DE69226509T2 - Verwendung von einer Schmierfettzusammensetzung für homokinetische Kupplung - Google Patents

Verwendung von einer Schmierfettzusammensetzung für homokinetische Kupplung

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Publication number
DE69226509T2
DE69226509T2 DE69226509T DE69226509T DE69226509T2 DE 69226509 T2 DE69226509 T2 DE 69226509T2 DE 69226509 T DE69226509 T DE 69226509T DE 69226509 T DE69226509 T DE 69226509T DE 69226509 T2 DE69226509 T2 DE 69226509T2
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Germany
Prior art keywords
group
compounds
thickener
soap
grease composition
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Revoked
Application number
DE69226509T
Other languages
English (en)
Other versions
DE69226509D1 (de
Inventor
Hirotugu Yokohama-Shi Kanagawa-Ken Kinoshita
Masaru Kawasaki-Shi Kanagawa-Ken Mishima
Souichi Tokyo Nomura
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Eneos Corp
Original Assignee
Nippon Oil Corp
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Filing date
Publication date
Family has litigation
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Application filed by Nippon Oil Corp filed Critical Nippon Oil Corp
Application granted granted Critical
Publication of DE69226509D1 publication Critical patent/DE69226509D1/de
Publication of DE69226509T2 publication Critical patent/DE69226509T2/de
Anticipated expiration legal-status Critical
Revoked legal-status Critical Current

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    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/06—Mixtures of thickeners and additives
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Description

  • Die vorliegende Erfindung betrifft die Verwendung einer Schmierfettzusammensetzung für eine homokinetische Kupplung oder einer Kupplung vom festen Typ und einer Kupplung vom Gleittyp.
  • Im allgemeinen wird eine Kombination aus einer Kupplung vom festen Typ, einer Welle und einer Kupplung vom Schubtyp verwendet, wenn eine homokinetische Kupplung bei Autos vom FF-Typ oder vom Typ des Vorderradantriebes verwendet wird.
  • Bezüglich der Kupplung vom festen Typ gibt es eine Birfield-Kupplung, eine Rzeppa-Kupplung, eine freiarbeitende Freikupplung und eine Dreibein-Kupplung. Bezüglich der Kupplung vom Gleittyp gibt es eine Winkel-Kupplung, eine Dreibein-Kupplung und eine Querrillen-Kupplung.
  • Als ein in die homokinetischen Kupplungen gefülltes Schmiermittel wird hauptsächlich ein Hochdruck-Schmierfett verwendet, in welchem ein Basisschmierfett, das aus gereinigtem Mineralöl, einer Lithiumseife und einem Urea-Verdickungsmittel (Urea = Harnstoff), welches mit Molybdändisulfid, einer Schwefel - Phosphor-Verbindung, einer Bleiverbindung, etc. kombiniert ist, besteht.
  • Bei der Schmierfettzusammensetzung für die homokinetische Kupplung gibt es erforderliche Eigenschaften, wie etwa Anti-Flocken, Anti-Blockieren, Verschleißfestigkeit oder niedrige Reibungseigenschaften. Jedoch gibt es Tendenzen zu einem Hochleistungs- und Qualitätsauto, so daß die herkömmlichen Schmierfettzusammensetzungen es im allgemeinen an diesen Fähigkeiten fehlen lassen. Insbesondere ist es im Hinblick auf eine verlängerte Lebensdauer der homokinetischen Kupplung erwünscht gewesen, ihre jeweilige Leistung zu verbessern.
  • EP-A-0 456 565 offenbart eine Schmiermittelzusammensetzung für Warmwalzstahl, die ein Basisöl, ein Verdickungsmittel und Bornitrid umfaßt.
  • Es ist eine Aufgabe der vorliegenden Erfindung, eine Schmiermittelzusammensetzung für eine homokinetische Kupplung bereitzustellen, welche überragend im Hinblick auf die Lebensdauer der homokinetischen Kupplung ist.
  • Die obige und andere Aufgaben der vorliegenden Erfindung werden aus der folgenden Beschreibung offensichtlich.
  • Entsprechend der vorliegenden Erfindung wird eine Schmiermittelzusammensetzung, welche ein Basisöl umfaßt, das ein Verdickungsmittel und Bornitridpulver beinhaltet, für eine homokinetische Kupplung verwendet.
  • Die vorliegende Erfindung wird nachfolgend detaillierter beschrieben.
  • Jedes Öl, wie etwa ein Erdöl-Basisschmieröl und ein synthetisches Basisschmieröl, welches üblicherweise als das Basisschmieröl verwendet wird, kann als Basisöl gemäß der vorliegenden Erfindung verwendet werden. Vorzugsweise kann Erdöl- Basisschmieröl verwendet werden.
  • Beispiele für die Erdöl-Basisschmieröle beinhalten Basisöle, wie etwa Paraffin- Basisschmieröl, Naphthen-Basisschmieröl und dergleichen, welche durch Unterwerfen, der durch Destillation unter atmosphärischem oder reduziertem Druck erhaltenen Schmiermittelfunktionen, einer Raffinination, wie etwa Lösungsmittel -Entasphaltierung, Lösungsmittel-Extraktion, Hydrokracken, Lösungsmittel- Entparaffinieren, Kontakt-Entparaffmieren, Hydrofinieren, Waschen mit schwefeliger Säure, Ton-Behandlung und dergleichen, erhalten werden.
  • Beispiele für synthetische Basisschmieröle beinhalten Poly-α-Olefm, wie etwa Polybuten, 1-Octen-Oligomere und 1-Decen-Oligomere, Alkylbenzol; Alkylnaphtha len; Diester, wie etwa Ditridecyl-Glutarat, Di-2-ethylhexyl-Adipat, Diisodecyl- Adipat, Ditridecyl-Adipat und Di-3-ethylhexyl-sebacat; Polyolester, wie etwa Trimethylolpropan-caprylat, Trimethylolpropan-pelargonat, Pentaerythritol-2-ethylhexanoat und Pentaerythritol-pelargonat; Polyoxyalkylen-glycol; Polyphenyl-ether; Siliconöl oder Perfluoralkyl-ether können verwendet werden. Zwei oder mehrere der oben erwähnten Öle können ebenso als ein Gemisch verwendet werden. Jeder allgemein übliche Viskositätsbereich kann verwendet werden. Insbesondere kann er 2 bis 40 cSt bei 100ºC betragen. Der Gehalt an dem Basisöl kann vorzugsweise 50 bis 97.5 Gew.-% basierend auf dem Gesamtgewicht der Zusammensetzung betragen.
  • Jedes Verdickungsmittel kann in dem Basisöl verwendet werden. Zum Beispiel kann ein Verdickungsmittel auf Seifenbasis, wie etwa eine Metallseife und eine komplexe Metallseife; ein Verdickungsmittel auf Nichtseifenbasis, wie etwa Bentonit, Silicagel, Urea-Verbindungen, Urea-Urethan-Verbindungen und Urethan -Verbindungen verwendet werden. Insbesondere können Urea-Verbindungen, Urea-Urethan-Verbindungen, Urethan-Verbindungen und Gemische derjenigen, welche bessere Wärmebeständigkeit haben, verwendet werden.
  • Beispiele der für die Metallseife und die komplexe Metallseife beinhalten eine Natriumseife, eine Calciumseife, eine Aluminiumseife, eine Lithiumseife und dergleichen. Beispiele der Urea-Verbindungen, der Urea-Urethan-Verbindungen und der Urethan-Verbindungen beinhalten Diurea-Verbindungen, Triurea-Verbindungen, Tetraurea-Verbindungen, Polyurea-Verbindungen, Urea-Urethan- Verbindungen, Diurethan-Verbindungen und Gemische davon. Es wird bevorzugt, daß Diurea-Verbindungen, Urea-Urethan-Verbindungen, Diurethan- Verbindungen und Gemische davon verwendet werden. Vorzugsweise kann eine Verbindung oder Gemische verwendet werden, die durch Vermischen zweier oder mehrerer Verbindungen erhalten werden, welche durch die Formel (1) dargestellt sind:
  • worin R für eine zweiwertige Kohlenwasserstoff-Gruppe steht, und A und B gleiche oder verschieden voneinander sein können und jedes für R¹-NH-,
  • oder R&sup4;-O-, worin R¹, R², R&sup5; und R&sup4; gleich oder verschieden sein können und jedes für einen Kohlenwasserstoffrest, der 6 bis 20 Kohlenstoffatome hat, steht.
  • Das oben erwähnte R in der Formel (1) kann vorzugsweise eine zweiwertige Kohlenwasserstoffgruppe mit 6 bis 20 Kohlenstoffatome sein, bevorzugt mit 6 bis 15 Kohlenstoffatomen. Als zweiwertige Kohlenwasserstoffgruppe kann vorzugsweise eine gradkettige oder eine verzweigte Alken-Gruppe oder Alkenylen-Gruppe, eine Cycloalken-Gruppe oder eine aromatische Gruppe verwendet werden. Zum Beispiel kann sie -(CH&sub2;)- und durch die folgenden Formeln dargestellte Gruppen und dergleichen beinhalten:
  • (and = und)
  • Für die oben erwähnten R¹, R², R³ und R&sup4; kann vorzugsweise eine gerade Kette oder verzweigte Alkyl-Gruppe oder Alkenyl-Gruppe, eine Cycloalkyl-Gruppe und eine aromatische Gruppe verwendet werden. Zum Beispiel kann sie eine Hexyl -Gruppe, Heptyl-Gruppe, Octyl-Gruppe, Nonyl-Gruppe, Decyl-Gruppe, Undecyl-Gruppe, Dodecyl-Gruppe, Tridecyl-Gruppe, Tetradecyl-Gruppe, Pentadecyl-Gruppe, Hexadecyl-Gruppe, Heptadecyl-Gruppe, Octadecyl-Gruppe, Nonadecyl-Gruppe, Eicocyl-Gruppe, Hexenyl-Gruppe, Heptenyl-Gruppe, Octenyl -Gruppe, Nonenyl-Gruppe, Decenyl-Gruppe, Undecenyl-Gruppe, Dodecenyl- Gruppe, Tridecenyl-Gruppe, Tetradecenyl-Gruppe, Pentadecenyl-Gruppe, Hexadecenyl-Gruppe, Heptadecenyl-Gruppe, Octadecenyl-Gruppe, Nonadecenyl- Gruppe, Eicocenyl-Gruppe, Cyclohexyl-Gruppe, Methylcyclohexyl-Gruppe, Dimethylcyclohexyl-Gruppe, Ethylcyclohexyl-Gruppe, Diethylcyclohexyl-Gruppe, Propylcyclohexyl-Gruppe, Isopropylcyclohexyl-Gruppe, 1-Methyl-3-propylcyclohexyl-Gruppe, Butylcyclohexyl-Gruppe, Amylcyclohexyl-Gruppe, Amylmethylcyclohexyl-Gruppe, Hexylcyclohexyl-Gruppe, Heptylcyclohexyl-Gruppe, Octylcyclohexyl-Gruppe, Nonylcyclohexyl-Gruppe, Decylcyclohexyl-Gruppe, Undecylcyclohexyl-Gruppe, Dodecylcyclohexyl-Gruppe, Tridecylcyclohexyl- Gruppe, Tetradecylcyclohexyl-Gruppe, Phenyl-Gruppe, Toluyl-Gruppe, Benzyl -Gruppe, Ethylphenyl-Gruppe, Methylbenzyl-Gruppe, Xylyl-Gruppe, Propylphenyl-Gruppe, Cumenyl-Gruppe, Etheylbenzyl-Gruppe, Naphthyl-Gruppe, Methylnaphthyl-Gruppe, Ethylnaphthyl-Gruppe, Dimethylnaphthyl-Gruppe und Propylnaphthyl-Gruppe beinhalten.
  • Die in der Formel (1) dargestellte Verbindung kann die folgenden Verbindungen beinhalten:
  • Detaillierter können z. B. die Verbindungen verwendet werden, welche in der japanischen Patentveröffentlichung Nr. 55-11156, der offengelegten japanischen Patentanmeldung Nr. 62-250097 und der offengelegten japanischen Patentanmeldung Nr. 64-9296 beschrieben werden.
  • Um die Diurea-Verbindung, die Urea-Urethan-Verbindung oder die Diurethan -Verbindung herzustellen, kann z. B. Diisocyanat, das durch OCN-R-NCO dargestellt ist, mit einer Verbindung, die durch
  • R¹-NH&sub2;,
  • oder R&sup4;-OH oder Gemische
  • derjenigen dargestellt ist, in dem Basisöl bei der Temperatur von 10 bis 200ºC reagieren gelassen werden. R, R¹, R², R&sup5; und R&sup4; können die gleichen wie in der Formel (1) sein.
  • Der Gehalt des Verdickungsmittels kann vorzugsweise 2 bis 25 Gew.-%, besonders bevorzugt 3 bis 20 Gew.-% betragen, berechnet auf dem Gesamtgewicht der Zusammensetzung. Wenn der Gehalt weniger als 2 Gew.-% ist, so kann der Anteil des Verdickungsmittels so gering sein, daß der ausreichende Schmierzustand nicht erhalten werden kann. Wenn der Gehalt mehr als 25 Gew.-% beträgt, so kann das Schmierfett so hart werden, daß die zufriedenstellende Schmierung nicht erhalten werden kann.
  • Eine Partikelgröße des in dem Basisöl enthaltenen Bornitridpulvers muß nicht beschränkt werden. Die durchschnittliche Partikelgröße kann vorzugsweise in dem Bereich von 0.05 bis 5 um, noch bevorzugter von 0.4 bis 2 um sein.
  • Ein Gehalt des Bornitridpulvers kann vorzugsweise in dem Bereich von 0.5 bis 20 Gew.-%, noch bevorzugter von 1 bis 10 Gew.-%, berechnet auf dem Gesamtgewicht der Zusammensetzung sein. Wenn der Gehalt weniger als 0.5 Gew.-% beträgt, so kann die Anti-Flockenleistung schlechter werden, und wenn der Gehalt mehr als 20 Gew.-% beträgt, so kann die Schmierfettzusammensetzung so hart werden, daß die zufriedenstellende Schmierung nicht erhalten werden kann.
  • Zu der Schmierfettzusammensetzung für eine homokinetische Kupplung, die entsprechend der vorliegenden Erfindung verwendet wird, können weiterhin feste Schmierstoffe, Hochdruckmittel, Anti-Oxidationsmittel, ölige Mittel, Rostvermeider, Viskositätsindex-Verbesserer und Gemische derjenigen hinzugefügt werden, um die Leistung der Zusammensetzung zu verbessern, solange ihre Eigenschaften nicht zerstört werden.
  • Das Festschmiermittel kann z. B. Ruß, fluorierten Kohlenstoff, Polytetrafluorethylen, Molybdändisulfid, Antimonsulfid und Alkali- oder Erdalkaliborate beinhalten.
  • Das Hochdruckmittel kann z. B. eine Schwefelverbindung, wie etwa Monosulfid, Disulfid, Sulfoxid und Sulfinat; eine Phosphorverbindung, wie etwa Phosphat, Phosphit, Phosphinat, Phosphonat und deren Amin-Salze; eine Chlorverbindung, wie etwa Chlorparaffin, chlorierte Ester und Molybdän-Verbindungen, wie etwa Molybdän-Dithiophosphat und Molybdän-Dithiocarbamat, beinhalten.
  • Das Anti-Oxidationsmittel kann z. B. eine Phenol-Verbindung, wie etwa 2,6-di- t-buthylphenol und 2,5-di-t-buthyl-p-cresol; eine Aminverbindung, wie etwa Dialkyldiphenylamin, Phenyl-α-naphthylamin und p-Alkylphenyl-α-naphthylamin; eine Schwefelverbindung; und eine Phenothiazin-Verbindung beinhalten.
  • Das ölige Mittel kann z. B. ein Amin, wie etwa Lauryl-Amin, Myristol-Amin, Palmityl-Amin, Stearyl-Amin und Oleyl-Amin; einen höheren Alkohol, wie etwa Lauryl-Alkohol, Myristol-Alkohol, Palmityl-Alkohol, Stearyl-Alkohol und Oleyl-Alkohol; eine höhere Fettsäure, wie etwa Laurinsäure, Myristinsäure, Palmitinsäure, Stearinsäure und Oleylinsäure; ein Fettsäureester, wie etwa Methyllaurat, Methylmyristat, Methylpalmitat, Methylstearat und Methyloleat, ein Amido, wie etwa Laurylamido, Myristylamido, Palmitylamido, Stearylamido und Oleylamido; und Fette und Öle beinhalten.
  • Der Rostunterdrücker kann ein synthetisches Sulfonat, wie etwa Metallseife, Erdöl -Sulfonat, Alkylbenzol-Sulfonat und Dinonylnaphthalen-Sulfonat; ein Teilester von Polyalkoholen, wie etwa Sorbitan-Fettsäure-Ester; Amine; Phosphorsäure; und Phosphat beinhalten.
  • Der Viskositätsindexverbesserer kann z. B. Polymethacrylat, Polyisobutylen und Polystearin beinhalten.
  • Um die Schmierfettzusammensetzung für eine homokinetische Kupplung, die entsprechend der vorliegenden Erfindung verwendet wird, herzustellen, kann das Verdickungsmittel und das Bornitridpulver und wahlweise die anderen Zusätze zu dem Basisöl hinzugefügt werden, das Gemisch durchgerührt werden und dann das resultierende Gemisch durch ein Walzstuhl und dergleichen hindurchgeführt werden, um die Schmierfettzusammensetzung zu erhalten. Weiterhin können die Bestandteile des Verdickungsmittels die eingespeist werden bereits, einleitend zugegeben, aufgelöst und verrührt werden, so daß das Verdickungsmittel hergestellt werden kann, um in ähnlicher Weise die Schmiermittelzusammensetzung zu erhalten.
  • Die Schmierfettzusammensetzung für eine homokinetische Kupplung, die entsprechend der vorliegenden Erfindung verwendet wird, enthält mindestens sowohl das Verdickungsmittel als auch das Bornitridpulver, so daß es eine verbesserte Standzeit der homokinetischen Kupplung mit sich bringt.
    • BEISPIELE
  • Die vorliegende Erfindung wird detaillierter mit Bezug auf ein Beispiel und ein Vergleichsbeispiel beschrieben werden.
    • Beispiel 1
  • Zu 97 Gewichtsanteilen von kommerziell erhältlichem Lithiumseifen-Schmierfett A (60 mal bearbeitete Konsistenz: 278), welches 11 Gew.-% eines Verdickungsmittels enthält, wurden 3.0 Gewichtsanteile an Bornitridpulver, welches eine durchschnittliche Partikelgröße von 0.7 um hat, hinzugefügt. Das Gemisch wurde dann durch ein Drei-Walzen-Walzenstuhl hindurchgeführt, um eine Schmierfettzusammensetzung herzustellen.
  • Der folgende Test bezüglich der Standzeit wurde an dem hergestellten Schmierfett durchgeführt. Das Ergebnis wird in Tabelle 1 gezeigt.
    • (Test zum Auswerten der Standzeit) Haltbarkeitstest auf der Werkbank
  • Unter Verwendung einer Kupplung vom kommerziell erhältlichen Perfield-Typ mit der Größe #87 bei einer vorbestimmten Hochgeschwindigkeit und einem hohen Drehmoment wurde die Standzeit der Kupplung ausgewertet.
    • Vergleichsbeispiel 1
  • Mit dem in Beispiel 1 verwendeten kommerziell erhältliche Litiumseifen- Schmierfett A wurde derselbe Test entsprechend dem Beispiel 1 durchgeführt. Das Ergebnis wird in Tabelle 1 gezeigt.
    • Tabelle 1 Durchschnittliche Standzeit (Stunden) Beispiel 1 120 Vergleichsbeispiel 1 42
  • Im Licht der Tabelle 1 ist die Schmierfettzusammensetzung der vorliegenden Erfindung für eine homokinetische Kupplung hinsichtlich der Standzeit der homokinetischen Kupplungen, im Vergleich zu der Zusammensetzung des Vergleichsbeispieles 1, überlegen.

Claims (3)

1. Verwendung von einer Schmierfettzusammensetzung, die ein Basisöl umfaßt, welches ein Verdickungsmittel und Bornitrid-Pulver für eine homokinetische Kupplung enthält.
2. Verwendung nach Anspruch 1, worin das Verdickungsmittel aus Natriumseife, Kalziumseife, Aluminiumseife, Lithiumseife und Gemischen davon ausgewählt wird.
3. Verwendung nach Anspruch 1, worin das Verdickungsmittel aus Bentonit, Sillkagel, Diureaverbindungen, Triureaverbindungen, Tetraureaverbindungen, Polyreaverbindungen, Urea-Urethan-Verbindungen, Diurethanverbindungen und Gemische davon ausgewählt wird.
DE69226509T 1991-03-07 1992-03-06 Verwendung von einer Schmierfettzusammensetzung für homokinetische Kupplung Revoked DE69226509T2 (de)

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DE69223833D1 (de) 1998-02-12
JPH04279698A (ja) 1992-10-05
EP0558099B1 (de) 1998-08-05
JP2799634B2 (ja) 1998-09-21
US5512188A (en) 1996-04-30
EP0508115A1 (de) 1992-10-14
DE69223833T2 (de) 1998-08-27
DE69226509D1 (de) 1998-09-10
EP0558099A1 (de) 1993-09-01

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