EP3167976A1 - Verfahren zur schätzung eines geschmolzenen stahlflussstatus und vorrichtung zur schätzung eines flussstatus - Google Patents
Verfahren zur schätzung eines geschmolzenen stahlflussstatus und vorrichtung zur schätzung eines flussstatus Download PDFInfo
- Publication number
- EP3167976A1 EP3167976A1 EP15819360.7A EP15819360A EP3167976A1 EP 3167976 A1 EP3167976 A1 EP 3167976A1 EP 15819360 A EP15819360 A EP 15819360A EP 3167976 A1 EP3167976 A1 EP 3167976A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- fluidity
- external force
- molten steel
- error
- state
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/16—Controlling or regulating processes or operations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/04—Continuous casting of metals, i.e. casting in indefinite lengths into open-ended moulds
- B22D11/057—Manufacturing or calibrating the moulds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/10—Supplying or treating molten metal
- B22D11/11—Treating the molten metal
- B22D11/114—Treating the molten metal by using agitating or vibrating means
- B22D11/115—Treating the molten metal by using agitating or vibrating means by using magnetic fields
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D11/00—Continuous casting of metals, i.e. casting in indefinite lengths
- B22D11/16—Controlling or regulating processes or operations
- B22D11/20—Controlling or regulating processes or operations for removing cast stock
- B22D11/201—Controlling or regulating processes or operations for removing cast stock responsive to molten metal level or slag level
- B22D11/202—Controlling or regulating processes or operations for removing cast stock responsive to molten metal level or slag level by measuring temperature
Definitions
- the present invention relates to a technique of estimating fluidity of molten steel in a casting mold with a view to the quality improvement of a cast piece manufactured in a continuous casting machine.
- molten steel is continuously poured from a tundish into a casting mold in which water-cooled tubes are buried, cooled in the casting mold, and is drawn out from the lower part of the casting mold.
- the opening degree of a nozzle is adjusted depending on a drawing-out speed.
- drift in which a discharge flow from each of right-and-left discharge openings becomes nonuniform, occurs.
- Each steel manufacturer has introduced, in order to decrease such instability, a flow control device that applies a braking force to the molten steel by applying a magnetic field from the outside of the casting mold. Furthermore, in order to remove inclusions and bubbles that are trapped on a surface of a solidified shell, a flow control device has been increasingly introduced that applies a dynamic magnetic field to the molten steel to apply a stirring force thereto.
- Patent Literatures 2 to 4 describe a technique that estimates the fluidity of the molten steel by performing conversion based on temperatures of the molten steel that are measured by using thermocouples buried in the casting mold.
- Patent Literatures 2 to 4 the technique that estimates the fluidity of the molten steel from the temperature of the molten steel can be applied only in the case of a solidification interface in the vicinity of the casting mold and hence, it is impossible to estimate the fluidity of the molten steel in three dimensions in the whole casting mold.
- the present invention has been made to overcome such problems, and it is an object of the present invention to provide a molten steel fluidity estimation method and a fluidity estimation device in which fluidity of molten steel can be estimated online in three dimensions in the whole casting mold.
- a molten steel fluidity estimation method estimates fluidity of molten steel in a casting mold of a continuous casting machine, and includes: an error calculating step of calculating, at positions of respective sensors arranged in the casting mold, an error between distribution of physical quantities measured by the respective sensors and distribution of physical quantities calculated by using a physical model; an external force applying step of applying an external force in a vicinity of a discharge opening of a nozzle configured to discharge the molten steel into the casting mold; and an estimating step of estimating fluidity by calculating the fluidity in a state in which the external force adjusted to compensate the error is applied.
- the estimating step includes: a perturbation calculating step of calculating a difference between fluidity in a state in which the external force is applied and fluidity in a steady state in which the external force is not applied, as perturbation of the fluidity due to the external force; a correction term calculating step of calculating a correction term by adjusting the external force and the perturbation of the fluidity so that the error is compensated; and a fluidity calculating step of calculating the fluidity by superposing the correction term on the fluidity in the steady state.
- the perturbation calculating step calculates, corresponding to each type of the external force, a difference between the distribution of the physical quantities in the state in which the external force is applied and the distribution of the physical quantities in the steady state in which the external force is not applied, and calculates a degree of influence of each type of the external force compensating the error by performing linear regression analyses of the difference and the error
- the correction term calculating step calculates a correction term compensating the error based on the degree of influence and the difference between the fluidity calculated corresponding to each type of external force in the state in which the external force is applied and the fluidity in the steady state in which the external force is not applied.
- the senor is a thermocouple
- the physical quantities represent a temperature of the molten steel at the position in which the thermocouple is arranged.
- a molten steel fluidity estimation device is adapted to estimate fluidity of molten steel in a casting mold of a continuous casting machine, and includes: an error calculation unit configured to calculate, at positions of respective sensors arranged in the casting mold, an error between distribution of physical quantities measured by the respective sensors and distribution of the physical quantities calculated by using a physical model; an external-force application unit configured to apply an external force in a vicinity of a discharge opening of a nozzle configured to discharge the molten steel into the casting mold; and an estimation unit configured to calculate fluidity in a state in which the external force adjusted to compensate the error is applied.
- fluidity of molten steel can be estimated online in three dimensions in the whole casting mold.
- FIG. 1 in a continuous casting machines 1, a casting mold 4 is arranged below a tundish 3 filled with molten steel 2 in the vertical direction, and a nozzle 5 that is a feed opening for feeding the molten steel 2 to the casting mold 4 is arranged on the bottom of the tundish 3.
- the molten steel 2 is continuously poured into the casting mold 4 from the tundish 3, cooled by the casting mold 4 in which water-cooled tubes are buried, and drawn out from the lower part of the casting mold 4 thus forming a slab.
- the opening degree of the nozzle 5 is adjusted depending on a drawing-out speed.
- thermocouples 41 are arranged on a face F and a face B, the face F and the face B constituting both ends of the slab to be cast in the thickness direction thereof (the vertical direction on the paper on which FIG. 2 is drawn).
- Each thermocouple 41 measures a temperature of the molten steel 2 at the position at which the thermocouple 41 is arranged.
- the thermocouples 41 are buried on each face so as to be arranged in 7 rows in the height direction and in 16 columns in the width direction.
- the casting mold 4 includes therein a coil (not illustrated in the drawings) used for generating a stirrer magnetic field that rotates the surface of molten steel.
- the fluidity of the molten steel 2 is calculated using a turbulence model.
- operational conditions such as a casting speed, a width and thickness of the slab, and a coil current of the stirrer magnetic field are input conditions
- the fluidity (flow speed distribution) of the molten steel 2 is calculated using a standard k- ⁇ model of the turbulence model. In this case, boundary conditions are specified as illustrated in FIG. 3 .
- FIG. 4 and FIG. 5 are views each illustrating, as an example, fluidity of the molten steel 2 that is calculated in this manner.
- FIG. 4 is a view illustrating, as an example, flow speed distribution of the molten steel 2 in the cross section at the center in the thickness direction of the slab to be cast.
- FIG. 5 is a view illustrating, as an example, flow speed distribution of the molten steel 2 in the vicinity of the casting mold 4 in the thickness direction of the slab to be cast.
- a heat transfer coefficient between the molten steel 2 and a solidified shell varies depending on the flow speed of a solidification interface, and is reflected in change of the temperature of the casting mold 4 at the position of the thermocouple 41 (see Patent Literature 4). Accordingly, in the present embodiment, the fluidity of the molten steel 2 is calculated using the turbulence model, and converted into temperature distribution thus obtaining the temperature distribution. To be more specific, the temperature-flow speed conversion rule described in Patent Literature 4 is reversely used.
- FIG. 6 is a view illustrating, as an example, temperature distribution of the molten steel 2 that is calculated in this manner. In FIG.
- the axis of ordinate and the axis of abscissa correspond to each row position of the thermocouples arranged in 7 rows and each column position of the thermocouples arranged in 16 columns that are illustrated in FIG. 2 , respectively. That is, the axis of ordinate indicates the row numbers 1 to 7 of the thermocouples from the bottom, and the axis of abscissa indicates the column numbers 1 to 16 of the thermocouples from the left.
- the axis of ordinate and the axis of abscissa are used in the same manner as above.
- the difference between the temperature distribution T calc calculated by the physical model mentioned above and the temperature distribution T act measured using the thermocouples 41 can be attributed mainly to the changes in the shape of the nozzle 5, such as clogging due to deposits, (boundary conditions in the vicinity of the nozzle 5).
- the molten steel 2 discharged from the nozzle 5 moves in accordance with the equation of motion of fluidity. Accordingly, in the present embodiment, since the change in the shape of the nozzle 5 is simply expressed without using a fixed wall, an external force that causes the perturbation of fluidity is applied in the vicinity of the discharge opening of the nozzle 5 thus compensating the error on the physical model.
- a horizontal external force Fx (Fx (left), Fx (right)) and a vertical external force Fy (Fy (left), Fy (right)) are applied in the vicinities of respective right-and-left discharge openings 51 of the nozzle 5 depending on the degree of influence of each of the horizontal external force Fx and the vertical external force Fy.
- fluidity of the molten steel 2 is referred to as "U i ", the fluidity being calculated using the physical model in a state that each external force is applied.
- the suffix i means the identification information of the type of the external force to be applied, and takes an integer from 1 to 4.
- temperature distribution of the molten steel 2 that is calculated using the physical model in a state that the external force is applied is referred to as “T i ".
- a difference between fluidity U i of the molten steel 2 that is calculated using the physical model in a state that the external force is applied, and fluidity of molten steel 2 that is calculated using the physical model in the steady state in which the external force is not applied (hereinafter, referred to as "U calc ”) is referred to as “ ⁇ U i ".
- U calc fluidity of molten steel 2 that is calculated using the physical model in the steady state in which the external force is not applied
- ⁇ T i a difference between temperature distribution T i of the molten steel 2 that is calculated using the physical model in a state in which the external force is applied and temperature distribution T calc of the molten steel 2 that is calculated using the physical model in the steady state.
- FIG. 9 is a block diagram illustrating the constitution of the molten steel fluidity estimation device according to one embodiment of the present invention.
- a fluidity estimation device 100 of molten steel according to one embodiment of the present invention is provided with an information processing unit 101, an input unit 102, and an output unit 103.
- the information processing unit 101 is constituted of a general-purpose information processing unit, such as a personal computer or a workstation, and provided with a RAM 111, a ROM 112, and a CPU 113.
- the RAM 111 temporarily stores a control program and control data with respect to processing executed by the CPU 113, and functions as a working area for the CPU 113.
- the ROM 112 stores an estimation program 112a that executes fluidity estimation processing of molten steel according to one embodiment of the present invention, a control program that controls overall operation of the information processing unit 101, and control data.
- the CPU 113 controls overall operation of the information processing unit 101 in accordance with the estimation program 112a and the control program that are stored in the ROM 112. To be more specific, the CPU113 calculates, as described later, fluidity based on input operation information and a known physical model, and converts the fluidity calculated into temperature distribution thus obtaining the temperature distribution. Furthermore, the CPU 113 analyzes a difference between the calculated temperature distribution and the temperature distribution measured by using the thermocouples 41 buried in the casting mold 4 thus estimating the fluidity of the molten steel 2.
- the input unit 102 is constituted of input units, such as a keyboard, a mouse pointer, and a numeric keypad, and operated in inputting the various kinds of information to the information processing unit 101.
- the output unit 103 is constituted of output units, such as a display and a printer, and outputs various kinds of processing information from the information processing unit 101.
- FIG. 10 is the flowchart illustrating the flow of the fluidity estimation processing of the molten steel according to one embodiment of the present invention.
- the flowchart illustrated in FIG. 10 is started at a timing where an operator has operated the input unit 102 to instruct the information processing unit 101 to execute the fluidity estimation processing, and the fluidity estimation processing advances to S1.
- the fluidity estimation processing mentioned below is achieved by the fact that the CPU 113 executes the estimation program 112a stored in the ROM 112.
- the CPU 113 uses the operation information acquired from an outside DB (not illustrated in the drawings) as an input condition, and the turbulence model to calculate the fluidity U calc and the temperature distribution T calc of the molten steel 2 in the steady state. Then, the processing of S1 is completed, and the fluidity estimation processing advances to S2.
- the CPU 113 calculates, using the turbulence model, the fluidity U i and the temperature distribution T i of the molten steel 2 in a state in which the above-mentioned external force is applied in the vicinity of the discharge opening 51 of the nozzle 5. Then, the processing of S2 is completed, and the fluidity estimation processing advances to S3.
- FIG. 11A to FIG. 12B are views each illustrating, as an example, fluidity and temperature distribution of the molten steel 2, the fluidity and temperature distribution being calculated in a state in which the external force is applied.
- FIG. 11B illustrates temperature distribution T 1 of the molten steel 2 that is calculated in the same manner as the case above.
- FIG. 11B illustrates temperature distribution T 1 of the molten steel 2 that is calculated in the same manner as the case above.
- FIG. 11A illustrates fluidity U 1 of the molten steel 2 that is calculated in a
- FIG. 12B illustrates temperature distribution T 2 of the molten steel 2 that is calculated in the same manner as the case above.
- the CPU 113 performs a sensitivity analysis. That is, in terms of the fluidity of the molten steel 2, the CPU 113 calculates a difference ⁇ U i between the fluidity U i calculated in a state in which the external force is applied and the fluidity U calc calculated in the steady state. Furthermore, in terms of the temperature distribution of the molten steel 2, the CPU 113 calculates a difference ⁇ T i between temperature distribution T i calculated in a state in which the external force is applied, and temperature distribution T calc calculated in the steady state.
- ⁇ U i and ⁇ T i mean the fluidity and the temperature distribution that are affected by the external force; that is, the fluidity and the temperature distribution in a state in which the external force is applied, respectively. Then, the processing of S3 is completed, and the fluidity estimation processing advances to S4.
- FIG. 13A to FIG. 14B are views illustrating, as examples, ⁇ U i and ⁇ T i that are calculated, respectively.
- FIG. 13B illustrates ⁇ T 1 in the same state as above.
- FIG. 14B illustrates ⁇ T 2 in the same state as above.
- the CPU 113 compares temperature distribution T act of the molten steel 2 that is measured by using the thermocouples 41, with temperature distribution T calc of the molten steel 2 that is calculated in the steady state, and calculates an error between the temperature distribution T act and the temperature distribution T calc . Then, the processing of S4 is completed, and the fluidity estimation processing advances to S5.
- the CPU 113 performs a linear regression analysis of the error calculated in the processing of S4 depending on ⁇ T i , which is a result of the sensitivity analysis, calculated in the processing of S3.
- the CPU 113 performs, as illustrated in the following expressions (3) to (7), the linear regression analysis of the error between T act and T calc depending on a total of nine bases (regression variables) including four bases corresponding to the respective four types of external forces, and five bias-correction-use bases corresponding to the respective five rows in which the thermocouples 41 are arranged.
- thermocouples 41 out of seven rows of the thermocouples 41 are used for the fluidity estimation processing.
- a certain bias is on both the face F and the face B that is not influenced by the external force
- five bases are provided corresponding to the respective bias corrections for five rows.
- the number of lines of a bias matrix B illustrated in the above-mentioned expressions (4) and (6) is the total number of the thermocouples 41 arranged in five rows (sum total of the thermocouples 41 arranged in the face F and the face B), and the number of columns of the bias matrix B is five, which corresponds to the respective five rows of the thermocouples 41.
- the number of elements of a vector 1 illustrated in the above-mentioned expressions (6) and (7) is the number of the thermocouples 41 arranged in each row (sum total of the thermocouples 41 arranged in the face F and the face B). Then, the processing of S5 is completed, and the fluidity estimation processing advances to S6.
- FIG. 15A is a view illustrating a time transition of the external force Fx (defined as positive in the outward direction) applied to each of the right-and-left discharge openings 51 of the nozzle 5 in the horizontal direction.
- FIG. 15B is a view illustrating a time transition of the external force Fy (defined as positive in the downward direction) applied to each of the right-and-left discharge openings 51 of the nozzle 5 in the vertical direction.
- FIG. 16A to FIG. 18B are views each illustrating the relation among the measured (observed) temperature distribution T act , the temperature distribution T calc calculated in a steady state before being corrected, and the temperature distribution Test after being corrected by applying the external force.
- the CPU 113 superposes a correction term U correct obtained by multiplying the element of the vector w' indicating a regression coefficient by the difference ⁇ U i of the above-mentioned fluidity on the fluidity U calc in the steady state thus calculating (estimating) the fluidity U est of the molten steel 2 after being corrected.
- a correction term U correct obtained by multiplying the element of the vector w' indicating a regression coefficient by the difference ⁇ U i of the above-mentioned fluidity on the fluidity U calc in the steady state thus calculating (estimating) the fluidity U est of the molten steel 2 after being corrected.
- the CPU 113 estimates the fluidity U est of the molten steel 2 after being corrected, by calculating the following expressions (8) and (9). Then, the processing of S6 is completed, and a series of fluidity estimation processes are terminated.
- U correct ⁇ U 1 ⁇ U 2 ⁇ U 3 ⁇ U 4 w ′
- U est U calc + U correct
- FIG. 19A is a view illustrating, as an example, the fluidity U calc before being corrected in the steady state.
- FIG. 19B is a view illustrating, as an example, fluidity (after being corrected) estimated by the fluidity estimation processing of the present embodiment.
- the CPU 113 analyzes the difference between temperature distribution calculated based on a physical model and observed temperature distribution to correct the fluidity calculated based on the physical model. Accordingly, the fluidity calculated based on the physical model is corrected with the law of conservation of mass satisfied, and thus, while excellent physical consistency is being maintained, fluidity is estimated online in three dimensions for the whole casting mold 4.
- the molten steel fluidity estimation method and the fluidity estimation device according to the present invention are capable of estimating online the fluidity of the molten steel in three dimensions for the whole casting mold thus being applicable to the continuous casting process in the continuous casting machine.
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Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2014139302A JP5935837B2 (ja) | 2014-07-07 | 2014-07-07 | 溶鋼の流動状態推定方法及び流動状態推定装置 |
PCT/JP2015/069338 WO2016006559A1 (ja) | 2014-07-07 | 2015-07-03 | 溶鋼の流動状態推定方法及び流動状態推定装置 |
Publications (3)
Publication Number | Publication Date |
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EP3167976A1 true EP3167976A1 (de) | 2017-05-17 |
EP3167976A4 EP3167976A4 (de) | 2018-05-02 |
EP3167976B1 EP3167976B1 (de) | 2018-10-31 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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EP15819360.7A Not-in-force EP3167976B1 (de) | 2014-07-07 | 2015-07-03 | Verfahren zur schätzung eines geschmolzenen stahlflussstatus und vorrichtung zur schätzung eines flussstatus |
Country Status (4)
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EP (1) | EP3167976B1 (de) |
JP (1) | JP5935837B2 (de) |
KR (1) | KR101993969B1 (de) |
WO (1) | WO2016006559A1 (de) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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US11890671B2 (en) | 2019-02-19 | 2024-02-06 | Jfe Steel Corporation | Control method for continuous casting machine, control device for continuous casting machine, and manufacturing method for casting |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
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JP6607215B2 (ja) * | 2016-03-02 | 2019-11-20 | Jfeスチール株式会社 | 溶鋼の流動状態推定方法、流動状態推定装置、溶鋼の流動状態のオンライン表示装置および鋼の連続鋳造方法 |
JP7087746B2 (ja) * | 2018-07-11 | 2022-06-21 | 日本製鉄株式会社 | 溶鋼流動制御装置、溶鋼流動制御方法、およびプログラム |
WO2020170563A1 (ja) | 2019-02-19 | 2020-08-27 | Jfeスチール株式会社 | 連続鋳造機の制御方法、連続鋳造機の制御装置、及び鋳片の製造方法 |
JP6835297B1 (ja) | 2019-03-22 | 2021-02-24 | Jfeスチール株式会社 | 鋳型内凝固シェル厚推定装置及び鋳型内凝固シェル厚推定方法 |
JP7335499B2 (ja) * | 2019-09-13 | 2023-08-30 | 日本製鉄株式会社 | 連続鋳造鋳型内可視化装置、方法、およびプログラム |
JP7332875B2 (ja) * | 2019-09-13 | 2023-08-24 | 日本製鉄株式会社 | 連続鋳造鋳型内可視化装置、方法、およびプログラム |
Family Cites Families (8)
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JPH0747453A (ja) * | 1993-08-10 | 1995-02-21 | Nippon Steel Corp | 連続鋳造における品質制御方法 |
JP3747216B2 (ja) * | 1995-05-13 | 2006-02-22 | 株式会社エビス | 連続鋳造方法及び装置 |
JPH105957A (ja) | 1996-06-26 | 1998-01-13 | Nkk Corp | 連続鋳造鋳型内における溶鋼流動検知方法及び制御方法 |
WO2000051762A1 (fr) * | 1999-03-02 | 2000-09-08 | Nkk Corporation | Procede et dispositif permettant, en coulee continue, de predire et de reguler la configuration d'ecoulement de l'acier en fusion |
JP2003181609A (ja) | 1999-03-02 | 2003-07-02 | Jfe Engineering Kk | 連続鋳造における溶鋼の流動パターン推定・制御方法およびそのための装置 |
JP3598078B2 (ja) * | 2001-06-13 | 2004-12-08 | 新日本製鐵株式会社 | 連続鋳造鋳型内の流速ベクトル分布の推定方法及び可視化方法、並びにそれらの装置。 |
DE102008055034A1 (de) * | 2008-12-19 | 2010-07-01 | Forschungszentrum Dresden - Rossendorf E.V. | Verfahren und Anordnung zur kontaktlosen Bestimmung von Geschwindigkeitsverteilungen eines flüssigen Metalls in einer Stranggießkokille |
JP4984000B1 (ja) * | 2010-09-30 | 2012-07-25 | Jfeスチール株式会社 | 流体系の温度推定方法、流体系の温度分布推定方法、流体系の温度分布モニタリング方法、温度推定装置、溶融亜鉛めっきポット内の溶融亜鉛温度制御方法、溶融亜鉛めっき鋼板、およびタンディッシュ内の溶鋼温度制御方法 |
-
2014
- 2014-07-07 JP JP2014139302A patent/JP5935837B2/ja active Active
-
2015
- 2015-07-03 KR KR1020167037070A patent/KR101993969B1/ko active IP Right Grant
- 2015-07-03 EP EP15819360.7A patent/EP3167976B1/de not_active Not-in-force
- 2015-07-03 WO PCT/JP2015/069338 patent/WO2016006559A1/ja active Application Filing
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US11890671B2 (en) | 2019-02-19 | 2024-02-06 | Jfe Steel Corporation | Control method for continuous casting machine, control device for continuous casting machine, and manufacturing method for casting |
Also Published As
Publication number | Publication date |
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KR101993969B1 (ko) | 2019-06-27 |
JP5935837B2 (ja) | 2016-06-15 |
EP3167976A4 (de) | 2018-05-02 |
WO2016006559A1 (ja) | 2016-01-14 |
EP3167976B1 (de) | 2018-10-31 |
JP2016016414A (ja) | 2016-02-01 |
KR20170013360A (ko) | 2017-02-06 |
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