EP2543265A2 - Herstellungsverfahren für Flüssigkeit für eine elektronischen Zigarette - Google Patents
Herstellungsverfahren für Flüssigkeit für eine elektronischen Zigarette Download PDFInfo
- Publication number
- EP2543265A2 EP2543265A2 EP12155467A EP12155467A EP2543265A2 EP 2543265 A2 EP2543265 A2 EP 2543265A2 EP 12155467 A EP12155467 A EP 12155467A EP 12155467 A EP12155467 A EP 12155467A EP 2543265 A2 EP2543265 A2 EP 2543265A2
- Authority
- EP
- European Patent Office
- Prior art keywords
- cigarette liquid
- preparation
- extract
- tobacco
- minutes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/10—Devices using liquid inhalable precursors
Definitions
- This invention relates to a kind of preparation method of E-cigarette liquid which belongs to the field of chemical preparing technology.
- E-cigarette liquid (or E-cigarette atomizing liquid) is the popular cigarette substitute product currently. Concerning the mixing prescription, preparation process, health caring function and other aspects of E-cigarette liquid, there has been many documentary or patented reports. Mixed by 25-90 proportions of polyethylene glycol, 9-50 proportions of propylene glycol and 0.3-52 proportions of taste regulator, a kind of electronic simulation cigarette atomizing liquid disclosed by Chinese patent 200910104922.6 belongs to typical essence and spice mixing products.
- the purpose of this invention is to provide a kind of preparation method of E-cigarette liquid. Letting the natural aroma elements of tobacco enter the E-cigarette liquid, this method makes the aroma and taste come from the tobacco and be closer to those of cigarettes, which can cater to the smoking feeling of customers and makes the time much longer for keeping the natural aroma in cigarette liquid.
- E-cigarette liquid should be prepared according to the plan. First, get the tobacco (weight) with 5-20% (w/v) of E-cigarette liquid amount (volume) and put into the extracting tank. Then add the mixed solvent into the tank and soak the tobacco for 30-100 minutes. After heating it up to 40-60°C and extract with warm soak for 2-8 hours, filter the extract and get the filtrate. Then add chocolate extract with the amount of 1-10% (w/v) of the E-cigarette liquid into the filtrate and stir the mixture for 20-40 minutes. After that, complement the E-cigarette liquid volume of 100% planning preparation with propylene glycol or polyethylene glycol and stir them until mix uniformly to finish the product.
- the preparation of the solvent above is to respectively get the propylene glycol and/or polyethylene glycol with the amount of 30-80% of the E-cigarette liquid volume and 0.1-0.5% of tween 80, and then stir them for 20-40 minutes to get the uniformly mixed solvent;
- the preparation of chocolate extractive above includes the following steps. Smash the chocolate to 20-60 sections and put into the extracting tank with interlayer, add distilled water of which the weight is 3-10 times of the chocolate powder, soak the powder for 30-90 minutes and heat it up to 80-90°C, extract with heat preservation for 2-6 hours, pour out and filter the extract and keep the residue for other functions, then decompress and concentrate the extract to the extract with the proportion of 1.1-1.4 to get the chocolate extractive;
- propylene glycol or polyethylene glycol solvent and tween 80 above are all with the officinal or edible level, among which propylene glycol and polyethylene glycol can be used solely as well as in combination.
- Case 1 Plan to prepare 500 liters of E-cigarette liquid. Get 50 kilograms of tobacco and put into the extracting tank with interlayer; respectively get 350 liters of propylene glycol and 1 liter of tween 80, then pour the latter into the former and stir the mixture for 30 minutes. Add the mixed liquor into the extracting tank and soak the tobacco for 50 minutes. Then use steam to heat it up to 50°C through the interlayer. After extracting with heat preservation for 4 hours, pour out the extract and filter it to get the filtrate. Add 18 kilograms of chocolate extractive into the filtrate and stir the mixture for 30 minutes. Then add 500 liters of propylene glycol into the filtrate to complement the planning preparation and stir the mixture for 35 minutes to get the E-cigarette liquid.
- Case 2 Plan to prepare 500 liters of E-cigarette liquid. Get 50 kilograms of tobacco and put into the extracting tank with interlayer; get and mix 380 liters of propylene glycol and polyethylene glycol according to the proportion of 1:1, and get 1.5 liters of tween 80. Pour the tween 80 into the mixture of propylene glycol and polyethylene glycol and stir it for 40 minutes and then add it to the extracting tank and soak the tobacco for 60 minutes. Use steam to heat it up to 60°C through the interlayer. After extracting with heat preservation for 6 hours, pour out the extract and filter it to get the filtrate. Add 20 kilograms of chocolate extractive into the filtrate and stir the mixture for 40 minutes. Then add 500 liters of polyethylene glycol into the filtrate and stir the mixture for 30 minutes to get the E-cigarette liquid.
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Manufacture Of Tobacco Products (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Extraction Or Liquid Replacement (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2011101840686A CN102349699B (zh) | 2011-07-04 | 2011-07-04 | 一种电子烟液的制备方法 |
Publications (3)
Publication Number | Publication Date |
---|---|
EP2543265A2 true EP2543265A2 (de) | 2013-01-09 |
EP2543265A3 EP2543265A3 (de) | 2014-12-10 |
EP2543265B1 EP2543265B1 (de) | 2017-09-13 |
Family
ID=45573426
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP12155467.9A Not-in-force EP2543265B1 (de) | 2011-07-04 | 2012-02-14 | Herstellungsverfahren einer Flüssigkeit für eine elektronische Zigarette |
Country Status (8)
Country | Link |
---|---|
US (1) | US20130008457A1 (de) |
EP (1) | EP2543265B1 (de) |
JP (1) | JP5752008B2 (de) |
CN (1) | CN102349699B (de) |
CA (1) | CA2766749A1 (de) |
RU (1) | RU2542547C2 (de) |
TW (1) | TW201302106A (de) |
WO (1) | WO2013004160A1 (de) |
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CN103622154A (zh) * | 2013-12-17 | 2014-03-12 | 郑悦 | 电子烟液及其制备方法 |
EP2815741A1 (de) * | 2013-06-20 | 2014-12-24 | Changning Dekang Biotechnology Co., Ltd | Orale, zerstäubte Flüssigkeit mit nikotinsubstitutiertem Cytisin und deren Herstellungsverfahren |
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WO2017144400A1 (fr) | 2016-02-23 | 2017-08-31 | Thomas Boudier | Dispositif de filtration avec compression |
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US10034988B2 (en) | 2012-11-28 | 2018-07-31 | Fontem Holdings I B.V. | Methods and devices for compound delivery |
US10194693B2 (en) | 2013-09-20 | 2019-02-05 | Fontem Holdings 1 B.V. | Aerosol generating device |
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JP4824571B2 (ja) * | 2003-11-03 | 2011-11-30 | ユーエス スモークレス タバコ カンパニー リミテッド ライアビリティ カンパニー | 香味付け無煙たばこおよび製造方法 |
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CN101731750B (zh) * | 2008-03-26 | 2012-08-22 | 修运强 | 一种电子模拟香烟雾化液 |
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US20110036365A1 (en) * | 2009-08-17 | 2011-02-17 | Chong Alexander Chinhak | Vaporized tobacco product and methods of use |
CN102905565B (zh) * | 2010-05-21 | 2016-08-24 | 环球蒸汽商标公司 | 制备用于电吸烟设备的烟草提取物的方法 |
CN101862026B (zh) * | 2010-06-07 | 2013-04-17 | 中国烟草总公司郑州烟草研究院 | 一种无烟气烟草制品添加剂及其制备方法和应用 |
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CN102349699B (zh) * | 2011-07-04 | 2013-07-03 | 郑俊祥 | 一种电子烟液的制备方法 |
-
2011
- 2011-07-04 CN CN2011101840686A patent/CN102349699B/zh active Active
- 2011-10-27 JP JP2011235884A patent/JP5752008B2/ja not_active Expired - Fee Related
- 2011-11-22 TW TW100142675A patent/TW201302106A/zh not_active IP Right Cessation
-
2012
- 2012-01-30 RU RU2012102830/12A patent/RU2542547C2/ru not_active IP Right Cessation
- 2012-02-07 CA CA2766749A patent/CA2766749A1/en not_active Abandoned
- 2012-02-14 EP EP12155467.9A patent/EP2543265B1/de not_active Not-in-force
- 2012-03-31 US US13/436,839 patent/US20130008457A1/en not_active Abandoned
- 2012-07-02 WO PCT/CN2012/078053 patent/WO2013004160A1/zh active Application Filing
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US10034988B2 (en) | 2012-11-28 | 2018-07-31 | Fontem Holdings I B.V. | Methods and devices for compound delivery |
EP3010824B1 (de) * | 2013-06-18 | 2018-07-18 | Vallar, Ramon, Manolo | Verfahren zum nachfüllen einer elektronische zigarette |
EP2815741A1 (de) * | 2013-06-20 | 2014-12-24 | Changning Dekang Biotechnology Co., Ltd | Orale, zerstäubte Flüssigkeit mit nikotinsubstitutiertem Cytisin und deren Herstellungsverfahren |
CN103349355A (zh) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | 黑胡椒乌梅复合提取物及其制备方法和作为烟草制品添加剂的用途 |
CN103349355B (zh) * | 2013-06-28 | 2016-03-09 | 湖北中烟工业有限责任公司 | 黑胡椒乌梅复合提取物及其制备方法和作为烟草制品添加剂的用途 |
US10194693B2 (en) | 2013-09-20 | 2019-02-05 | Fontem Holdings 1 B.V. | Aerosol generating device |
CN103622154A (zh) * | 2013-12-17 | 2014-03-12 | 郑悦 | 电子烟液及其制备方法 |
WO2015192834A3 (de) * | 2014-06-18 | 2016-04-14 | Klaus Hagen | Verfahren zur herstellung eines zur verdampfung vorgesehenen verbrauchsstoffs |
CN104473323A (zh) * | 2014-12-03 | 2015-04-01 | 河南中烟工业有限责任公司 | 一种电子烟雾化剂 |
US10588351B2 (en) | 2015-06-29 | 2020-03-17 | Philip Morris Products S.A. | Cartridge and device for an aerosol-generating system |
WO2017144400A1 (fr) | 2016-02-23 | 2017-08-31 | Thomas Boudier | Dispositif de filtration avec compression |
Also Published As
Publication number | Publication date |
---|---|
RU2012102830A (ru) | 2013-08-10 |
EP2543265B1 (de) | 2017-09-13 |
JP2013013394A (ja) | 2013-01-24 |
CN102349699A (zh) | 2012-02-15 |
RU2542547C2 (ru) | 2015-02-20 |
JP5752008B2 (ja) | 2015-07-22 |
US20130008457A1 (en) | 2013-01-10 |
EP2543265A3 (de) | 2014-12-10 |
CA2766749A1 (en) | 2013-01-04 |
CN102349699B (zh) | 2013-07-03 |
TWI477237B (de) | 2015-03-21 |
WO2013004160A1 (zh) | 2013-01-10 |
TW201302106A (zh) | 2013-01-16 |
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