DE69111355D1 - Verfahren zur Herstellung von granulierter Zitronensäure und ihrer Salze. - Google Patents

Verfahren zur Herstellung von granulierter Zitronensäure und ihrer Salze.

Info

Publication number
DE69111355D1
DE69111355D1 DE69111355T DE69111355T DE69111355D1 DE 69111355 D1 DE69111355 D1 DE 69111355D1 DE 69111355 T DE69111355 T DE 69111355T DE 69111355 T DE69111355 T DE 69111355T DE 69111355 D1 DE69111355 D1 DE 69111355D1
Authority
DE
Germany
Prior art keywords
citric acid
salts
preparation
salt
granulated citric
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69111355T
Other languages
English (en)
Other versions
DE69111355T2 (de
Inventor
Helmut A Mothes
Bhalchandra H Patwardhan
Theo G Schroeder
David J Solow
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tate and Lyle Citric Acid Inc
Original Assignee
Haarmann and Reimer Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US07/594,548 external-priority patent/US5045459A/en
Application filed by Haarmann and Reimer Corp filed Critical Haarmann and Reimer Corp
Application granted granted Critical
Publication of DE69111355D1 publication Critical patent/DE69111355D1/de
Publication of DE69111355T2 publication Critical patent/DE69111355T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/40—Preparation of oxygen-containing organic compounds containing a carboxyl group including Peroxycarboxylic acids
    • C12P7/44—Polycarboxylic acids
    • C12P7/48—Tricarboxylic acids, e.g. citric acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00—Chemistry: molecular biology and microbiology
    • Y10S435/80—Elimination or reduction of contamination by undersired ferments, e.g. aseptic cultivation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00—Chemistry: molecular biology and microbiology
    • Y10S435/8215—Microorganisms
    • Y10S435/911—Microorganisms using fungi
    • Y10S435/913—Aspergillus
    • Y10S435/917—Aspergillus niger
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00—Chemistry: molecular biology and microbiology
    • Y10S435/8215—Microorganisms
    • Y10S435/911—Microorganisms using fungi
    • Y10S435/921—Candida
    • Y10S435/923—Candida lipolytica

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Zoology (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
DE69111355T 1990-10-05 1991-09-23 Verfahren zur Herstellung von granulierter Zitronensäure und ihrer Salze. Expired - Fee Related DE69111355T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/594,548 US5045459A (en) 1990-10-05 1990-10-05 Method for the production of granular citric acid
US07/692,616 US5104799A (en) 1990-10-05 1991-04-29 Method for the production of granular citric acid and salts thereof

Publications (2)

Publication Number Publication Date
DE69111355D1 true DE69111355D1 (de) 1995-08-24
DE69111355T2 DE69111355T2 (de) 1996-01-04

Family

ID=27082008

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69111355T Expired - Fee Related DE69111355T2 (de) 1990-10-05 1991-09-23 Verfahren zur Herstellung von granulierter Zitronensäure und ihrer Salze.

Country Status (9)

Country Link
US (1) US5104799A (de)
EP (1) EP0479084B1 (de)
JP (1) JPH04262786A (de)
AT (1) ATE125249T1 (de)
CA (1) CA2051366A1 (de)
DE (1) DE69111355T2 (de)
ES (1) ES2074620T3 (de)
GR (1) GR3017363T3 (de)
MX (1) MX9101283A (de)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4027927A1 (de) * 1990-09-04 1992-03-05 Bayer Ag Brausekomponente und verfahren zu ihrer herstellung
US5268283A (en) * 1990-10-05 1993-12-07 Miles Inc. Method for the production of detergent builder formulations utilizing spray granulated citric acid and salts thereof
US5352825A (en) * 1993-07-06 1994-10-04 Hoarmann & Reimer Corp. Recovery of organic acid salts from impure process streams by addition of bases
AU7471694A (en) * 1993-07-12 1995-02-13 Avraham Baniel A process for the production of water-soluble salts of carboxylic and amino acids
ES2173976T3 (es) * 1994-09-12 2002-11-01 Aeci Ltd Procedimiento para recuperar acido citrico.
US5965028A (en) * 1994-09-12 1999-10-12 Reilly Industries, Inc. Process for treating a liquid
AT402923B (de) * 1995-06-06 1997-09-25 Jungbunzlauer Ag Wasserfreies trinatriumcitrat, verfahren zu seiner herstellung und seine verwendung als trägermaterial
US5532148A (en) * 1995-08-30 1996-07-02 Ntec, Inc. Process for producing of citric acid and monovalent citrate salts
SK279219B6 (sk) * 1995-10-27 1998-08-05 Likospol Spôsob koncentračnej purifikácie kyseliny citrónov
US20040081735A1 (en) * 1998-12-18 2004-04-29 Birgit Schleifenbaum Encapsulated flavor and/or fragrance preparations
DE19956604A1 (de) * 1998-12-18 2000-11-02 Haarmann & Reimer Gmbh Eingekapselte Aroma- und/oder Riechstoffzubereitungen
DE102005056669A1 (de) * 2005-11-28 2007-05-31 Basf Ag Fermentative Herstellung organischer Verbindungen unter Einsatz Dextrin-haltiger Medien
DE102006004833A1 (de) * 2006-02-02 2007-08-16 Holger Mannweiler Verfahren zum Trocknen von Saft
CA2615150A1 (en) * 2006-12-20 2008-06-20 Kraft Foods Holdings, Inc. Instant acidified milk beverages
CN106146292B (zh) * 2015-04-02 2018-09-11 中粮生物化学（安徽）股份有限公司 一种无水柠檬酸晶体的生产方法
CN105111070B (zh) * 2015-08-28 2017-01-11 安徽丰原马鞍山生物化学有限公司 一种柠檬酸钾的制备方法
CN115572222B (zh) * 2022-08-11 2024-05-10 山东金禾保健品有限公司 一种柠檬酸钙球形晶体的制备方法及其应用

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3086928A (en) * 1958-08-09 1963-04-23 Benckiser Gmbh Joh A Process of producing citric acid
US4391908A (en) * 1967-06-07 1983-07-05 Takeda Chemical Industries, Ltd. Method for producing citric acids
US3936352A (en) * 1970-06-01 1976-02-03 Aktiengesellschaft Jungbunzlauer Spiritus- Und Chemische Fabrik Process for the production of citric acid
IL39710A (en) * 1972-06-19 1975-04-25 Imi Inst For Res & Dev Recovery of acids from aqueous solutions by solvent extraction
DE2360091A1 (de) * 1972-12-06 1974-07-04 Erap Verfahren zur herstellung von zitronensaeure durch fermentation
US4178211A (en) * 1977-03-03 1979-12-11 Ethyl Corporation Process for producing citric acid
JPS53144526A (en) * 1977-05-19 1978-12-15 Tokuyama Soda Co Ltd Recovery of organic acid
IT1099546B (it) * 1978-10-27 1985-09-18 Euteco Spa Procedimento per la preparazione di acido citrico
JPS5886091A (ja) * 1981-11-18 1983-05-23 Showa Shell Sekiyu Kk クエン酸の製法
JPS58118538A (ja) * 1981-12-29 1983-07-14 Toray Eng Co Ltd 有機酸の回収方法
DE3570866D1 (en) * 1984-02-03 1989-07-13 Ladenburg Biochemie Process for the isolation of citric acid
DE3502924A1 (de) * 1984-02-03 1985-08-08 Joh. A. Benckiser Gmbh, 6700 Ludwigshafen Verfahren zur gewinnung von citronensaeure
DE3808277A1 (de) * 1988-03-12 1989-09-21 Bayer Ag Verfahren und vorrichtung zur wirbelschichtspruehgranulation
EP0163836B1 (de) * 1984-04-07 1988-10-12 Bayer Ag Verfahren und Vorrichtung zur Herstellung von Granulaten
DE3425358A1 (de) * 1984-07-10 1986-02-20 Hoechst Ag, 6230 Frankfurt Verfahren zur isolierung wasserloeslicher saurer verbindungen
US4851573A (en) * 1986-12-18 1989-07-25 Uop Separation of citric acid from fermentation broth with a weakly basic anionic exchange resin adsorbent
KR890005273A (ko) * 1987-09-09 1989-05-13 이정오 2중 실관 반응기에 의한 구연산의 연속 생산방법

Also Published As

Publication number Publication date
DE69111355T2 (de) 1996-01-04
ATE125249T1 (de) 1995-08-15
CA2051366A1 (en) 1992-04-06
EP0479084A2 (de) 1992-04-08
EP0479084A3 (en) 1992-12-02
JPH04262786A (ja) 1992-09-18
ES2074620T3 (es) 1995-09-16
EP0479084B1 (de) 1995-07-19
MX9101283A (es) 1994-05-31
US5104799A (en) 1992-04-14
GR3017363T3 (en) 1995-12-31

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee
8327 Change in the person/name/address of the patent owner

Owner name: TATE & LYLE CITRIC ACID, INC., DECATUR, ILL., US

8328 Change in the person/name/address of the agent

Free format text: REITSTOETTER, KINZEBACH & PARTNER, 81679 MUENCHEN