DE69921347T2 - Nickel katalysator - Google Patents
Nickel katalysator Download PDFInfo
- Publication number
- DE69921347T2 DE69921347T2 DE69921347T DE69921347T DE69921347T2 DE 69921347 T2 DE69921347 T2 DE 69921347T2 DE 69921347 T DE69921347 T DE 69921347T DE 69921347 T DE69921347 T DE 69921347T DE 69921347 T2 DE69921347 T2 DE 69921347T2
- Authority
- DE
- Germany
- Prior art keywords
- nickel
- catalyst
- alumina
- silica
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims abstract description 134
- 239000003054 catalyst Substances 0.000 claims abstract description 63
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 53
- 239000011148 porous material Substances 0.000 claims abstract description 33
- 229910052751 metal Inorganic materials 0.000 claims abstract description 5
- 239000002184 metal Substances 0.000 claims abstract description 5
- 229910052752 metalloid Inorganic materials 0.000 claims abstract description 4
- 150000002738 metalloids Chemical class 0.000 claims abstract description 4
- 150000002739 metals Chemical class 0.000 claims abstract description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 16
- 238000005984 hydrogenation reaction Methods 0.000 claims description 14
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 13
- 239000000377 silicon dioxide Substances 0.000 claims description 7
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 4
- 235000019353 potassium silicate Nutrition 0.000 claims description 4
- 239000004927 clay Substances 0.000 claims description 3
- -1 metasilicate Substances 0.000 claims description 3
- 230000002378 acidificating effect Effects 0.000 claims description 2
- CETPSERCERDGAM-UHFFFAOYSA-N ceric oxide Chemical compound O=[Ce]=O CETPSERCERDGAM-UHFFFAOYSA-N 0.000 claims description 2
- 229910000422 cerium(IV) oxide Inorganic materials 0.000 claims description 2
- 239000008119 colloidal silica Substances 0.000 claims description 2
- 239000000395 magnesium oxide Substances 0.000 claims description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 2
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims description 2
- 239000004408 titanium dioxide Substances 0.000 claims description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 1
- 235000012239 silicon dioxide Nutrition 0.000 claims 1
- 239000000243 solution Substances 0.000 description 21
- 239000000463 material Substances 0.000 description 16
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 239000002243 precursor Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000007868 Raney catalyst Substances 0.000 description 5
- 229910000564 Raney nickel Inorganic materials 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 239000002002 slurry Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 4
- 229910004298 SiO 2 Inorganic materials 0.000 description 4
- 238000006477 desulfuration reaction Methods 0.000 description 4
- 230000023556 desulfurization Effects 0.000 description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 description 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- 230000032683 aging Effects 0.000 description 3
- 238000001354 calcination Methods 0.000 description 3
- 150000002196 fatty nitriles Chemical class 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 229910052717 sulfur Inorganic materials 0.000 description 3
- 239000011593 sulfur Substances 0.000 description 3
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
- 239000004115 Sodium Silicate Substances 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 229910052681 coesite Inorganic materials 0.000 description 2
- 229910052906 cristobalite Inorganic materials 0.000 description 2
- 239000003925 fat Substances 0.000 description 2
- 239000012065 filter cake Substances 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 229910000008 nickel(II) carbonate Inorganic materials 0.000 description 2
- ZULUUIKRFGGGTL-UHFFFAOYSA-L nickel(ii) carbonate Chemical compound [Ni+2].[O-]C([O-])=O ZULUUIKRFGGGTL-UHFFFAOYSA-L 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052911 sodium silicate Inorganic materials 0.000 description 2
- 229910052682 stishovite Inorganic materials 0.000 description 2
- 229910052905 tridymite Inorganic materials 0.000 description 2
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000011149 active material Substances 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229940053200 antiepileptics fatty acid derivative Drugs 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 210000001035 gastrointestinal tract Anatomy 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 150000002815 nickel Chemical class 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 238000004375 physisorption Methods 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 150000003141 primary amines Chemical class 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000012916 structural analysis Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B01J23/755—Nickel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
- B01J35/391—Physical properties of the active metal ingredient
- B01J35/392—Metal surface area
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/61—Surface area
- B01J35/613—10-100 m2/g
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/64—Pore diameter
- B01J35/647—2-50 nm
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/64—Pore diameter
- B01J35/651—50-500 nm
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP98202878 | 1998-08-28 | ||
| EP98202878A EP0985448A1 (en) | 1998-08-28 | 1998-08-28 | Nickel catalyst |
| PCT/NL1999/000534 WO2000012210A1 (en) | 1998-08-28 | 1999-08-27 | Nickel catalyst |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69921347D1 DE69921347D1 (de) | 2004-11-25 |
| DE69921347T2 true DE69921347T2 (de) | 2005-11-03 |
Family
ID=8234069
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69921347T Expired - Lifetime DE69921347T2 (de) | 1998-08-28 | 1999-08-27 | Nickel katalysator |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6524994B1 (https=) |
| EP (2) | EP0985448A1 (https=) |
| JP (1) | JP4473450B2 (https=) |
| AT (1) | ATE279980T1 (https=) |
| AU (1) | AU5534799A (https=) |
| DE (1) | DE69921347T2 (https=) |
| DK (1) | DK1117481T3 (https=) |
| ES (1) | ES2232164T3 (https=) |
| WO (1) | WO2000012210A1 (https=) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102007009556A1 (de) * | 2007-02-27 | 2008-10-23 | Mtu Cfc Solutions Gmbh | Reformierungskatalysator für Schmelzcarbonatbrennstoffzellen |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001513697A (ja) * | 1997-02-24 | 2001-09-04 | スーペリア マイクロパウダーズ リミテッド ライアビリティ カンパニー | エアロゾル法及び装置、粒子製品、並びに該粒子製品から製造される電子装置 |
| DE10124600A1 (de) * | 2001-05-21 | 2002-11-28 | Basf Ag | Ni/Ti02-Hydrierkatalysator |
| US7468342B2 (en) * | 2001-05-22 | 2008-12-23 | Mitsubishi Gas Chemical Company, Inc. | Catalysts and process for producing aromatic amines |
| US6914033B2 (en) * | 2002-08-13 | 2005-07-05 | Conocophillips Company | Desulfurization and novel compositions for same |
| US20040063576A1 (en) * | 2002-09-30 | 2004-04-01 | Sud-Chemie Inc. | Catalyst adsorbent for removal of sulfur compounds for fuel cells |
| WO2004035194A2 (en) * | 2002-10-16 | 2004-04-29 | Conocophillips Company | High hydrothermal stability catalyst support |
| US20050032640A1 (en) * | 2003-08-07 | 2005-02-10 | He Huang | Method and structure for desulfurizing gasoline or diesel fuel for use in a fuel cell power plant |
| US12203035B2 (en) | 2005-07-05 | 2025-01-21 | Neste Oyj | Process for the manufacture of diesel range hydrocarbons |
| US8022258B2 (en) | 2005-07-05 | 2011-09-20 | Neste Oil Oyj | Process for the manufacture of diesel range hydrocarbons |
| JP5063988B2 (ja) | 2006-01-27 | 2012-10-31 | 花王株式会社 | 脂肪酸エステルの製造方法 |
| US7563742B2 (en) | 2006-09-22 | 2009-07-21 | Headwaters Technology Innovation, Llc | Supported nickel catalysts having high nickel loading and high metal dispersion and methods of making same |
| US8119847B2 (en) * | 2007-06-15 | 2012-02-21 | E. I. Du Pont De Nemours And Company | Catalytic process for converting renewable resources into paraffins for use as diesel blending stocks |
| US20090326285A1 (en) * | 2008-06-30 | 2009-12-31 | Bauer Lorenz J | Use of Supported Mixed Metal Sulfides for Hydrotreating Biorenewable Feeds |
| JP5654018B2 (ja) | 2009-08-24 | 2015-01-14 | インヴィスタ テクノロジーズ エスアエルエル | 改善されたポリエーテルグリコールの製造法 |
| JP2013514258A (ja) * | 2009-12-18 | 2013-04-25 | インビスタ テクノロジーズ エス エイ アール エル | 塩基性炭酸ニッケルから生じさせたニッケル金属組成物およびニッケル錯体 |
| EP2614070B1 (en) * | 2010-09-07 | 2017-07-26 | Invista Technologies S.à r.l. | Nickel compositions for preparing nickel metal and nickel complexes |
| EP2718013A2 (en) | 2011-06-10 | 2014-04-16 | Invista Technologies S.à.r.l. | Nickel calcination and reduction process including a fluidizing bed reactor |
| CN103732323B (zh) * | 2011-06-10 | 2016-09-14 | 因温斯特技术公司 | 用于催化镍-配体配合物的制备的镍形式 |
| JP6624634B2 (ja) | 2014-11-20 | 2019-12-25 | 花王株式会社 | 脂肪酸エステルの製造方法 |
| EP3903926A1 (en) * | 2020-04-30 | 2021-11-03 | Basf Se | Catalytic material comprising ni supported on an oxidic support comprising zr and si |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4010025A (en) * | 1975-04-07 | 1977-03-01 | Plessey Incorporated | Oxidation and sinter-resistant metal powders and pastes |
| US3933883A (en) * | 1975-04-14 | 1976-01-20 | W. R. Grace & Co. | Methanation catalyst and process of use |
| US4588709A (en) * | 1983-12-19 | 1986-05-13 | Intevep, S.A. | Catalyst for removing sulfur and metal contaminants from heavy crudes and residues |
| NL190750C (nl) * | 1984-06-21 | 1994-08-01 | Unilever Nv | Nikkelaluminaat katalysator, de bereiding daarvan en het hydrogeneren van onverzadigde organische verbindingen daarmee. |
| US4990243A (en) * | 1989-05-10 | 1991-02-05 | Chevron Research And Technology Company | Process for hydrodenitrogenating hydrocarbon oils |
| US5389595A (en) * | 1993-09-30 | 1995-02-14 | Union Oil Company Of California | Hydroprocessing catalyst, its use, and method of preparation |
| US5403806A (en) * | 1993-10-22 | 1995-04-04 | Union Oil Company Of California | Phosphorous-containing hydroprocessing catalyst and method of preparation |
| JP3774474B2 (ja) * | 1994-08-26 | 2006-05-17 | エンゲルハード デ メールン ビー．ブイ． | シクロヘキサンの製造方法 |
-
1998
- 1998-08-28 EP EP98202878A patent/EP0985448A1/en not_active Withdrawn
-
1999
- 1999-08-27 AU AU55347/99A patent/AU5534799A/en not_active Abandoned
- 1999-08-27 JP JP2000567301A patent/JP4473450B2/ja not_active Expired - Fee Related
- 1999-08-27 EP EP99941872A patent/EP1117481B1/en not_active Expired - Lifetime
- 1999-08-27 WO PCT/NL1999/000534 patent/WO2000012210A1/en not_active Ceased
- 1999-08-27 DK DK99941872T patent/DK1117481T3/da active
- 1999-08-27 ES ES99941872T patent/ES2232164T3/es not_active Expired - Lifetime
- 1999-08-27 US US09/763,846 patent/US6524994B1/en not_active Expired - Lifetime
- 1999-08-27 AT AT99941872T patent/ATE279980T1/de not_active IP Right Cessation
- 1999-08-27 DE DE69921347T patent/DE69921347T2/de not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102007009556A1 (de) * | 2007-02-27 | 2008-10-23 | Mtu Cfc Solutions Gmbh | Reformierungskatalysator für Schmelzcarbonatbrennstoffzellen |
Also Published As
| Publication number | Publication date |
|---|---|
| US6524994B1 (en) | 2003-02-25 |
| EP0985448A1 (en) | 2000-03-15 |
| AU5534799A (en) | 2000-03-21 |
| ATE279980T1 (de) | 2004-11-15 |
| JP4473450B2 (ja) | 2010-06-02 |
| EP1117481A1 (en) | 2001-07-25 |
| ES2232164T3 (es) | 2005-05-16 |
| DE69921347D1 (de) | 2004-11-25 |
| WO2000012210A1 (en) | 2000-03-09 |
| EP1117481B1 (en) | 2004-10-20 |
| JP2002523230A (ja) | 2002-07-30 |
| DK1117481T3 (da) | 2004-12-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition |