Classifications

• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
  • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
  • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
  • B01F25/40—Static mixers
  • B01F25/44—Mixers in which the components are pressed through slits
  • B01F25/441—Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits
  • B01F25/4413—Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits the slits being formed between opposed conical or cylindrical surfaces
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
  • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
  • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
  • B01F25/40—Static mixers
  • B01F25/44—Mixers in which the components are pressed through slits
  • B01F25/441—Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits
  • B01F25/4416—Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits the opposed surfaces being provided with grooves
  • B01F25/44162—Circumferential grooves formed on opposed surfaces, e.g. on planar surfaces or on cylinders or cones
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
  • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
  • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
  • B01F25/40—Static mixers
  • B01F25/44—Mixers in which the components are pressed through slits
  • B01F25/441—Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits
  • B01F25/4416—Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits the opposed surfaces being provided with grooves
  • B01F25/44167—Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits the opposed surfaces being provided with grooves the grooves being formed on the outer surface of the cylindrical or conical core of the slits
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
  • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
  • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
  • B01F35/71—Feed mechanisms
  • B01F35/717—Feed mechanisms characterised by the means for feeding the components to the mixer
  • B01F35/7174—Feed mechanisms characterised by the means for feeding the components to the mixer using pistons, plungers or syringes
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
  • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
  • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
  • B01F35/71—Feed mechanisms
  • B01F35/717—Feed mechanisms characterised by the means for feeding the components to the mixer
  • B01F35/71805—Feed mechanisms characterised by the means for feeding the components to the mixer using valves, gates, orifices or openings
• • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
  • F04—POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
  • F04B—POSITIVE-DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS
  • F04B53/00—Component parts, details or accessories not provided for in, or of interest apart from, groups F04B1/00 - F04B23/00 or F04B39/00 - F04B47/00

Definitions

• the invention relates to an apparatus for homogenizing liquid and musty substances, consisting of a high-pressure pump with a crank drive and at least one piston guided in a cylinder block and driven by connecting rods and push rods, connected to a homogenizing device arranged on the cylinder block and having a homogenizing head which consists of a bushing with a smooth-walled, conical through-bore to be widened towards the outlet side and a piston arranged in it and held by axial prestressing, which has a solid body of essentially truncated cone.
• % has a shaped lateral surface on which axially successive annular steps are formed, each of which abuts the through bore with its outer circumference.
• the high-pressure pump is designed as a piston pump, the piston of which is driven by a crank mechanism with a flanged motor via connecting rods and push rods.
• the actual homogenizing device namely the homogenizing head with the stamp, is arranged directly on the cylinder block of the piston pump.
• the liquid to be homogenized is sucked into the cylinder by the pistons in the reverse gear through inlet ports and pressed out of the cylinder through the homogenizing head during the compression process.
• Such devices can work without inlet or outlet valves and several pistons can also act on the homogenizing head in a parallel manner.
• a disadvantage of these known homogenizers is that the pistons operate in an uneven manner due to the parallel operation. In order to avoid this disadvantage, it is known that the pistons are not offset in parallel, but offset depending on the number.
• each cylinder In order to do without valves in such a design, each cylinder must be assigned its own homogenizing head.
• Continuous passage through the homogenizing head is advantageous for good dispersion of the liquids. This can be achieved in that, in the case of a multi-cylinder design with at least two cylinders acting on a single homogenizing head, valves are provided both on the inlet connection and on the outlet side of the cylinder head.
• a further critical point in the formation of homogenizing devices is the formation of the stamp contained in the homogenizing head. It is known to design the stamps with axially successive annular steps so that they contain the longitudinal axis of the stamp of the body Cut have the shape of a rectangle. The steps are consequently in contact with the conical passage bore with frustoconical ring surfaces, the size of which depends on the height of the individual steps. Recesses of the same height are provided between the steps, in which the substance to be homogenized can swirl and re-mix after passing through a step. All stages have the same height and therefore each absorb the same amount of the substance before they pass the next stage.
• the object of the invention is to design an apparatus of the aforementioned type in such a way that the disadvantages mentioned above are eliminated and, in particular, a homogenizing device is created which has an even better dispersibility and at the same time a better hourly output. Furthermore, it should be achieved that the better dispersion performance is possible at lower pressure, so that the substance to be homogenized is treated more gently and, for example, suffers less heating and at the same time the substance is not only finely dispersed but also mixed particularly well. This output should also be met for more viscous or pulpy substances, the aim being to make the homogenizing device less susceptible to blockages
• This object is achieved according to the invention in an apparatus of the type mentioned in the introduction in that an intermediate chamber to be opened is arranged between the homogenizing device and the cylinder block of the high-pressure pump.
• This embodiment of the homogenizing device according to the invention ensures that it can be charged with compressed substance by more than one pressure cylinder when the pistons are operating in a non-parallel manner, thereby ensuring a much more continuous supply. Furthermore, the possibility of being able to open the intermediate chamber makes it easy to clean both the homogenizing head and the outlet valves.
• the intermediate chamber consists of a first chamber part, which is attached to the end of the cylinder block, and a second chamber part which is detachably connected to it and carries the homogenizing device.
• the separating joint of the two chamber parts is advantageously arranged in a plane perpendicular to the axes of the cylinder arranged in parallel in the cylinder block and the homogenizing device mounted on a wall of the second chamber part parallel to the parting line in such a way that the longitudinal axis of the plunger is parallel to the axes of the cylinders.
• the second chamber part is held on the first chamber part by a hinge with a hinge axis parallel to the parting line. This makes opening the intermediate chamber much easier and can be done without removing the movable part of the chamber.
• an outlet valve installed between the compression space of the respective cylinder and the intermediate chamber can be removed when the second chamber part is open. This ensures that the outlet valves through which the highly compressed substance flows can be cleaned or even replaced as quickly as possible without the need for major assembly or disassembly of the homogenizing device.
• a valve plate contained in the valves is based on a circular one
• Base plate with an outer diameter d. which corresponds to the largest a inner diameter of the valves, arranged at an angular distance of ⁇ * 30 ° in the outer edge of the base plate, four segment-shaped recesses which comprise an angle of 60, the inner diameter d . is greater than
• valve plate ensures that the valves are closed and thus sealed, particularly when processing pulpy substances.
• the high-pressure pump designed with horizontal cylinders is connected by a trough to the crankcase receiving the crankshaft drive and sealingly designed straight guides, the trough receives the straight guides with the connecting rods connecting the pistons and annular sleeves are arranged on the connecting rods.
• the arrangement of a trough between the straight guides and the cylinder block of the high-pressure pump prevents the oil contained in the crankcase from being mixed with the substance to be homogenized and possibly emerging from the cylinders.
• the arrangement of the sleeves on the push rods makes it possible to arrange the homogenizing device in a horizontal manner, since the sleeves prevent the oil from overflowing along the push rods. This possibility of arranging the homogenizing device in a horizontal manner in turn results in easier operation of the intermediate chamber part with homogenizing device and thus better accessibility to the valves.
• the cylinder block is provided with bores which can be heated or cooled by the liquid.
• the cylinder block of the high-pressure pump can be cooled or warmed by a suitably prepared liquid.
• each step of the stamp has two flanks which meet in an annular cutting edge and are arranged in a section in the form of a triangle which contains the longitudinal axis of the body, the triangle passing through the through hole ⁇ lying tip going bisector is essentially in a radial plane of the body.
• the configuration according to the invention ensures that the contact surface between the bore and the punch pressed in with axial preload is kept to a minimum while maintaining the smooth-walled, conical and therefore easily producible passage bore.
• the steps of the stamp form, with the passage bore, linear ring-shaped cutting edges, between which the substance to be homogenized is cut.
• the tip angle is v-. which is enclosed by the two flanks forming the ring cutting edge of each step, 60.
• the axial spacing of the radial planes passing through the annular cutting edges successively is advantageously alternately substantially equal to the length of the triangle side opposite the tip or substantially equal to twice the value.
• the punch has a total of seven steps, each with an annular cutting edge, two steps with the small spacing being provided at the outlet end and. has at the outlet end, arranged after the ring cutting edges, at least three centering lugs projecting beyond the circumference of the ring cutting edges, which are guided in recesses with cylindrical outer surfaces which are provided in the through bore of the bushing.
• This design according to the invention has the advantage that the punch is centered on the passage bore even when its ring cutters are not in contact and as a result the annular gaps between the individual ring cutters and the passage bore always have the same distance distributed over the circumference. This prevents that when the punch is pressurized by the liquid to be homogenized, the punch does not abut one side with its ring cutting edges against the through-hole and thus the sharp-edged ring cutting edges are very quickly worn or destroyed unevenly.
• the distance between the ring cutting edges assigned to the inlet end and the outlet end is substantially equal to the diameter of the latter ring cutting edge
• the conical pitch of the through hole is in the range from 1: 0.15 to 1: 0.05 and the diameter of the the cutting edge assigned to the outlet end is 5 . Centimeter.
• Fig. 1 is a perspective view of the apparatus for
• FIG. 3 shows a section along line III-III in FIG. 2,
• W1PO _ ⁇ ,, NAT ⁇ ⁇ > 5 is a plan view of the homogenizing head from the outlet side
• Fig. 6 is a view of a valve plate.
• FIG. 1 shows the apparatus for homogenizing 1, which essentially consists of the drive block Z. of the high pressure pump 3, the intermediate chamber 4 and the homogenizing device 5.
• the homogenizing apparatus 1 works in a lying arrangement and is driven by a motor (not shown) via a crankshaft 6.
• two connecting rods 8 are driven by the crankshaft 6 via eccentric disks 7.
• the connecting rods 8 are movably attached with their upper end to push rods 9 and are mounted in straight guides 10.
• the push rods 9 emerge from the straight guides 10 and are sealed against the oil-filled crankcase 11 with push rod seals 12.
• the push rods 9 transmit the lifting movements of the connecting rods 8 to pistons 14 movable in bushings 13 (shown in FIGS. 2 and 3). Before entry into the bushings 13, the push rods 9 bridge a trough 15, which may emerge from the crankcase 11 should catch emerging l. So that any escaping oil cannot reach the bushings along the stroke movements of the push rods ' , 9 cuff rings are arranged on the push rods, which cause the oil to be thrown off by the movement of the push rods 9. On the other hand, the interposition of the trough 15 and the arrangement of the sleeves 16 ensure that the substance to be homogenized cannot get into the crankcase 11 either.
• Ip the cylinder block 3 bores 17 a are provided, which can be charged with the cylinder warming or cooling liquid as required.
• FIGS. 2 and 3 show the high pressure pump 3, the intermediate chamber 4 and the homogenizing device 5.
• the end of the piston 14 shown in FIGS. 2 and 3 runs in a bushing 13, preferably made of bronze, which is mounted in the cylinder block 17 of the high-pressure pump 3.
• a bushing 13 preferably made of bronze, which is mounted in the cylinder block 17 of the high-pressure pump 3.
• the compression chamber 18 At the end of the liner 13 is the compression chamber 18, into which the inlet opening 20 provided with an inlet valve 19 leads perpendicular to the axis of the piston 14 or the compression chamber 18.
• the inlet valve 19 contains a valve plate 21 which, when the pressure in the compression space 18 rises, bears against sealing rings 22 and the inlet Closes opening 20.
• a line supplying the substance to be homogenized is connected to the inlet connection 23.
• the valve plate 21 is shown in FIG. 6. Starting from a circular base plate with an outer diameter d, which corresponds to the largest inner diameter of the valve 19, recesses 24 in the form of circular segments are arranged at an angular spacing of 0.degree. To 30 ° in the outer edge of the base plate and have an angle of .beta - Include 60. The inner diameter d touching these circular recesses 24. is larger than the diameter of the inlet opening 20.
• valve plate 21 is pressed against the sealing rings 22 and closes the inlet opening 20.
• the substance to be homogenized can pass through the inlet opening 20 and the circular recesses 24 between the webs 25 in the valve plate 21 enter the compression space 18.
• the entire valve 19 can be screwed out together with the inlet connection 23 and is sealed off from the cylinder block 17 by a seal 26.
• An outlet valve 27 is arranged in the axial extension of the compression space 18.
• the structure of this outlet valve 27 with valve plate and sealing rings corresponds to that of valve 19. It is also sealed off from cylinder block 17 with seals 26.
• the intermediate chamber 4 connects to the cylinder block 17 of the high-pressure pump 3.
• the intermediate chamber 4 forms the connection between the individual compression spaces 18 or cylinders and the homogenizing device 5. So that the outlet valve 27 can be replaced easily and in a short time, the intermediate chamber 4 is formed in two parts and consists of the first chamber part attached to the high-pressure pump 3 28 and a detachably connected second chamber part 29 carrying the homogenizing device 5.
• the parting line 30 of the two chamber parts 28 and 29 is arranged in a plane perpendicular to the axis of the cylinder arranged in parallel axis in the cylinder block 17 and the second chamber part 29 is through a hinge 31 with hinge axes 32 parallel to the parting plane is held on the first chamber part 28, so that after removing the wing screws 33 the second chamber part 29 can be folded down from the first chamber part 28 like a door.
• the hinge 31 is designed such that the second chamber part 29 can be removed to such an extent that access to the outlet valves 27 is free and there is sufficient scope to unscrew these valves and also to be able to clean the intermediate chamber.
• the intermediate chamber 4 is connected to a special manometer 34, which indicates the pressure contained in this chamber.
• the homogenizing device is built on a wall 35 of the second chamber part 29 parallel to the parting line in such a way that the longitudinal axis of the punch 36 is parallel to the axes of the cylinders.
• the homogenizing device 5 essentially consists of the two-part homogenizing head 37 and a pretensioning device 38 which can be actuated by hand.
• the socket 40 of the two-part homogenizing head 37 connects to the outlet opening 39 provided in the wall 35 of the second chamber part 29 of the intermediate chamber 4 .
• the socket 40 is screwed into a flange 41 with a thread and closes off against the wall 35 of the second chamber part 29 of the intermediate chamber 4 with a seal 42.
• the bushing 40 of the homogenizing head 37 has a smooth-walled conical bore 43 to be widened towards the outlet side, into which a stamp 36 of the homogenizing head 37 provided with axially successively arranged annular steps 63 is pressed.
• This stamp 36 is four centering lugs 44, which are arranged downstream of the steps 63 towards the outlet end and protrude beyond the circumference of these steps 63, into recesses 45 with cylindrical jacket surfaces 45 a, which are arranged in the bushing 40.
• the punch 36 is mounted with its shaft 46 in the outlet direction in a housing 47 so that it can be moved longitudinally.
• the housing 47 is provided with an enlarged bore 48 at its lower end and is placed with the radial flange 49 on the bush 40 of the two-part homogenizing head 37.
• a cap nut 50 is screwed onto the external thread of the flange 41 and holds the housing 47 firmly on a bead 51.
• a seal 52 is provided between the bush 40 of the two-part homogenizing head 37 and the bead 51 of the housing.
• the shaft 46 of the stamp 36 is mounted in the housing 47 in an annular web 53 with a seal 54.
• a lower pressure plate 55 rests on the end of the shaft 46 above the annular web 53.
• a plate spring 56 is arranged above this pressure plate 55, which in turn connects upwards to an upper pressure plate 57.
• a spindle 58 is screwed through the housing plate 59 and can be adjusted with a handwheel 60, so that the plate spring 56 is more or less compressed and the inner punch 36 of the two-part homogenizing head 37 is correspondingly strong the conical bore of the bush 40 is pressed.
• An outlet connection 61 is provided above the two-part homogenizing head 37.
• the two-part homogenizing head 37 is shown in FIG. 4.
• the plunger 36 of the homogenizing head 37 has, in axial succession on its solid body 62 of essentially frustoconical lateral surface 62 ', annular steps 63 which are located in one containing the longitudinal axis of the body Cross-section have a triangular shape and with their flanks 65, each forming an annular cutting edge 64, bear against the wall of the conical bore 43 of the bush 40.
• the bisector passing through the tip of the angle f of approximately 60 ° between the acute angle f enclosed by the flanks 65 lies essentially in a radial plane * of the body 62.
• the axial distance A of the radial planes passing through the annular cutting edges 64 successive steps 63 is essentially equal to the length of the triangle side opposite the tip or substantially twice the value in the next step arranged.
• annular recesses 67 are formed in the body 62 of the punch 36, each of which has the shape of a triangle on a section containing the longitudinal axis of the body, the flanks 68 of the recesses being in the flanks Extend 65 of the adjoining steps 63.
• the punch 36 of the homogenizing head 37 has a total of seven steps 63, each with an annular cutting edge 64, two steps being initially arranged with the small spacing, seen from the outlet end.
• the distance between the first annular cutting edges arranged at the inlet end and at the outlet end is substantially equal to the diameter of the annular cutting edge arranged at the outlet end.
• the diameter of this ring cutter is 5 centimeters, while the conical pitch of the through hole 43 is in the range from 1: 0.15 to 1: 0.05.
• the punch 36 is finally provided with an obtuse-angled cone 69 at its inlet end.
• the above-described embodiment of the device according to the invention is used in the production of foods, such as Margarine, mayonnaises, dairy products, pasta, sauces of all kinds, mustard etc. as well as used in the manufacture of emulsions, creams, pastes and ointments for cosmetics, medicines and chemical-technical products.
• Such a homogenizing device is particularly suitable for use in the production of paints. So far, the colors were only rubbed on roller mills in the course of the production process with a great deal of time. However, it is now possible to disperse such a pulpy substance with the above-described homogenizing device. It is possible to repeat the homogenization process and it is an advantage that the color changes its color after each pass. It is essential that each individual dispersion process
• OMPI is more time-saving than the rubbing process on the known roller mills.
• the substance to be homogenized is sucked into the compression space 18 through the inlet valve 19 and the inlet nozzle 23.
• the pressure in the compression space 18 is increased and the inlet valve 19 closes.
• the outlet valve 27 opens and the substance located in the compression chamber 18 is compressed and pressed into the intermediate chamber 4.
• the plunger 36 of the two-part homogenizing head 37 guided with its centering lugs 44 in the recesses 45 of the bush 40 is pressed slightly upward against the prestress caused by the plate spring 56, so that the compacted substance between the ring edges 64 of the plunger 36 and the smooth one Wall of the bore 43 of the socket 40 can pass through.
• the substance is cut or cut between the ring edges 64 and the wall of the bore 43 and at the same time intensely swirled in the differently sized recesses 67 between the ring edges 64 and again homogenized by the subsequent ring edges 64. After passing through the homogenizing head, the substance can emerge from the outlet nozzle 61.

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• Chemical & Material Sciences (AREA)
• Chemical Kinetics & Catalysis (AREA)
• Dispersion Chemistry (AREA)
• Engineering & Computer Science (AREA)
• Mechanical Engineering (AREA)
• General Engineering & Computer Science (AREA)
• Details Of Reciprocating Pumps (AREA)
• Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)

Applications Claiming Priority (2)

Publications (1)

Family

ID=6012961

Family Applications (1)

Country Status (8)

Families Citing this family (16)

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• 1977
  • 1977-07-01 DE DE2729855A patent/DE2729855C2/de not_active Expired
• 1978
  • 1978-06-26 US US06/015,952 patent/US4333729A/en not_active Expired - Lifetime
  • 1978-06-26 CH CH329879A patent/CH632937A5/de not_active IP Right Cessation
  • 1978-06-26 WO PCT/EP1978/000002 patent/WO1979000020A1/de not_active Ceased
  • 1978-06-26 GB GB7906899A patent/GB2035817B/en not_active Expired
  • 1978-06-26 DE DE78EP7800002T patent/DE2856969D2/de not_active Expired
• 1979
  • 1979-01-30 EP EP78900030A patent/EP0006863A1/de active Pending
  • 1979-03-01 SE SE7901878A patent/SE425596B/sv unknown
  • 1979-12-26 FR FR7932096A patent/FR2443276A1/fr active Granted

Non-Patent Citations (1)

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