DK168330B1 - Fremgangsmåde til fremstilling af transparente, uklarhedsfrie tinoxidbelægninger - Google Patents
Fremgangsmåde til fremstilling af transparente, uklarhedsfrie tinoxidbelægninger Download PDFInfo
- Publication number
- DK168330B1 DK168330B1 DK013687A DK13687A DK168330B1 DK 168330 B1 DK168330 B1 DK 168330B1 DK 013687 A DK013687 A DK 013687A DK 13687 A DK13687 A DK 13687A DK 168330 B1 DK168330 B1 DK 168330B1
- Authority
- DK
- Denmark
- Prior art keywords
- tin oxide
- substrate
- cloudless
- glass
- oxide coating
- Prior art date
Links
- 238000000576 coating method Methods 0.000 title claims description 70
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 title claims description 70
- 229910001887 tin oxide Inorganic materials 0.000 title claims description 70
- 238000000034 method Methods 0.000 title claims description 29
- 239000011521 glass Substances 0.000 claims description 42
- 239000011248 coating agent Substances 0.000 claims description 39
- UBOGEXSQACVGEC-UHFFFAOYSA-K phenyltin(3+);trichloride Chemical compound Cl[Sn](Cl)(Cl)C1=CC=CC=C1 UBOGEXSQACVGEC-UHFFFAOYSA-K 0.000 claims description 28
- 239000000758 substrate Substances 0.000 claims description 26
- YMLFYGFCXGNERH-UHFFFAOYSA-K butyltin trichloride Chemical compound CCCC[Sn](Cl)(Cl)Cl YMLFYGFCXGNERH-UHFFFAOYSA-K 0.000 claims description 15
- DTQVDTLACAAQTR-UHFFFAOYSA-N Trifluoroacetic acid Chemical compound OC(=O)C(F)(F)F DTQVDTLACAAQTR-UHFFFAOYSA-N 0.000 claims description 8
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 6
- 239000002019 doping agent Substances 0.000 claims description 6
- 239000001301 oxygen Substances 0.000 claims description 6
- 229910052760 oxygen Inorganic materials 0.000 claims description 6
- 150000003606 tin compounds Chemical class 0.000 claims description 6
- 229910052731 fluorine Inorganic materials 0.000 claims description 2
- 239000011737 fluorine Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims 1
- 230000000873 masking effect Effects 0.000 description 10
- 239000012159 carrier gas Substances 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 6
- 239000010410 layer Substances 0.000 description 6
- 230000005540 biological transmission Effects 0.000 description 5
- 238000000151 deposition Methods 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 238000010276 construction Methods 0.000 description 4
- 230000008021 deposition Effects 0.000 description 4
- 229910021627 Tin(IV) chloride Inorganic materials 0.000 description 3
- ISKQADXMHQSTHK-UHFFFAOYSA-N [4-(aminomethyl)phenyl]methanamine Chemical compound NCC1=CC=C(CN)C=C1 ISKQADXMHQSTHK-UHFFFAOYSA-N 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- HPGGPRDJHPYFRM-UHFFFAOYSA-J tin(iv) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 description 3
- STSCVKRWJPWALQ-UHFFFAOYSA-N TRIFLUOROACETIC ACID ETHYL ESTER Chemical compound CCOC(=O)C(F)(F)F STSCVKRWJPWALQ-UHFFFAOYSA-N 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- 238000005229 chemical vapour deposition Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- PKKGKUDPKRTKLJ-UHFFFAOYSA-L dichloro(dimethyl)stannane Chemical compound C[Sn](C)(Cl)Cl PKKGKUDPKRTKLJ-UHFFFAOYSA-L 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- QAEDZJGFFMLHHQ-UHFFFAOYSA-N trifluoroacetic anhydride Chemical compound FC(F)(F)C(=O)OC(=O)C(F)(F)F QAEDZJGFFMLHHQ-UHFFFAOYSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- VUYQBMXVCZBVHP-UHFFFAOYSA-N 1,1-difluoroethanol Chemical compound CC(O)(F)F VUYQBMXVCZBVHP-UHFFFAOYSA-N 0.000 description 1
- LRMSQVBRUNSOJL-UHFFFAOYSA-N 2,2,3,3,3-pentafluoropropanoic acid Chemical compound OC(=O)C(F)(F)C(F)(F)F LRMSQVBRUNSOJL-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- VOPWNXZWBYDODV-UHFFFAOYSA-N Chlorodifluoromethane Chemical compound FC(F)Cl VOPWNXZWBYDODV-UHFFFAOYSA-N 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- GCTFWCDSFPMHHS-UHFFFAOYSA-M Tributyltin chloride Chemical compound CCCC[Sn](Cl)(CCCC)CCCC GCTFWCDSFPMHHS-UHFFFAOYSA-M 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000007605 air drying Methods 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- RJGHQTVXGKYATR-UHFFFAOYSA-L dibutyl(dichloro)stannane Chemical compound CCCC[Sn](Cl)(Cl)CCCC RJGHQTVXGKYATR-UHFFFAOYSA-L 0.000 description 1
- AYOHIQLKSOJJQH-UHFFFAOYSA-N dibutyltin Chemical compound CCCC[Sn]CCCC AYOHIQLKSOJJQH-UHFFFAOYSA-N 0.000 description 1
- UTLYKVGGKZYRRQ-UHFFFAOYSA-L dibutyltin(2+);difluoride Chemical compound CCCC[Sn](F)(F)CCCC UTLYKVGGKZYRRQ-UHFFFAOYSA-L 0.000 description 1
- PXBRQCKWGAHEHS-UHFFFAOYSA-N dichlorodifluoromethane Chemical compound FC(F)(Cl)Cl PXBRQCKWGAHEHS-UHFFFAOYSA-N 0.000 description 1
- 235000019404 dichlorodifluoromethane Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- -1 monophenyl tin tin chloride Chemical compound 0.000 description 1
- ODOPKAJVFRHHGM-UHFFFAOYSA-N phenyltin Chemical compound [Sn]C1=CC=CC=C1 ODOPKAJVFRHHGM-UHFFFAOYSA-N 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- AFCAKJKUYFLYFK-UHFFFAOYSA-N tetrabutyltin Chemical compound CCCC[Sn](CCCC)(CCCC)CCCC AFCAKJKUYFLYFK-UHFFFAOYSA-N 0.000 description 1
- GOWIXKGLTIIPQR-UHFFFAOYSA-K tribromo(ethyl)stannane Chemical compound CC[Sn](Br)(Br)Br GOWIXKGLTIIPQR-UHFFFAOYSA-K 0.000 description 1
- YFRLQYJXUZRYDN-UHFFFAOYSA-K trichloro(methyl)stannane Chemical compound C[Sn](Cl)(Cl)Cl YFRLQYJXUZRYDN-UHFFFAOYSA-K 0.000 description 1
- YSCVYRUCAPMZFG-UHFFFAOYSA-K trichlorotin Chemical class Cl[Sn](Cl)Cl YSCVYRUCAPMZFG-UHFFFAOYSA-K 0.000 description 1
- 238000007740 vapor deposition Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D3/00—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/22—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
- C23C16/30—Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
- C23C16/40—Oxides
- C23C16/407—Oxides of zinc, germanium, cadmium, indium, tin, thallium or bismuth
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D5/00—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures
- B05D5/12—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures to obtain a coating with specific electrical properties
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
- C03C17/23—Oxides
- C03C17/245—Oxides by deposition from the vapour phase
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
- C03C17/23—Oxides
- C03C17/245—Oxides by deposition from the vapour phase
- C03C17/2453—Coating containing SnO2
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Metallurgy (AREA)
- Mechanical Engineering (AREA)
- Inorganic Chemistry (AREA)
- Surface Treatment Of Glass (AREA)
- Chemical Vapour Deposition (AREA)
- Paints Or Removers (AREA)
Applications Claiming Priority (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/733,997 US4600654A (en) | 1985-05-14 | 1985-05-14 | Method of producing transparent, haze-free tin oxide coatings |
| US73399785 | 1985-05-14 | ||
| US79302385A | 1985-10-30 | 1985-10-30 | |
| US79302385 | 1985-10-30 | ||
| US80255185 | 1985-11-27 | ||
| US06/802,551 US4737388A (en) | 1985-05-14 | 1985-11-27 | Non-iridescent, haze-free infrared reflecting coated glass structures |
| PCT/US1986/000890 WO1986006658A1 (en) | 1985-05-14 | 1986-04-25 | Method of producing transparent, haze-free tin oxide coatings |
| US8600890 | 1986-04-25 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DK13687A DK13687A (da) | 1987-01-12 |
| DK13687D0 DK13687D0 (da) | 1987-01-12 |
| DK168330B1 true DK168330B1 (da) | 1994-03-14 |
Family
ID=27419186
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DK013687A DK168330B1 (da) | 1985-05-14 | 1987-01-12 | Fremgangsmåde til fremstilling af transparente, uklarhedsfrie tinoxidbelægninger |
Country Status (16)
| Country | Link |
|---|---|
| EP (1) | EP0225342B1 (https=) |
| KR (1) | KR920007956B1 (https=) |
| CN (1) | CN1015185B (https=) |
| AU (1) | AU576676B2 (https=) |
| BR (1) | BR8606673A (https=) |
| CA (1) | CA1268673A (https=) |
| DE (1) | DE3673612D1 (https=) |
| DK (1) | DK168330B1 (https=) |
| ES (1) | ES8800365A1 (https=) |
| FI (1) | FI83416C (https=) |
| IE (1) | IE58959B1 (https=) |
| IL (1) | IL78736A (https=) |
| IN (1) | IN170102B (https=) |
| MX (1) | MX163869B (https=) |
| TR (1) | TR23083A (https=) |
| WO (1) | WO1986006658A1 (https=) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5102721A (en) * | 1987-08-31 | 1992-04-07 | Solarex Corporation | Textured tin oxide |
| US4880664A (en) * | 1987-08-31 | 1989-11-14 | Solarex Corporation | Method of depositing textured tin oxide |
| WO1989003114A1 (fr) * | 1987-09-30 | 1989-04-06 | Catalysts & Chemicals Industries Co., Ltd. | Base revetue de ceramique conductive transparente, procede de production et son utilisation |
| WO1990002157A1 (fr) * | 1988-08-24 | 1990-03-08 | Catalysts & Chemicals Industries Co., Ltd. | Fluide de revetement formant un revetement ceramique conducteur transparent, materiau de base revetu de ceramique conductrice transparente, production dudit materiau et applications de ce materiau de base revetu de ceramique conductrice transparente |
| JPH02258691A (ja) * | 1989-03-31 | 1990-10-19 | Agency Of Ind Science & Technol | 透明導電膜の製造方法 |
| US5233465A (en) * | 1992-05-27 | 1993-08-03 | The Dow Chemical Company | Visibly transparent infrared reflecting film with color masking |
| AU4386399A (en) * | 1998-07-10 | 2000-02-01 | Gilles Merienne | Liquid precursor for chemical vapor deposition |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3406085A (en) * | 1964-05-11 | 1968-10-15 | Corning Glass Works | Photochromic window |
| US3420693A (en) * | 1964-06-05 | 1969-01-07 | Ball Brothers Co Inc | Glass having dual protective coatings thereon and a method for forming such coatings |
| US3949146A (en) * | 1973-08-24 | 1976-04-06 | Rca Corporation | Process for depositing transparent electrically conductive tin oxide coatings on a substrate |
| US4265974A (en) * | 1976-11-01 | 1981-05-05 | Gordon Roy G | Electrically conductive, infrared reflective, transparent coatings of stannic oxide |
| US4440822A (en) * | 1977-04-04 | 1984-04-03 | Gordon Roy G | Non-iridescent glass structures |
| US4459789A (en) * | 1982-05-20 | 1984-07-17 | Ford Donald F | Window |
| US4590096A (en) * | 1984-12-28 | 1986-05-20 | M&T Chemicals Inc. | Water vapor, reaction rate and deposition rate control of tin oxide film by CVD on glass |
| US4547400A (en) * | 1985-02-25 | 1985-10-15 | Ford Motor Company | Method of making infrared reflective glass sheet-I |
| US4548836A (en) * | 1985-02-25 | 1985-10-22 | Ford Motor Company | Method of making an infrared reflective glass sheet-II |
-
1986
- 1986-04-25 KR KR1019870700025A patent/KR920007956B1/ko not_active Expired
- 1986-04-25 WO PCT/US1986/000890 patent/WO1986006658A1/en not_active Ceased
- 1986-04-25 BR BR8606673A patent/BR8606673A/pt not_active IP Right Cessation
- 1986-04-25 AU AU58103/86A patent/AU576676B2/en not_active Ceased
- 1986-04-25 EP EP86903044A patent/EP0225342B1/en not_active Expired - Lifetime
- 1986-04-25 DE DE8686903044T patent/DE3673612D1/de not_active Expired - Fee Related
- 1986-04-29 IN IN384/DEL/86A patent/IN170102B/en unknown
- 1986-05-08 MX MX2429A patent/MX163869B/es unknown
- 1986-05-08 IL IL78736A patent/IL78736A/xx not_active IP Right Cessation
- 1986-05-13 IE IE126186A patent/IE58959B1/en not_active IP Right Cessation
- 1986-05-13 ES ES554900A patent/ES8800365A1/es not_active Expired
- 1986-05-13 CA CA000509005A patent/CA1268673A/en not_active Expired - Fee Related
- 1986-05-14 CN CN86103417A patent/CN1015185B/zh not_active Expired
- 1986-05-14 TR TR267/86A patent/TR23083A/xx unknown
-
1987
- 1987-01-09 FI FI870078A patent/FI83416C/fi not_active IP Right Cessation
- 1987-01-12 DK DK013687A patent/DK168330B1/da not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| FI870078A0 (fi) | 1987-01-09 |
| EP0225342A1 (en) | 1987-06-16 |
| AU576676B2 (en) | 1988-09-01 |
| TR23083A (tr) | 1989-03-13 |
| CN86103417A (zh) | 1986-11-12 |
| IE861261L (en) | 1986-11-14 |
| ES8800365A1 (es) | 1987-11-01 |
| DK13687A (da) | 1987-01-12 |
| ES554900A0 (es) | 1987-11-01 |
| IL78736A (en) | 1989-03-31 |
| CA1268673A (en) | 1990-05-08 |
| KR870700415A (ko) | 1987-12-29 |
| FI83416B (fi) | 1991-03-28 |
| FI870078L (fi) | 1987-01-09 |
| EP0225342B1 (en) | 1990-08-22 |
| MX163869B (es) | 1992-06-29 |
| CN1015185B (zh) | 1991-12-25 |
| EP0225342A4 (en) | 1987-08-12 |
| IL78736A0 (en) | 1986-08-31 |
| FI83416C (fi) | 1991-07-10 |
| DE3673612D1 (de) | 1990-09-27 |
| KR920007956B1 (ko) | 1992-09-19 |
| BR8606673A (pt) | 1987-08-11 |
| IE58959B1 (en) | 1993-12-01 |
| IN170102B (https=) | 1992-02-08 |
| AU5810386A (en) | 1986-12-04 |
| DK13687D0 (da) | 1987-01-12 |
| WO1986006658A1 (en) | 1986-11-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B1 | Patent granted (law 1993) | ||
| PBP | Patent lapsed |