EA201990713A1 - Способ и устройство для количественного анализа технологического потока газа - Google Patents
Способ и устройство для количественного анализа технологического потока газаInfo
- Publication number
- EA201990713A1 EA201990713A1 EA201990713A EA201990713A EA201990713A1 EA 201990713 A1 EA201990713 A1 EA 201990713A1 EA 201990713 A EA201990713 A EA 201990713A EA 201990713 A EA201990713 A EA 201990713A EA 201990713 A1 EA201990713 A1 EA 201990713A1
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- quantitative analysis
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- technological gas
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/0004—Gaseous mixtures, e.g. polluted air
- G01N33/0006—Calibrating gas analysers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/008—Feed or outlet control devices
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
- B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
- B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
- B01J8/0457—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being placed in separate reactors
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/24—Automatic injection systems
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/64—Electrical detectors
- G01N30/68—Flame ionisation detectors
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/64—Electrical detectors
- G01N30/70—Electron capture detectors
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00796—Details of the reactor or of the particulate material
- B01J2208/00946—Features relating to the reactants or products
- B01J2208/00955—Sampling of the particulate material, the reactants or the products
- B01J2208/00964—Reactants
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00245—Avoiding undesirable reactions or side-effects
- B01J2219/00247—Fouling of the reactor or the process equipment
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/18—Polyhydroxylic acyclic alcohols
- C07C31/20—Dihydroxylic alcohols
- C07C31/202—Ethylene glycol
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
- C07D317/32—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D317/34—Oxygen atoms
- C07D317/36—Alkylene carbonates; Substituted alkylene carbonates
- C07D317/38—Ethylene carbonate
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N2030/022—Column chromatography characterised by the kind of separation mechanism
- G01N2030/025—Gas chromatography
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
- G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
- G01N2030/884—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds
- G01N2030/8845—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds involving halogenated organic compounds
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
- G01N2030/8886—Analysis of industrial production processes
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Combustion & Propulsion (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Sampling And Sample Adjustment (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Epoxy Compounds (AREA)
Abstract
Настоящее изобретение относится к способу и устройству для количественного анализа технологического потока газа, в частности, потока, получаемого посредством процесса получения этиленкарбоната и/или этиленгликоля, в частности, когда такой поток содержит газообразные органические иодиды.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP16193878 | 2016-10-14 | ||
PCT/EP2017/076069 WO2018069445A1 (en) | 2016-10-14 | 2017-10-12 | Method and apparatus for quantitatively analyzing a gaseous process stream |
Publications (2)
Publication Number | Publication Date |
---|---|
EA201990713A1 true EA201990713A1 (ru) | 2019-09-30 |
EA037588B1 EA037588B1 (ru) | 2021-04-19 |
Family
ID=57153327
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EA201990713A EA037588B1 (ru) | 2016-10-14 | 2017-10-12 | Способ и устройство для количественного анализа технологического потока газа |
Country Status (8)
Country | Link |
---|---|
US (2) | US11408869B2 (ru) |
EP (1) | EP3526601B1 (ru) |
KR (1) | KR102499556B1 (ru) |
CN (1) | CN109791134A (ru) |
BR (1) | BR122023008656B1 (ru) |
EA (1) | EA037588B1 (ru) |
TW (1) | TWI772330B (ru) |
WO (1) | WO2018069445A1 (ru) |
Families Citing this family (6)
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TWI772330B (zh) | 2016-10-14 | 2022-08-01 | 荷蘭商蜆殼國際研究所 | 用於定量分析氣態製程流之方法及設備 |
WO2019110713A1 (en) | 2017-12-08 | 2019-06-13 | Shell Internationale Research Maatschappij B.V. | Process for preparing ethylene carbonate and ethylene glycol |
CN110441101B (zh) * | 2018-05-04 | 2022-07-01 | 研能科技股份有限公司 | 气相层析设备的分离系统 |
CN109490447B (zh) * | 2019-01-11 | 2023-11-17 | 国网安徽省电力有限公司电力科学研究院 | 一种六氟化硫混合气体混合比色谱检测装置 |
CN112394113A (zh) * | 2019-08-15 | 2021-02-23 | 中国石油化工股份有限公司 | 一种液化烃原料中氯杂质在线监测系统、方法及应用 |
CN111679038B (zh) * | 2020-06-17 | 2023-08-11 | 中国计量科学研究院 | 一种烟气排放二氧化碳浓度的在线自校准监测仪 |
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GB201402782D0 (en) | 2014-02-17 | 2014-04-02 | Johnson Matthey Davy Technologies Ltd | Process |
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US20170129827A1 (en) | 2014-07-04 | 2017-05-11 | Sabic Global Technologies B.V. | A process for converting natural gas to higher hydrocarbon(s) |
KR102579625B1 (ko) | 2014-09-24 | 2023-09-18 | 쉘 인터내셔날 리써취 마트샤피지 비.브이. | 알킬렌 글리콜의 제조 방법 및 제조 장치 |
TWI723100B (zh) | 2015-12-15 | 2021-04-01 | 荷蘭商蜆殼國際研究所 | 從環氧乙烷製造中的循環氣體流移除烷基碘雜質之方法及系統 |
TWI740863B (zh) | 2015-12-15 | 2021-10-01 | 荷蘭商蜆殼國際研究所 | 防護床系統及方法 |
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KR20180093935A (ko) | 2015-12-15 | 2018-08-22 | 쉘 인터내셔날 리써취 마트샤피지 비.브이. | 에틸렌 옥사이드의 제조 시 재순환 가스 스트림으로부터 요오드화비닐 불순물을 제거하기 위한 방법 및 시스템 |
TWI772330B (zh) | 2016-10-14 | 2022-08-01 | 荷蘭商蜆殼國際研究所 | 用於定量分析氣態製程流之方法及設備 |
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2017
- 2017-10-11 TW TW106134644A patent/TWI772330B/zh active
- 2017-10-12 US US16/341,216 patent/US11408869B2/en active Active
- 2017-10-12 CN CN201780062019.0A patent/CN109791134A/zh active Pending
- 2017-10-12 BR BR122023008656-2A patent/BR122023008656B1/pt active IP Right Grant
- 2017-10-12 KR KR1020197010241A patent/KR102499556B1/ko active IP Right Grant
- 2017-10-12 EA EA201990713A patent/EA037588B1/ru unknown
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KR20190069420A (ko) | 2019-06-19 |
BR122023008656B1 (pt) | 2023-10-24 |
TWI772330B (zh) | 2022-08-01 |
TW201819885A (zh) | 2018-06-01 |
EP3526601A1 (en) | 2019-08-21 |
EP3526601B1 (en) | 2020-04-15 |
EA037588B1 (ru) | 2021-04-19 |
US11774420B2 (en) | 2023-10-03 |
WO2018069445A1 (en) | 2018-04-19 |
BR112019007010A2 (pt) | 2019-06-25 |
CN109791134A (zh) | 2019-05-21 |
US11408869B2 (en) | 2022-08-09 |
KR102499556B1 (ko) | 2023-02-14 |
US20220334095A1 (en) | 2022-10-20 |
US20190317065A1 (en) | 2019-10-17 |
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