TW201302106A - 一種電子煙液的製備方法 - Google Patents
一種電子煙液的製備方法 Download PDFInfo
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/10—Devices using liquid inhalable precursors
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- Manufacture Of Tobacco Products (AREA)
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- Extraction Or Liquid Replacement (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
本發明涉及一種電子煙液的製備方法，秤取電子煙液量的5-20%的煙葉投入提取罐，將配製好的溶媒加入到提取罐中浸泡煙葉30-100分鐘，加熱至40-60℃，溫浸提取2-8小時，過濾提取液，向濾液中加入電子煙液量的1-10%的可可豆提取物，攪拌混合20-40分鐘；再以丙二醇或聚乙二醇補足到100%計劃製備的電子煙液體積，攪拌混合均勻即得電子煙液。該法使煙葉中的天然香氣成分進入電子煙液，使電子煙液的香氣、口味基本是來自煙葉的，能更接近香煙的香氣，更能迎合消費者的品煙感覺，還能使進入煙液中的天然香氣成分留香時間更長。
Description
本發明涉及一種電子煙液的製備方法。屬於化工製備技術領域。
電子煙液(或稱電子煙霧化液)是目前流行的香煙替代產品。關於電子煙液的調配處方、製備過程，以及其保健功能等方面，已經有許多的文獻或專利報導。中國專利200910104922.6公開的一種電子模擬香煙霧化液，以聚乙二醇25-90份，丙二醇9-50份，以及口感味道調節劑0.3-52份調配而成，屬於典型的香精香料調配產品。中國專利200910310536.2公開的電子香煙霧化液，以煙葉提取物3-5%w/v，煙草香精3-5%w/v，煙鹼0-3%w/v，穩定劑0.2-1%w/v，增稠劑3-8%w/v，純水5-10%w/v，丙二醇50-70%w/v，以及其他如磷酸可待因、撲爾敏等調配而成，雖然使用了煙葉提取物，但仍然是模仿香煙口味以煙葉提取物與其他香精香料調配的產品。由於越來越多的吸煙者開始接受使用電子煙代替香煙，用於這些電子煙的電子煙液的一些不足也就越來越明顯。吸煙者普遍反應，電子煙與香煙相比，雖然形狀、手感、煙霧等感覺像香煙，但在香氣、口味等方面，與品香煙的感覺差距比較大，尤其以各種香精香料調配成的產品，他們難以接受或習慣其香氣和口味。另外，目前電子煙液的香氣成分難以長期保留，最好的也只能存放半年左右，“煙味”就很淡或幾乎沒有了，這也是使用者普遍反應的問題。這些不足，大大影響了電子煙的品質，同時也限制電子煙的普及和流行。
本發明的目的是針對電子煙液存在的香氣、口味差，以及留香時間短等不足，提供一種電子煙液的製備方法。該法使煙葉中的天然香氣成分進入電子煙液，使電子煙液的香氣、口味基本是來自煙葉的，能更接近香煙的香氣，更能迎合消費者的品煙感覺，還能使進入煙液中的天然香氣成分留香時間更長。
本發明係依據以下技術方案實施：
按計劃製備一定量的電子煙液。秤取電子煙液量(體積)5-20%(w/v)的煙葉(重量)投入提取罐，將配製好的溶媒加入到提取罐中浸泡煙葉30-100分鐘，加熱至40-60℃温浸提取2-8小時，過濾提取液得濾液，向濾液中加入電子煙液量的1-10%(w/v)的可可豆提取物，攪拌混合20-40分鐘；再以丙二醇或聚乙二醇補足到100%計劃製備的電子煙液體積，攪拌混合均勻即得電子煙液。
所述的溶媒的配製是分別量取電子煙液量30-80%的丙二醇和/或聚乙二醇及0.1-0.5%的吐温80，將二者攪拌混合20-40分鐘，得到混合均勻的溶媒；所述的可可豆提取物，是將可可豆粉碎至20-60目，投入帶夾層的提取罐，加入可可豆粉重量的3-10倍蒸餾水，浸泡可可豆粉30-90分鐘，加熱升温至80-90℃，保温提取2-6小時，放出並過濾提取液，濾渣留作它用，濾液減壓濃縮至比重為1.1-1.4的浸膏，即得可可豆提取物；所述的丙二醇或聚乙二醇溶媒及吐温80，均為藥用或食用級別，丙二醇和聚乙二醇可以單獨用，也可以混合用。
本發明與現有技術相比的優點及積極效果：
以含吐温80的丙二醇或聚乙二醇溶媒作提取液，在比較温和的條件下直接提取煙葉，一是煙葉的香氣成分直接進入提取液，二是在温和條件下提取煙葉，會避免複雜工序及高温濃縮條件下對某些易揮發或對温度比較敏感的煙葉香氣成分的損失和破壞，另外，與其他常用的提取香氣成分的溶媒比較，由於丙二醇或聚乙二醇等溶媒粘度大、有一定的保濕性能等特點，對香氣成分會有更好的保留作用。本發明的電子煙液經過大量試用者使用後，一致反應口味接近香煙的口味，他們更喜歡這種電子煙液，而且本發明的電子煙液存放二至三年，香氣仍然能很好的保留。
實例1：計劃製備500升的電子煙液。秤取50公斤煙葉，投入帶夾層的提取罐中；分別量取350升丙二醇和1升吐温80，將吐温80倒入丙二醇中並攪拌混合30分鐘，將此混合液加入至提取罐中浸泡煙葉50分鐘，然後向夾層中通入蒸汽加熱升温至50℃，保温浸提4小時後，放出提取液並過濾得濾液，向濾液中加入18公斤可可豆提取物，攪拌混合30分鐘，再向濾液中加入丙二醇補足至計劃製備的500升，再攪拌混合35分鐘，即得所述電子煙液。
實例2：計劃製備500升的電子煙液。秤取50公斤煙葉，投入帶夾層的提取罐中；先按1：1的比例量取丙二醇和聚乙二醇380升混合，再量取1.5升吐温80，將吐温80倒入丙二醇和聚乙二醇混合液中並攪拌混合40分鐘，加入至提取罐中浸泡煙葉60分鐘，然後向夾層中通入蒸汽加熱升温至60℃，保温浸提6小時後，放出提取液並過濾得濾液，向濾液中加入20公斤可可豆提取物，攪拌混合40分鐘；再向濾液中加入聚乙二醇補足至500升，攪拌混合30分鐘，即得所述電子煙液。
Claims (4)
- 一種電子煙液的製備方法，其包括下列步驟：秤取電子煙液量5-20% w/v的煙葉投入提取罐，將配製好的溶媒加入到提取罐中浸泡煙葉30-100分鐘後加熱至40-60℃温浸提取2-8小時，過濾提取液，向濾液中加入電子煙液量的1-10% w/v的可可豆提取物，攪拌混合20-40分鐘，再以丙二醇或聚乙二醇補足到100%計劃製備的電子煙液體積，攪拌混合均勻即得電子煙液。
- 依據請求項1所述的電子煙液的製備方法，其中所述的溶媒的配製是分別量取電子煙液體積量的30-80%的丙二醇和/或聚乙二醇及0.1-0.5%的吐温80，將二者攪拌混合20-40分鐘，得到混合均勻的溶媒。
- 依據請求項1所述的電子煙液的製備方法，其中所述的可可豆提取物，是將可可豆粉碎至20-60目，投入帶夾層的提取罐，加入可可豆粉重量的3-10倍蒸餾水，浸泡可可豆粉30-90分鐘，加熱升温至80-90℃，保温提取2-6小時，放出並過濾提取液，濾液減壓濃縮至比重為1.1-1.4的浸膏，即得可可豆提取物。
- 依據請求項1所述的電子煙液的製備方法，其中所述的丙二醇或聚乙二醇溶媒及吐温80，均為藥用或食用級別，丙二醇和聚乙二醇單獨用或混合用。
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011101840686A CN102349699B (zh) | 2011-07-04 | 2011-07-04 | 一种电子烟液的制备方法 |
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| Publication Number | Publication Date |
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| TW201302106A true TW201302106A (zh) | 2013-01-16 |
| TWI477237B TWI477237B (zh) | 2015-03-21 |
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| TW100142675A TW201302106A (zh) | 2011-07-04 | 2011-11-22 | 一種電子煙液的製備方法 |
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| Country | Link |
|---|---|
| US (1) | US20130008457A1 (zh) |
| EP (1) | EP2543265B1 (zh) |
| JP (1) | JP5752008B2 (zh) |
| CN (1) | CN102349699B (zh) |
| CA (1) | CA2766749A1 (zh) |
| RU (1) | RU2542547C2 (zh) |
| TW (1) | TW201302106A (zh) |
| WO (1) | WO2013004160A1 (zh) |
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| WO2013004160A1 (zh) | 2013-01-10 |
| RU2012102830A (ru) | 2013-08-10 |
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