DE916253C - Verfahren zur Erzeugung von Oberflaechenschichten auf Eisen und Stahl - Google Patents
Verfahren zur Erzeugung von Oberflaechenschichten auf Eisen und StahlInfo
- Publication number
- DE916253C DE916253C DEW608A DEW0000608A DE916253C DE 916253 C DE916253 C DE 916253C DE W608 A DEW608 A DE W608A DE W0000608 A DEW0000608 A DE W0000608A DE 916253 C DE916253 C DE 916253C
- Authority
- DE
- Germany
- Prior art keywords
- iron
- steel
- surface layers
- alkali
- layers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 title claims description 26
- 229910052742 iron Inorganic materials 0.000 title claims description 14
- 238000000034 method Methods 0.000 title claims description 13
- 239000002344 surface layer Substances 0.000 title claims description 7
- 229910000831 Steel Inorganic materials 0.000 title claims description 6
- 239000010959 steel Substances 0.000 title claims description 6
- 238000004519 manufacturing process Methods 0.000 title description 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 30
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 15
- 239000000243 solution Substances 0.000 claims description 15
- 239000003513 alkali Substances 0.000 claims description 11
- XTEGARKTQYYJKE-UHFFFAOYSA-M Chlorate Chemical compound [O-]Cl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-M 0.000 claims description 9
- 235000006408 oxalic acid Nutrition 0.000 claims description 9
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 7
- 239000004254 Ammonium phosphate Substances 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 3
- 239000003929 acidic solution Substances 0.000 claims description 3
- 150000007513 acids Chemical class 0.000 claims description 3
- 235000019289 ammonium phosphates Nutrition 0.000 claims description 3
- VBIXEXWLHSRNKB-UHFFFAOYSA-N ammonium oxalate Chemical compound [NH4+].[NH4+].[O-]C(=O)C([O-])=O VBIXEXWLHSRNKB-UHFFFAOYSA-N 0.000 claims description 2
- 229910000148 ammonium phosphate Inorganic materials 0.000 claims description 2
- 150000001450 anions Chemical class 0.000 claims description 2
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 claims description 2
- 239000010410 layer Substances 0.000 description 13
- 230000015572 biosynthetic process Effects 0.000 description 9
- -1 fatty alcohol sulfonate Chemical class 0.000 description 9
- 238000000576 coating method Methods 0.000 description 7
- 239000010802 sludge Substances 0.000 description 7
- 229910019142 PO4 Inorganic materials 0.000 description 4
- 229940039748 oxalate Drugs 0.000 description 4
- 235000021317 phosphate Nutrition 0.000 description 4
- BZSXEZOLBIJVQK-UHFFFAOYSA-N 2-methylsulfonylbenzoic acid Chemical compound CS(=O)(=O)C1=CC=CC=C1C(O)=O BZSXEZOLBIJVQK-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- VEPSWGHMGZQCIN-UHFFFAOYSA-H ferric oxalate Chemical compound [Fe+3].[Fe+3].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O VEPSWGHMGZQCIN-UHFFFAOYSA-H 0.000 description 3
- 230000007062 hydrolysis Effects 0.000 description 3
- 238000006460 hydrolysis reaction Methods 0.000 description 3
- 229910000398 iron phosphate Inorganic materials 0.000 description 3
- WBJZTOZJJYAKHQ-UHFFFAOYSA-K iron(3+) phosphate Chemical compound [Fe+3].[O-]P([O-])([O-])=O WBJZTOZJJYAKHQ-UHFFFAOYSA-K 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 3
- 239000010452 phosphate Substances 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 230000003213 activating effect Effects 0.000 description 2
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000029142 excretion Effects 0.000 description 2
- 229960004887 ferric hydroxide Drugs 0.000 description 2
- IEECXTSVVFWGSE-UHFFFAOYSA-M iron(3+);oxygen(2-);hydroxide Chemical compound [OH-].[O-2].[Fe+3] IEECXTSVVFWGSE-UHFFFAOYSA-M 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
- IQUPABOKLQSFBK-UHFFFAOYSA-N 2-nitrophenol Chemical compound OC1=CC=CC=C1[N+]([O-])=O IQUPABOKLQSFBK-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 229910000640 Fe alloy Inorganic materials 0.000 description 1
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical class OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- 229920002253 Tannate Polymers 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- ZRIUUUJAJJNDSS-UHFFFAOYSA-N ammonium phosphates Chemical class [NH4+].[NH4+].[NH4+].[O-]P([O-])([O-])=O ZRIUUUJAJJNDSS-UHFFFAOYSA-N 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 150000001642 boronic acid derivatives Chemical class 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- KXZJHVJKXJLBKO-UHFFFAOYSA-N chembl1408157 Chemical compound N=1C2=CC=CC=C2C(C(=O)O)=CC=1C1=CC=C(O)C=C1 KXZJHVJKXJLBKO-UHFFFAOYSA-N 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 150000001913 cyanates Chemical class 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000004675 formic acid derivatives Chemical class 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 150000003893 lactate salts Chemical class 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 150000002826 nitrites Chemical class 0.000 description 1
- 150000003891 oxalate salts Chemical class 0.000 description 1
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical class OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- JRKICGRDRMAZLK-UHFFFAOYSA-L persulfate group Chemical group S(=O)(=O)([O-])OOS(=O)(=O)[O-] JRKICGRDRMAZLK-UHFFFAOYSA-L 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- VKJKEPKFPUWCAS-UHFFFAOYSA-M potassium chlorate Chemical compound [K+].[O-]Cl(=O)=O VKJKEPKFPUWCAS-UHFFFAOYSA-M 0.000 description 1
- 239000004323 potassium nitrate Substances 0.000 description 1
- 235000010333 potassium nitrate Nutrition 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- ARENMZZMCSLORU-UHFFFAOYSA-N propan-2-yl naphthalene-1-sulfonate Chemical compound C1=CC=C2C(S(=O)(=O)OC(C)C)=CC=CC2=C1 ARENMZZMCSLORU-UHFFFAOYSA-N 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
- ZNCPFRVNHGOPAG-UHFFFAOYSA-L sodium oxalate Chemical compound [Na+].[Na+].[O-]C(=O)C([O-])=O ZNCPFRVNHGOPAG-UHFFFAOYSA-L 0.000 description 1
- 229940039790 sodium oxalate Drugs 0.000 description 1
- 239000001488 sodium phosphate Substances 0.000 description 1
- 229910000162 sodium phosphate Inorganic materials 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical class [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 150000003892 tartrate salts Chemical class 0.000 description 1
- 150000004764 thiosulfuric acid derivatives Chemical class 0.000 description 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
- 239000002966 varnish Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- LRXTYHSAJDENHV-UHFFFAOYSA-H zinc phosphate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LRXTYHSAJDENHV-UHFFFAOYSA-H 0.000 description 1
- 229910000165 zinc phosphate Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/46—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing oxalates
- C23C22/47—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing oxalates containing also phosphates
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Treatment Of Metals (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEW608A DE916253C (de) | 1949-12-12 | 1949-12-12 | Verfahren zur Erzeugung von Oberflaechenschichten auf Eisen und Stahl |
| DEC3279A DE917159C (de) | 1949-12-12 | 1950-10-11 | Verfahren zur Erzeugung von Oberflaechenschichten auf Eisen und Stahl |
| NL157883A NL81686C (nl) | 1949-12-12 | 1950-12-11 | Werkwijze voor het aanbrengen van oppervlaktelagen op ijzer en staal alsmede volgens deze werkwijze verkregen van oppervlaktelagen voorziene ijzeren of stalen voorwerpen |
| GB30283/50A GB684204A (en) | 1949-12-12 | 1950-12-11 | Process for the production of a surface layer on iron or steel |
| NL202774A NL88522C (nl) | 1949-12-12 | 1950-12-11 | Werkwijze voor het aanbrengen van oppervlaktelagen op ijzer en staal alsmede de aldus van oppervlaktelagen voorziene ijzeren of stalen voorwerpen |
| BE500006A BE500006A (fr) | 1949-12-12 | 1950-12-12 | Procédé pour la production de couches de revêtement sur le fer et l'acier |
| FR1032645D FR1032645A (fr) | 1949-12-12 | 1950-12-12 | Procédé pour la production de couches de revêtement sur le fer et l'acier |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEW608A DE916253C (de) | 1949-12-12 | 1949-12-12 | Verfahren zur Erzeugung von Oberflaechenschichten auf Eisen und Stahl |
| DEC3279A DE917159C (de) | 1949-12-12 | 1950-10-11 | Verfahren zur Erzeugung von Oberflaechenschichten auf Eisen und Stahl |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE916253C true DE916253C (de) | 1954-08-05 |
Family
ID=92174838
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEW608A Expired DE916253C (de) | 1949-12-12 | 1949-12-12 | Verfahren zur Erzeugung von Oberflaechenschichten auf Eisen und Stahl |
| DEC3279A Expired DE917159C (de) | 1949-12-12 | 1950-10-11 | Verfahren zur Erzeugung von Oberflaechenschichten auf Eisen und Stahl |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEC3279A Expired DE917159C (de) | 1949-12-12 | 1950-10-11 | Verfahren zur Erzeugung von Oberflaechenschichten auf Eisen und Stahl |
Country Status (5)
| Country | Link |
|---|---|
| BE (1) | BE500006A (en, 2012) |
| DE (2) | DE916253C (en, 2012) |
| FR (1) | FR1032645A (en, 2012) |
| GB (1) | GB684204A (en, 2012) |
| NL (2) | NL88522C (en, 2012) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1098784B (de) * | 1955-04-08 | 1961-02-02 | Metallgesellschaft Ag | Verfahren zur Herstellung von Oxalatschichten auf Eisen und Stahl |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2832706A (en) * | 1953-05-12 | 1958-04-29 | Victor Chemical Works | Metal cleaning and phosphating composition and method of cleaning and phosphating |
| US2930723A (en) * | 1954-12-07 | 1960-03-29 | Walterisation Company Ltd | Surface treatment of metals |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1895569A (en) * | 1932-02-09 | 1933-01-31 | Western Union Telegraph Co | Production of protective coatings on iron and steel articles |
| US2077450A (en) * | 1935-01-08 | 1937-04-20 | Alrose Chemical Company | Method and composition for coating iron and steel articles |
| US2236549A (en) * | 1937-06-11 | 1941-04-01 | Parker Rust Proof Co | Method of coloring metals and product |
| DE734859C (de) * | 1940-04-11 | 1943-04-29 | Dr Herbert Luckmann | Verfahren zur Erzeugung von Schichten auf Eisen und Eisenlegierungen |
-
1949
- 1949-12-12 DE DEW608A patent/DE916253C/de not_active Expired
-
1950
- 1950-10-11 DE DEC3279A patent/DE917159C/de not_active Expired
- 1950-12-11 GB GB30283/50A patent/GB684204A/en not_active Expired
- 1950-12-11 NL NL202774A patent/NL88522C/nl active
- 1950-12-11 NL NL157883A patent/NL81686C/nl active
- 1950-12-12 FR FR1032645D patent/FR1032645A/fr not_active Expired
- 1950-12-12 BE BE500006A patent/BE500006A/fr unknown
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1895569A (en) * | 1932-02-09 | 1933-01-31 | Western Union Telegraph Co | Production of protective coatings on iron and steel articles |
| DE642191C (de) * | 1932-02-09 | 1937-02-27 | Curtin Howe Corp | Verfahren zum UEberziehen von Eisen- und Stahlgegenstaenden mit einer Schutzschicht |
| US2077450A (en) * | 1935-01-08 | 1937-04-20 | Alrose Chemical Company | Method and composition for coating iron and steel articles |
| US2236549A (en) * | 1937-06-11 | 1941-04-01 | Parker Rust Proof Co | Method of coloring metals and product |
| DE734859C (de) * | 1940-04-11 | 1943-04-29 | Dr Herbert Luckmann | Verfahren zur Erzeugung von Schichten auf Eisen und Eisenlegierungen |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1098784B (de) * | 1955-04-08 | 1961-02-02 | Metallgesellschaft Ag | Verfahren zur Herstellung von Oxalatschichten auf Eisen und Stahl |
Also Published As
| Publication number | Publication date |
|---|---|
| FR1032645A (fr) | 1953-07-03 |
| NL81686C (nl) | 1956-05-17 |
| NL202774A (en, 2012) | 1958-01-15 |
| DE917159C (de) | 1954-08-26 |
| NL88522C (nl) | 1958-05-17 |
| GB684204A (en) | 1952-12-10 |
| BE500006A (fr) | 1950-12-30 |
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