EP2543265B1 - Herstellungsverfahren einer Flüssigkeit für eine elektronische Zigarette - Google Patents

Herstellungsverfahren einer Flüssigkeit für eine elektronische Zigarette Download PDF

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Publication number
EP2543265B1
EP2543265B1 EP12155467.9A EP12155467A EP2543265B1 EP 2543265 B1 EP2543265 B1 EP 2543265B1 EP 12155467 A EP12155467 A EP 12155467A EP 2543265 B1 EP2543265 B1 EP 2543265B1
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EP
European Patent Office
Prior art keywords
extract
cigarette liquid
chocolate
tobacco
chocolate powder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Not-in-force
Application number
EP12155467.9A
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English (en)
French (fr)
Other versions
EP2543265A3 (de
EP2543265A2 (de
Inventor
Junxiang Zheng
Zhixuan Zheng
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Individual
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Individual
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Publication of EP2543265A2 publication Critical patent/EP2543265A2/de
Publication of EP2543265A3 publication Critical patent/EP2543265A3/de
Application granted granted Critical
Publication of EP2543265B1 publication Critical patent/EP2543265B1/de
Not-in-force legal-status Critical Current
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Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • A24B15/303—Plant extracts other than tobacco
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/10—Devices using liquid inhalable precursors

Definitions

  • This invention relates to a kind of preparation method of E-cigarette liquid which belongs to the field of chemical preparing technology.
  • E-cigarette liquid (or E-cigarette atomizing liquid) is the popular cigarette substitute product currently. Concerning the mixing prescription, preparation process, health caring function and other aspects of E-cigarette liquid, there has been many documentary or patented reports. Mixed by 25-90 proportions of polyethylene glycol, 9-50 proportions of propylene glycol and 0.3-52 proportions of taste regulator, a kind of electronic simulation cigarette atomizing liquid disclosed by Chinese patent 200910104922.6 belongs to typical essence and spice mixing products.
  • CN101473999A discloses a kind of E-cigarette liquid mainly comprising 3-5% w/v of a tobacco leaf extract, 40-50%w/v of propylene glycol, 10-15%w/v of purified water, 3-5%w/v of tobacco flavor essence, 0.2-1 %w/v of a stabilizer, 3-8%w/v of a thickener, 0.5-4%w/v of xylitol, 0.5-4%w/v of L-arabinose and 3-9%w/v of sodium fluoride solution.
  • a method of preparing the E-cigarette liquid is not disclosed, and the ingredients as used are not substantially the same as the present invention.
  • CN101461565A also discloses a kind of E-cigarette liquid mainly comprising 3-5%w/v of tobacco leaf extract, 40-50%w/v of propylene glycol, 10-15%w/v of purified water, 3-5%w/v of tobacco flavor essence, 0.2-1.0%w/v of stabilizer, 3-8%w/v of thickener and 15-20%w/v of medicament, and the medicament may comprises various of herbal ingredients and/ or pharmaceutical ingredients.
  • a method of preparing the E-cigarette liquid is not disclosed, and the ingredients as used are not substantially the same as the present invention.
  • the purpose of this invention is to provide a kind of preparation method of E-cigarette liquid. Letting the natural aroma elements of tobacco enter the E-cigarette liquid, this method makes the aroma and taste come from the tobacco and be closer to those of cigarettes, which can cater to the smoking feeling of customers and makes the time much longer for keeping the natural aroma in cigarette liquid.
  • E-cigarette liquid should be prepared according to the plan. First, get the tobacco (weight) in an amount of 5-20% (w/v) of the E-cigarette liquid (volume) and put the tobacco into an extracting tank. Then add a mixed solvent into the extracting tank and soak the tobacco for 30-100 minutes. After heating the tobacco up to 40-60°C and extract the tobacco with warm soak for 2-8 hours to obtain an extract, filter the extract and get a filtrate. Then add chocolate extract in an amount of 1-10% (w/v) of the E-cigarette liquid into the filtrate to obtain a mixture, and stir the mixture for 20-40 minutes.
  • the preparation of the mixed solvent above is to respectively get the propylene glycol and/or polyethylene glycol in an amount of 30-80% w/v of the E-cigarette liquid and 0.1-0.5% w/v of tween 80, and then stir them for 20-40 minutes to get the uniformly mixed solvent.
  • the preparation of chocolate extract above includes the following steps: Smash chocolate to 20-60 sections to obtain chocolate powder and put the chocolate powder into an extracting tank with interlayer, add distilled water in a weight 3-10 times of the chocolate powder, soak the chocolate powder for 30-90 minutes and heat the chocolate powder up to 80-90°C, extract the chocolate powder with heat preservation for 2-6 hours to obtain a chocolate powder extract, pour out and filter the chocolate powder extract and keep the residue for other functions, then decompress and concentrate the chocolate powder extract to unconcentrated extract in a proportion of 1.1-1.4 to get the chocolate extract.
  • propylene glycol or polyethylene glycol solvent and tween 80 above are all with the officinal or edible level, among which propylene glycol and polyethylene glycol can be used solely as well as in combination.
  • Case 1 Plan to prepare 500 liters of E-cigarette liquid. Get 50 kilograms of tobacco and put into the extracting tank with interlayer; respectively get 350 liters of propylene glycol and 1 liter of tween 80, then pour the latter into the former and stir the mixture for 30 minutes. Add the mixed liquor into the extracting tank and soak the tobacco for 50 minutes. Then use steam to heat it up to 50°C through the interlayer. After extracting with heat preservation for 4 hours, pour out the extract and filter it to get the filtrate. Add 18 kilograms of chocolate extract into the filtrate and stir the mixture for 30 minutes. Then add 500 liters of propylene glycol into the filtrate to complement the planning preparation and stir the mixture for 35 minutes to get the E-cigarette liquid.
  • Case 2 Plan to prepare 500 liters of E-cigarette liquid. Get 50 kilograms of tobacco and put into the extracting tank with interlayer; get and mix 380 liters of propylene glycol and polyethylene glycol according to the proportion of 1:1, and get 1.5 liters of tween 80. Pour the tween 80 into the mixture of propylene glycol and polyethylene glycol and stir it for 40 minutes and then add it to the extracting tank and soak the tobacco for 60 minutes. Use steam to heat it up to 60°C through the interlayer. After extracting with heat preservation for 6 hours, pour out the extract and filter it to get the filtrate. Add 20 kilograms of chocolate extract into the filtrate and stir the mixture for 40 minutes. Then add 500 liters of polyethylene glycol into the filtrate and stir the mixture for 30 minutes to get the E-cigarette liquid.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Claims (3)

  1. Verfahren zum Herstellen von E-Zigaretten-Flüssigkeit, dadurch gekennzeichnet, dass das Verfahren die Schritte umfasst:
    Beschaffen von Tabak in einer Menge von 5 - 20 % Gewicht/Volumen (G/V) der E-Zigaretten-Flüssigkeit und Geben des Tabaks in einen Extraktionstank;
    Zugeben eines gemischten Lösemittels in den Extraktionstank und Einweichenlassen des Tabaks während 30 - 100 Minuten, wobei es das Verfahren zum Herstellen des gemischten Lösemittels ist, jeweils das Propylenglycol und/oder das Polyethylenglycol in einer Menge von 30 - 80 % G/V der E-Zigaretten-Flüssigkeit und 0,1 - 0,5 % G/V Tween 80 zu beschaffen und diese dann 20 - 40 Minuten lang zu rühren;
    Erhitzen des Tabaks auf 40 - 60 °C und Extrahieren des Tabaks unter warmem Einweichen während 2 - 8 Stunden, um einen Extrakt zu gewinnen;
    Filtern des Extraktes, um ein Filtrat zu gewinnen;
    Zugeben von Schokoladenextrakt in einer Menge von 1 - 10 % G/V der E-Zigaretten-Flüssigkeit in das Filtrat, um ein Gemisch zu gewinnen, und dann Rühren des Gemisches während 20 - 40 Minuten;
    danach Ergänzen der E-Zigaretten-Flüssigkeit zu 100 % eines Volumens der E-Zigaretten-Flüssigkeit, wie geplant, um durch Zugeben von Propylenglycol oder Polyethylenglycol hergestellt zu werden, um ein zweites Gemisch zu gewinnen, und dann Rühren des zweiten Gemisches, bis das zweite Gemisch einheitlich ist, wobei folglich die E-Zigaretten-Flüssigkeit gewonnen wird.
  2. Verfahren zum Herstellen von E-Zigaretten-Flüssigkeit nach Anspruch 1, dadurch gekennzeichnet, dass der Schokoladenextrakt durch die folgenden Schritte hergestellt wird:
    Zertrümmern von Schokolade zu 20 - 60 Abschnitten, um Schokoladenpulver zu gewinnen, und Geben des Schokoladenpulvers in einen Extraktionstank mit Zwischenschicht;
    Zugeben von destilliertem Wasser in einem Gewicht von dem 3- bis 10-fachen des Schokoladenpulvers;
    Einweichenlassen des Schokoladenpulvers während 30 - 90 Minuten und Erhitzen des Schokoladenpulvers auf 80 - 90 °C;
    Extrahieren des Schokoladenpulvers unter Wärmeerhaltung während 2 - 6 Stunden, um einen Schokoladenpulverextrakt zu gewinnen;
    Ausgießen und Filtern des Schokoladenpulverextraktes, dann Dekomprimieren und Konzentrieren des Schokoladenpulverextraktes in einem Verhältnis von 1,1 - 1,4 in Bezug auf unkonzentrierten Extrakt, um den Schokoladenextrakt zu erhalten.
  3. Verfahren zum Herstellen von E-Zigaretten-Flüssigkeit nach Anspruch 1, dadurch gekennzeichnet, dass das Propylenglycol und das Polyethylenglycol allein benutzt werden oder in Kombination benutzt werden.
EP12155467.9A 2011-07-04 2012-02-14 Herstellungsverfahren einer Flüssigkeit für eine elektronische Zigarette Not-in-force EP2543265B1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2011101840686A CN102349699B (zh) 2011-07-04 2011-07-04 一种电子烟液的制备方法

Publications (3)

Publication Number Publication Date
EP2543265A2 EP2543265A2 (de) 2013-01-09
EP2543265A3 EP2543265A3 (de) 2014-12-10
EP2543265B1 true EP2543265B1 (de) 2017-09-13

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Country Status (8)

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US (1) US20130008457A1 (de)
EP (1) EP2543265B1 (de)
JP (1) JP5752008B2 (de)
CN (1) CN102349699B (de)
CA (1) CA2766749A1 (de)
RU (1) RU2542547C2 (de)
TW (1) TW201302106A (de)
WO (1) WO2013004160A1 (de)

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JP5752008B2 (ja) 2015-07-22
RU2542547C2 (ru) 2015-02-20
EP2543265A3 (de) 2014-12-10
JP2013013394A (ja) 2013-01-24
CA2766749A1 (en) 2013-01-04
EP2543265A2 (de) 2013-01-09
CN102349699A (zh) 2012-02-15
CN102349699B (zh) 2013-07-03
US20130008457A1 (en) 2013-01-10
TW201302106A (zh) 2013-01-16
WO2013004160A1 (zh) 2013-01-10
TWI477237B (de) 2015-03-21

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