DE94399C - - Google Patents

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Publication number

DE94399C

DE94399C DENDAT94399D DE94399DA DE94399C DE 94399 C DE94399 C DE 94399C DE NDAT94399 D DENDAT94399 D DE NDAT94399D DE 94399D A DE94399D A DE 94399DA DE 94399 C DE94399 C DE 94399C

Authority

DE

Germany

Prior art keywords

acid

red

iron

parts

solution

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 12
• 229910052742 iron Inorganic materials 0.000 claims description 6
• NWCVEHKBLWQPKB-UHFFFAOYSA-N C12=C(S(O)(=O)=O)C([N+]([O-])=O)=C([N+]([O-])=O)C=C2C2=CC=C3C=C4C=CC=CC4=CC3=C2C2=C1C(S(=O)(=O)O)C(=O)C1=CC=CC=C12 Chemical compound C12=C(S(O)(=O)=O)C([N+]([O-])=O)=C([N+]([O-])=O)C=C2C2=CC=C3C=C4C=CC=CC4=CC3=C2C2=C1C(S(=O)(=O)O)C(=O)C1=CC=CC=C12 NWCVEHKBLWQPKB-UHFFFAOYSA-N 0.000 claims description 5
• 230000002378 acidificating effect Effects 0.000 claims description 4
• 239000003638 chemical reducing agent Substances 0.000 claims description 3
• HKOOXMFOFWEVGF-UHFFFAOYSA-N phenylhydrazine Chemical compound NNC1=CC=CC=C1 HKOOXMFOFWEVGF-UHFFFAOYSA-N 0.000 claims description 3
• 229940067157 phenylhydrazine Drugs 0.000 claims description 3
• 230000007935 neutral effect Effects 0.000 claims description 2
• 238000000034 method Methods 0.000 claims 1
• 230000004048 modification Effects 0.000 claims 1
• 238000012986 modification Methods 0.000 claims 1
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
• 239000000243 solution Substances 0.000 description 6
• QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 5
• 239000002253 acid Substances 0.000 description 3
• 239000000975 dye Substances 0.000 description 3
• 210000002268 wool Anatomy 0.000 description 3
• IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
• VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 2
• BDKZHNJTLHOSDW-UHFFFAOYSA-N [Na].CC(O)=O Chemical compound [Na].CC(O)=O BDKZHNJTLHOSDW-UHFFFAOYSA-N 0.000 description 2
• 229960000583 acetic acid Drugs 0.000 description 2
• 239000003929 acidic solution Substances 0.000 description 2
• 238000004040 coloring Methods 0.000 description 2
• BFMYDTVEBKDAKJ-UHFFFAOYSA-L disodium;(2',7'-dibromo-3',6'-dioxido-3-oxospiro[2-benzofuran-1,9'-xanthene]-4'-yl)mercury;hydrate Chemical compound O.[Na+].[Na+].O1C(=O)C2=CC=CC=C2C21C1=CC(Br)=C([O-])C([Hg])=C1OC1=C2C=C(Br)C([O-])=C1 BFMYDTVEBKDAKJ-UHFFFAOYSA-L 0.000 description 2
• 239000000047 product Substances 0.000 description 2
• 235000002639 sodium chloride Nutrition 0.000 description 2
• BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical compound OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 description 2
• UWOGELSGKTUEAK-UHFFFAOYSA-N 9-oxoheptacyclo[16.12.0.02,11.03,8.012,17.021,30.023,28]triaconta-1,3,5,7,11,13,15,17,19,21,23,25,27,29-tetradecaene-10,13-disulfonic acid Chemical compound C1(C(C=2C3=C(C=CC=C3C3=C(C2C=2C=CC=CC12)C1=CC2=CC=CC=C2C=C1C=C3)S(=O)(=O)O)S(=O)(=O)O)=O UWOGELSGKTUEAK-UHFFFAOYSA-N 0.000 description 1
• -1 Dinitroanthraquinone disulfonic acid Chemical compound 0.000 description 1
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
• ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
• FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
• 239000003513 alkali Substances 0.000 description 1
• 239000012670 alkaline solution Substances 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• 230000015572 biosynthetic process Effects 0.000 description 1
• 239000007795 chemical reaction product Substances 0.000 description 1
• 239000000706 filtrate Substances 0.000 description 1
• 239000012362 glacial acetic acid Substances 0.000 description 1
• UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 1
• 235000013980 iron oxide Nutrition 0.000 description 1
• SURQXAFEQWPFPV-UHFFFAOYSA-L iron(2+) sulfate heptahydrate Chemical compound O.O.O.O.O.O.O.[Fe+2].[O-]S([O-])(=O)=O SURQXAFEQWPFPV-UHFFFAOYSA-L 0.000 description 1
• VBMVTYDPPZVILR-UHFFFAOYSA-N iron(2+);oxygen(2-) Chemical class [O-2].[Fe+2] VBMVTYDPPZVILR-UHFFFAOYSA-N 0.000 description 1
• 229910000359 iron(II) sulfate Inorganic materials 0.000 description 1
• 239000011259 mixed solution Substances 0.000 description 1
• 239000000983 mordant dye Substances 0.000 description 1
• 229910052757 nitrogen Inorganic materials 0.000 description 1
• 239000003960 organic solvent Substances 0.000 description 1
• 229910052700 potassium Inorganic materials 0.000 description 1
• 239000011591 potassium Substances 0.000 description 1
• 238000001953 recrystallisation Methods 0.000 description 1
• 238000005185 salting out Methods 0.000 description 1
• 150000003839 salts Chemical class 0.000 description 1
• 239000011780 sodium chloride Substances 0.000 description 1
• 159000000000 sodium salts Chemical class 0.000 description 1
• GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 1
• 239000002904 solvent Substances 0.000 description 1
• QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
• SWGJCIMEBVHMTA-UHFFFAOYSA-K trisodium;6-oxido-4-sulfo-5-[(4-sulfonatonaphthalen-1-yl)diazenyl]naphthalene-2-sulfonate Chemical compound [Na+].[Na+].[Na+].C1=CC=C2C(N=NC3=C4C(=CC(=CC4=CC=C3O)S([O-])(=O)=O)S([O-])(=O)=O)=CC=C(S([O-])(=O)=O)C2=C1 SWGJCIMEBVHMTA-UHFFFAOYSA-K 0.000 description 1
• 239000002966 varnish Substances 0.000 description 1