    • G01L7/022—Measuring the steady or quasi-steady pressure of a fluid or a fluent solid material by mechanical or fluid pressure-sensitive elements in the form of elastically-deformable gauges constructional details, e.g. mounting of elastically-deformable gauges
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L9/00—Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means
    • G01L9/0041—Transmitting or indicating the displacement of flexible diaphragms
    • G01L9/0042—Constructional details associated with semiconductive diaphragm sensors, e.g. etching, or constructional details of non-semiconductive diaphragms
    • G01L9/0044—Constructional details of non-semiconductive diaphragms
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L9/00—Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means
    • G01L9/0041—Transmitting or indicating the displacement of flexible diaphragms
    • G01L9/0051—Transmitting or indicating the displacement of flexible diaphragms using variations in ohmic resistance
    • G01L9/0052—Transmitting or indicating the displacement of flexible diaphragms using variations in ohmic resistance of piezoresistive elements
    • G01L9/0055—Transmitting or indicating the displacement of flexible diaphragms using variations in ohmic resistance of piezoresistive elements bonded on a diaphragm

Definitions

  • the present invention relates to a diaphragm, a pressure sensor using a diaphragm, and a diaphragm producing method.
  • a pressure sensor For pressure measurement of fluids such as liquids and gases, a pressure sensor is used in a wide range of fields including semiconductor manufacturing apparatuses, medical equipment, automobiles, and food.
  • a pressure sensor used for such applications includes a cap member provided with a conduit for introducing a measurement target fluid, and a diaphragm that is integral with the cap member.
  • the diaphragm is configured from a thick-walled, cylindrical support member, and a thin-walled pressure receiver closing the upper aperture of the cylindrical support member, and that makes contact with the measurement target fluid.
  • a pressure chamber On the bottom side of the diaphragm is a pressure chamber, depressed in shape, for accepting the measurement target.
  • a reference pressure chamber that accepts a reference gas is formed in the space partitioned by the diaphragm and the cap member.
  • the pressure receiver of the diaphragm deforms under the pressure difference between the pressure chamber and the reference pressure chamber.
  • a bridge circuit is provided on the top surface of the diaphragm, or the surface of the pressure receiver opposite the pressure chamber.
  • a measurement circuit measures a resistive change in the strain gauge of the bridge circuit provided for the pressure receiver that undergoes deformation according to the relative pressure of the pressure chamber and the reference pressure chamber.
  • the diaphragm used for such pressure sensors is required to have corrosion resistance against a wide range of highly corrosive fluids, and, at the same time, desirable levels of mechanical strength sufficient to withstand repeated deformation.
  • Various types of stainless steels, Co-base alloys, and other such metallic materials are used as material of a diaphragm having such properties (see, for example, JP-A-2011-164072 ).
  • the diaphragm of a shape having a cylindrical support member, and a pressure receiver formed on the upper portion of the support member can be produced from an ingot obtained by melting.
  • the ingot is drawn into a round rod shape, and sliced into a disc shape.
  • the disc can then be cut, and polished to form an integral unit of the pressure receiver and the support member.
  • the pressure receiver of the metallic diaphragm of such a shape is thin, and may allow passage of gas when, for example, fine pores (cracks) occur under the strain or other forces exerted during working. If used for a pressure sensor, such a diaphragm fails to produce an accurate relative pressure between the pressure chamber and the reference pressure chamber, with the result that the pressure reading becomes inaccurate.
  • a diaphragm of an aspect of the present invention is a metallic diaphragm that includes a plate-shaped pressure receiver, and a frame-like support member, wherein the pressure receiver has a metal structure grown parallel to a flat plate surface of the plate-shaped pressure receiver.
  • the metal structure in the pressure receiver of the diaphragm is parallel to the flat plate surface, and pore generation through the pressure receiver can be reduced. In this way, gas leakage in the pressure receiver can be prevented, and a diaphragm with excellent durability can be provided.
  • the pressure receiver may be bonded to an end surface of the support member.
  • the diaphragm has a structure in which the plate having reduced generation of vertically penetrating pores is welded to the support member. In this way, gas leakage in the pressure receiver can be prevented, and a diaphragm with excellent durability can be provided. Additionally, by using the plate that can be more easily finished (for example, by polishing) than a diaphragm of a depressed shape, the pressure receiver can have excellent flatness and surface smoothness, and the pressure measurement accuracy of the diaphragm can improve.
  • the pressure receiver and the support member may be integrally formed.
  • the pressure receiver and the support member of the diaphragm are integrally formed, and there is no joint such as by welding. This makes it possible to reduce lowering of mechanical strength or corrosion resistance due to a bonding failure, and the diaphragm can have excellent durability.
  • the pressure receiver may comprise a Co-Ni-base alloy of a composition containing, in mass%, Co: 28 to 42%, Ni: 15 to 40%, Cr: 10 to 27%, Mo: 3 to 12%, Ti: 0.1 to 1%, Mn: 1.5% or less, Fe: 0.1 to 26%, C: 0.1% or less, Nb: 3% or less, W: 5% or less, Al: 0.5% or less, and the balance unavoidable impurities.
  • a Co-Ni-base alloy having desirable corrosion resistance and desirable durability against a halogen corrosive gas is used for the pressure receiver, and the diaphragm can provide a pressure sensor suited for pressure measurement of a corrosive fluid, in addition to the foregoing effects.
  • the pressure receiver may comprise a duplex stainless steel of a composition range containing, in mass%, Cr: 24 to 26%, Mo: 2.5 to 3.5%, Ni: 5.5 to 7.5%, C: 0.03% or less, N: 0.08 to 0.3%, and the balance Fe and unavoidable impurities.
  • a duplex stainless steel having excellent electrochemical corrosion resistance against anode corrosion is used for the pressure receiver.
  • sufficient corrosion resistance can be provided even in an anode corrosive environment where a potential difference occurs between the pressure sensor using the diaphragm, and a pipe having the pressure sensor incorporated therein, in addition to the foregoing effects.
  • a pressure sensor of an aspect of the present invention uses the diaphragm of the foregoing characteristics.
  • the pressure sensor can have excellent durability.
  • a diaphragm producing method of an aspect of the present invention is a method for producing a metallic diaphragm that includes a plate-shaped pressure receiver, and a frame-like support member, the method including:
  • a plate with reduced generation of vertically penetrating pores is produced, and bonded to a support member.
  • gas leakage in the pressure receiver can be prevented, and a diaphragm having excellent durability can be produced.
  • the pressure receiver can have excellent flatness and surface smoothness, and the pressure measurement accuracy of the diaphragm can improve.
  • the pressure receiver and the end surface of the support member may be bonded to each other by diffusion bonding.
  • the pressure receiver and the support member can be bonded to each other at low temperature.
  • a diaphragm can be produced that is sufficiently strong, and can maintain corrosion resistance even when the pressure receiver and the support member, which are separate members, are combined.
  • a diaphragm producing method of an aspect of the present invention is a method for producing a metallic diaphragm that includes a plate-shaped pressure receiver, and a frame-like support member, the method including:
  • generation of vertically penetrating pores through the pressure receiver can be reduced while allowing the pressure receiver and the support member to be integrally formed. In this way, gas leakage in the pressure receiver can be prevented, and a diaphragm having excellent durability can be reliably produced.
  • the pressure receiver may comprise a Co-Ni-base alloy of a composition range containing, in mass%, Co: 28 to 42%, Ni: 15 to 40%, Cr: 10 to 27%, Mo: 3 to 12%, Ti: 0.1 to 1%, Mn: 1.5% or less, Fe: 0.1 to 26%, C: 0.1% or less, Nb: 3% or less, W: 5% or less, Al: 0.5% or less, and the balance unavoidable impurities.
  • a Co-Ni-base alloy having desirable corrosion resistance and desirable durability against a halogen corrosive gas is used for the pressure receiver, and the diaphragm can provide a pressure sensor suited for pressure measurement of a corrosive fluid, in addition to the foregoing effects.
  • the pressure receiver may comprise a duplex stainless steel of a composition range containing, in mass%, Cr: 24 to 26%, Mo: 2.5 to 3.5%, Ni: 5.5 to 7.5%, C: 0.03% or less, N: 0.08 to 0.3%, and the balance Fe and unavoidable impurities.
  • a diaphragm having anode corrosion resistance can be provided, in addition to the foregoing effects.
  • the present invention has enabled producing a diaphragm that is highly durable, and that does not involve the risk of gas leakage, and a pressure sensor using such a diaphragm.
  • FIG. 1 is a schematic cross sectional view of a diaphragm of an embodiment of the present invention.
  • a diaphragm 101 includes a thick-walled, cylindrical support member 101b, and a thin-walled pressure receiver 101a provided so as to close the upper aperture of the cylindrical support member 101b.
  • a depressed pressure chamber 7 On the bottom side of the diaphragm 101 is a depressed pressure chamber 7 for accepting a measurement target fluid.
  • a pressure sensor 10 of an embodiment of the present invention includes a cap member 4 that includes a measurement target fluid, and the diaphragm 101 integrally provided with the cap member 4 by being bonded thereto.
  • the cap member 4 has a form of a closed-end cylinder with an opening 4a, and has a flange portion 4b on the outer circumference of the opening 4a.
  • the cap member 4 is bonded to the peripheral portion of the diaphragm 101 at the inner circumference of the opening 4a.
  • the cap member 4 is formed of a material, for example, such as a metal, an alloy, and a composite material of an alloy and a resin mold.
  • a reference pressure chamber 8 partitioned by the cap member 4 and the diaphragm 101.
  • the cap member 4 has an inlet (not illustrated) for a reference gas.
  • the reference gas is introduced into the reference pressure chamber 8 to control the pressure inside the reference pressure chamber 8.
  • the pressure chamber 7 becomes in communication with the channel 6, and the fluid introduced through the channel 6 fills the pressure chamber 7. This brings the pressure receiver 101a in direct contact with the measurement target fluid.
  • a bridge circuit 3 is provided on the surface of the pressure receiver 101a opposite the pressure chamber 7, specifically, on the top surface side of the diaphragm 101, via an insulating film 2 such as a silicon oxide film.
  • the bridge circuit 3 is configured from four strain gauges (not illustrated), which are connected to connector wires 9, for example, wires 9a, 9b, 9c, and 9d.
  • the pressure receiver 101a undergoes deformation under the pressure difference between the reference pressure chamber 8 and the pressure chamber 7.
  • the pressure receiver 101a bends toward the reference pressure chamber 8 when the pressure inside the pressure chamber 7 is relatively higher than the pressure inside the reference pressure chamber 8.
  • the pressure receiver 101a bends toward the pressure chamber 7 when the pressure inside the reference pressure chamber 8 is relatively higher than the pressure inside the pressure chamber 7.
  • the resistive changes occurring in the four strain gauges of the bridge circuit 3 as a result of deformation of the pressure receiver 101a are measured with a measurement circuit, and the pressure of the pressure chamber 7 is calculated from the measured resistive changes.
  • FIGS. 3A to 3D are schematic diagrams representing a traditional process of producing a diaphragm from a raw material ingot.
  • a raw material metal or alloy is melted to produce an ingot 20 as shown in FIG. 3A .
  • the ingot 20 is drawn into a round rod shape as shown in FIG. 3B .
  • the round rod is sliced into a disc-shaped block unit 22 as shown in FIG. 3C , and cut and polished to produce the diaphragm 201 as an integral unit of the pressure receiver 201a and the support member 201b.
  • pores (voids) 21 may occur inside the ingot 20 as a result of segregation.
  • Drawing the ingot 20 elongates the metal structure in working direction.
  • the drawing also stretches the pores 21 in working direction, as shown in FIG. 3B .
  • gas leakage might occur between the reference pressure chamber 8 and the pressure chamber 7.
  • Such gas leakage occurring in the diaphragm 201 used as a pressure sensor leads to an inaccurate result in pressure measurement.
  • the present inventors conducted intensive studies to find a solution to this problem, and found that the problem can be overcome with a metal structure of a configuration that does not allow pore penetration through the thickness direction of the pressure receiver of the diaphragm.
  • the present invention was completed on the basis of this finding.
  • the present invention with the diaphragms of the embodiments below, and a pressure sensor using the diaphragm, has enabled reducing gas leakage, and provided a diaphragm and a pressure sensor having high durability.
  • a diaphragm 1 of the present embodiment is constructed from a disc-shaped pressure receiver 1a, and a cylindrical support member 1b.
  • the support member 1b of the present embodiment may be, for example, cylindrical in shape with a height of 5 mm, an upper end outer diameter of 30 mm, an upper end inner diameter of 10 mm, a lower end outer diameter of 35 mm, and a lower end inner diameter of 10 mm.
  • the support member 1b may have a range of shapes and dimensions as may be decided according to the characteristics and the use required of the pressure sensor used.
  • the support member 1b may be made by slicing a cylindrically shaped ingot in the direction orthogonal to height direction, machining the sliced ingot into a cylindrical shape, and polishing the machined product. A support member of the desired shape can be produced in this manner.
  • the pressure receiver 1a of the present embodiment has, for example, a form of a disc with an outer diameter of 30 mm, and a thickness of 0.1 mm.
  • the outer diameter matches the upper end outer diameter of the support member 1b.
  • the pressure receiver 1a can be obtained by punching a rolled plate of a metal ingot with a round forming press. Aside from rolling, the plate may be obtained by forging. The punched circular plate is polished to obtain the pressure receiver 1a that is sufficiently flat.
  • the present embodiment enables polishing the plate, both efficiently and in a manner that improves the flatness. Further, unlike the hand polishing required for the integrally carved diaphragm from a block, the plate-shaped pressure receiver 1a of the present embodiment can be mechanically polished while in the form of a rolled plate. This is preferred as it improves the efficiency of the polishing step, and the accuracy of the pressure measurement performed with the produced pressure sensor.
  • the metal structure is also drawn parallel to the flat plate surface, and grows parallel to the flat plate surface.
  • the pores that may have occurred in the process of melting are also drawn parallel to the flat plate surface. There accordingly will be no penetration of pores in height (thickness) direction. This makes it possible to reduce gas leakage in the produced pressure sensor.
  • the material of the pressure receiver 1a of the present embodiment may use a variety of metals as may be selected according to the characteristics and the intended use of the diaphragm or the pressure sensor using the pressure receiver 1a. Specifically, by using the various metallic materials described below for the pressure receiver 1a, the pressure receiver 1a can exhibit the desired mechanical characteristics and corrosion resistance suited for the desired characteristics and the intended use of the produced pressure sensor. It is preferable to use the same material for the pressure receiver and the support member, because it ensures easy bonding, and reliably prevents corrosion caused by contact between dissimilar metals.
  • the pressure receiver 1a and the support member 1b constituting the diaphragm 1 may be bonded to each other by using various metal bonding techniques, for example, such as resistance welding, laser welding, arc welding, ultrasonic welding, and diffusion bonding.
  • the bonding between the pressure receiver 1a and the support member 1b is made by diffusion bonding because it ensures that the pressure receiver 1a is sufficiently bonded to the whole upper surface of the support member 1b. Diffusion bonding is also preferred over other welding methods because it allows low temperature heating, and can reduce the poor bond strength or crevice corrosion that poses a problem when metal is welded while being melted at high temperature.
  • the support member 1b and the pressure receiver 1a are brought in contact with each other, and installed in a diffusion bonding apparatus, and heat or pressure is applied in a vacuum or in an inert gas atmosphere to bond the two members with the diffused metal atoms.
  • the applied heat may be 950°C
  • the applied pressure may be 30 MPa.
  • the process conditions are not limited to these, and may be appropriately adjusted according to the shape and the material of the diaphragm.
  • various metallic materials may be used for the diaphragm.
  • a wide range of corrosion resistant, durable metallic materials may be used so that the diaphragm can sufficiently exhibit its function.
  • various metallic materials used for metal diaphragms may be used, including stainless steels such as austenite stainless steels, austenite-ferrite duplex stainless steels, ferrite stainless steels, and martensite stainless steels, and alloys such as a Co-Ni-base alloy, a Ni-Mo-Cr-base alloy, and a Ni-Cr-base alloy.
  • the following metallic materials can provide sufficient corrosion resistance and durability, and may preferably be used as material of the metal diaphragm.
  • Such metallic material is a Co-Ni-base alloy of a composition range containing, in mass%, Co: 28 to 42%, Ni: 15 to 40%, Cr: 10 to 27%, Mo: 3 to 12%, Ti: 0.1 to 1%, Mn: 1.5% or less, Fe: 0.1 to 26%, C: 0.1% or less, Nb: 3% or less, W: 5% or less, Al: 0.5% or less, and the balance unavoidable impurities.
  • a Co-Ni-base alloy of such a composition has desirable mechanical characteristics, such as excellent fatigue strength against stress and repeated use, and excellent corrosion resistance against a halogen corrosive gas.
  • the diaphragm can provide a pressure sensor suited for pressure measurement of a corrosiveness fluid.
  • an austenite-ferrite duplex stainless steel (SUS329J4L) of a composition range containing, in mass%, Cr: 24 to 26%, Mo: 2.5 to 3.5%, Ni: 5.5 to 7.5%, C: 0.03% or less, N: 0.08 to 0.3%, and the balance Fe and unavoidable impurities.
  • a duplex stainless steel of such a composition has excellent electrochemical corrosion resistance against anode corrosion. Specifically, excellent corrosion resistance can be exhibited by using the duplex stainless steel for the pressure receiver of the diaphragm, even in an anode corrosive environment where an earthing device is installed in a pressure sensor incorporated in a pipe used for food and other applications.
  • a diaphragm 11 shown in FIG. 5 is configured from a pressure receiver 11a, and a support member 11b.
  • the pressure receiver 11a and the support member 11b are integrally made from a block unit by cutting and polishing.
  • the present embodiment differs from the related art and First Embodiment in that the diaphragm 11 is produced in the manner shown in FIGS. 6A to 6D . Specifically, the raw material ingot 20 after drawing is sliced into the block unit 22, and the block unit 22 is cut and polished after being tilted 90 degrees so that the flat plate surface of the pressure receiver 11a is oriented parallel to the longitudinal direction of original ingot 20.
  • the pores 21 are drawn in working direction (longitudinal direction) after the drawing of the ingot 20, as shown in FIG. 6B .
  • the disc-shaped block unit 22 cut out of the ingot is tilted 90 degrees as shown in FIG. 6C .
  • the pores 21 are oriented parallel to the flat plate surface.
  • the block unit 22 oriented in this direction can then be cut and polished to produce the diaphragm 11 having the pressure receiver 11a and the support member 11b.
  • the metal structure in the pressure receiver 11a of the diaphragm 11 is oriented parallel to the flat plate surface, and the pores 21, when present, also occur in a direction parallel to the flat plate surface. Accordingly, the pores 21 do not penetrate through the thickness direction of the pressure receiver 11a as in First Embodiment, and gas leakage in the pressure sensor can be reduced.
  • the support member 11b and the pressure receiver 11a are integrally formed as in the related art, and the bonding step is not required. This is advantageous as it prevents lowering of durability or corrosion resistance due to a bonding failure.
  • the diaphragm 11 was described as being produced from the raw material round rod.
  • the block unit may be formed from a rectangular column obtained by drawing the raw material ingot in a shape of a rectangular column. This is preferred because such a block unit can be stably mounted even when it is tilted 90 degrees.
  • the same materials used in First Embodiment may be used to constitute the support member 11b and the pressure receiver 11a of the diaphragm 11.
  • the pressure receiver 11a and the support member 11b are described as being integrally produced by cutting and polishing the block unit 22 sliced from the ingot 20.
  • the block unit 22 may be forged to produce the diaphragm 11 as an integral unit of the pressure receiver 11a and the support member 11b.
  • the block unit 22 is pressed into the shape of the diaphragm 11 with a tool such as a hammer and a forming press.
  • the forging can mechanically miniaturize the crystal grains in the metal structure of the pressure receiver 11a, or can orient defects in the metal structure in a direction parallel to the flat plate surface. In this way, defects penetrating through the thickness direction of the pressure receiver 11a can be removed, in addition to reducing the defects themselves present in the metal structure. This makes it possible to reduce gas leakage in the pressure sensor.

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Measuring Fluid Pressure (AREA)
  • Diaphragms And Bellows (AREA)
EP19152399.2A 2016-11-29 2017-07-28 Procédé de production de diaphragme Active EP3505896B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2016230759A JP6797649B2 (ja) 2016-11-29 2016-11-29 ダイヤフラムの製造方法
EP17183825.3A EP3327417A1 (fr) 2016-11-29 2017-07-28 Diaphragme, capteur de pression à l'aide du diaphragme et procédé de production de diaphragme

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
EP17183825.3A Division EP3327417A1 (fr) 2016-11-29 2017-07-28 Diaphragme, capteur de pression à l'aide du diaphragme et procédé de production de diaphragme

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EP3505896A1 true EP3505896A1 (fr) 2019-07-03
EP3505896B1 EP3505896B1 (fr) 2020-04-22

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EP17183825.3A Ceased EP3327417A1 (fr) 2016-11-29 2017-07-28 Diaphragme, capteur de pression à l'aide du diaphragme et procédé de production de diaphragme
EP19152399.2A Active EP3505896B1 (fr) 2016-11-29 2017-07-28 Procédé de production de diaphragme

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US (1) US10451506B2 (fr)
EP (2) EP3327417A1 (fr)
JP (1) JP6797649B2 (fr)
KR (1) KR102301591B1 (fr)
CN (1) CN108120545B (fr)

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CN112771359A (zh) * 2018-10-09 2021-05-07 株式会社富士金 压力传感器
US10892229B2 (en) 2019-04-05 2021-01-12 Nxp Usa, Inc. Media shield with EMI capability for pressure sensor
CN112775619A (zh) * 2019-11-11 2021-05-11 太原市精微测控技术有限公司 一种溅射薄膜压力传感器弹性膜片加工方法
EP4202392A1 (fr) * 2021-12-23 2023-06-28 Kistler Holding AG Capteur avec une membrane pour utilisation avec des fluides contenant de l'hydrogène

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0931577A (ja) * 1995-05-17 1997-02-04 Seiko Instr Inc ダイヤフラム
JP2011164072A (ja) 2010-02-15 2011-08-25 Seiko Instruments Inc ダイヤフラム、圧力センサ、及びダイヤフラムの製造方法

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5950331A (ja) * 1982-09-16 1984-03-23 Toshiba Corp 伝送器のダイアフラム構造
JPS60186726A (ja) * 1984-03-07 1985-09-24 Kyowa Dengiyou:Kk 圧力変換器
JPS63121619A (ja) * 1986-11-08 1988-05-25 Nippon Yakin Kogyo Co Ltd プラネタリ−ミルによる超塑性変形能を有する２相ステンレス鋼板帯の製造方法
JP2832894B2 (ja) * 1988-07-26 1998-12-09 日立建機株式会社 圧力センサ及びその製造方法、並びに圧力センサを備える油圧機器
WO1990001153A1 (fr) * 1988-07-26 1990-02-08 Hitachi Construction Machinery Co., Ltd Capteur de pression, procede de production et dispositif hydraulique pourvu de ce capteur
JPH04350529A (ja) * 1991-05-28 1992-12-04 Nok Corp 圧力センサ用ダイアフラム
JP3084304B2 (ja) * 1991-07-04 2000-09-04 長野計器株式会社 圧力センサの金属製ダイヤフラム
JPH052041U (ja) * 1992-05-21 1993-01-14 株式会社共和電業 圧力変換器
JP3368509B2 (ja) * 1993-11-11 2003-01-20 大同特殊鋼株式会社 圧力センサー部品とその製造方法
US6189205B1 (en) * 1996-08-27 2001-02-20 Robert Bosch Gmbh Process for producing pressure sensors
JP3598181B2 (ja) * 1996-09-13 2004-12-08 長野計器株式会社 ダイアフラムおよび圧力センサ
DE19700773A1 (de) * 1997-01-13 1998-07-16 Bosch Gmbh Robert Membran für einen Drucksensor
JPH11201846A (ja) * 1998-01-12 1999-07-30 Mitsubishi Electric Corp 半導体圧力検出装置
US6291806B1 (en) * 1998-10-01 2001-09-18 Usf Filtration And Separations Group, Inc. Process for bonding workpieces
JP4905024B2 (ja) * 2006-09-26 2012-03-28 Ｊｆｅスチール株式会社 スポット溶接継手強度の高いフェライト系ステンレス鋼板およびその製造方法
CN101413839B (zh) * 2008-11-25 2010-07-28 沈阳市传感技术研究所 传感器用防腐蚀膜片及其制备方法
CN101498610B (zh) * 2008-12-19 2010-12-22 北京布莱迪仪器仪表有限公司 一种隔膜装置制造方法及隔膜装置和隔膜式压力表
JP5714395B2 (ja) * 2010-05-25 2015-05-07 株式会社堀場エステック 静電容量型圧力センサ
KR101308104B1 (ko) * 2011-10-24 2013-09-12 한국과학기술연구원 생체용 압력 센서 및 그 제조 방법
JP6115935B2 (ja) * 2013-01-25 2017-04-19 セイコーインスツル株式会社 二相ステンレス鋼からなる時効熱処理加工材とそれを用いたダイヤフラムと圧力センサとダイヤフラムバルブ及び二相ステンレス鋼の製造方法
SG11201509040WA (en) * 2013-05-15 2015-12-30 Nisshin Steel Co Ltd Method for producing a stainless steel diffusion-bonded product
CN104956194B (zh) * 2013-05-24 2017-03-08 日立金属株式会社 压力传感器、使用该压力传感器的质量流量计以及质量流量控制器
JP6327633B2 (ja) * 2013-09-19 2018-05-23 セイコーインスツル株式会社 二相ステンレス鋼からなるダイヤフラム
US9208980B2 (en) * 2014-01-21 2015-12-08 Kidde Technologies, Inc. Pneumatic detector with integrated electrical contact

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0931577A (ja) * 1995-05-17 1997-02-04 Seiko Instr Inc ダイヤフラム
JP2011164072A (ja) 2010-02-15 2011-08-25 Seiko Instruments Inc ダイヤフラム、圧力センサ、及びダイヤフラムの製造方法

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KR102301591B1 (ko) 2021-09-13
US10451506B2 (en) 2019-10-22
US20180149535A1 (en) 2018-05-31
JP6797649B2 (ja) 2020-12-09
EP3327417A1 (fr) 2018-05-30
CN108120545A (zh) 2018-06-05
JP2018087730A (ja) 2018-06-07
EP3505896B1 (fr) 2020-04-22
KR20180060933A (ko) 2018-06-07

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