ES2074620T3 - Metodo para la produccion de acido citrico granular y sales del mismo. - Google Patents

Metodo para la produccion de acido citrico granular y sales del mismo.

Info

Publication number
ES2074620T3
ES2074620T3 ES91116121T ES91116121T ES2074620T3 ES 2074620 T3 ES2074620 T3 ES 2074620T3 ES 91116121 T ES91116121 T ES 91116121T ES 91116121 T ES91116121 T ES 91116121T ES 2074620 T3 ES2074620 T3 ES 2074620T3
Authority
ES
Spain
Prior art keywords
citric acid
salts
production
salt
granular citric
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES91116121T
Other languages
English (en)
Inventor
Helmut A Mothes
Bhalchandra H Patwardhan
Theo G Schroeder
David J Solow
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Haarmann and Reimer Corp
Original Assignee
Haarmann and Reimer Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US07/594,548 external-priority patent/US5045459A/en
Application filed by Haarmann and Reimer Corp filed Critical Haarmann and Reimer Corp
Application granted granted Critical
Publication of ES2074620T3 publication Critical patent/ES2074620T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/40—Preparation of oxygen-containing organic compounds containing a carboxyl group including Peroxycarboxylic acids
    • C12P7/44—Polycarboxylic acids
    • C12P7/48—Tricarboxylic acids, e.g. citric acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00—Chemistry: molecular biology and microbiology
    • Y10S435/80—Elimination or reduction of contamination by undersired ferments, e.g. aseptic cultivation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00—Chemistry: molecular biology and microbiology
    • Y10S435/8215—Microorganisms
    • Y10S435/911—Microorganisms using fungi
    • Y10S435/913—Aspergillus
    • Y10S435/917—Aspergillus niger
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S435/00—Chemistry: molecular biology and microbiology
    • Y10S435/8215—Microorganisms
    • Y10S435/911—Microorganisms using fungi
    • Y10S435/921—Candida
    • Y10S435/923—Candida lipolytica

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Zoology (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

SE PRESENTA UN METODO MEJORADO PARA PREPARAR UN ACIDO CITRICO EN PARTICULAS O UN METAL ALCALI O UNA SAL DE METAL DE TIERRA ALCALINA DEL MISMO. EL METODO COMPRENDE EL ROCIADO GRANULANTE DEL ACIDO CITRICO O UNA SAL DEL MISMO DE SU CALDO DE FERMENTACION PARCIALMENTE PURIFICADO PARA FORMAR GRANULOS QUE FLUYEN MAS LIBREMENTE Y ESTAN MENOS INCLINADOS A FRACTURARSE QUE SU ACIDO CITRICO O SUS SALES PREPARADAS MEDIANTE TECNICAS DE CRISTALIZACION, DICHAS PROPIEDADES CONVIERTEN AL MATERIAL PREPARADO MEDIANTE EL PRESENTE METODO MAS ADECUADO PARA SU MANEJO EN BRUTO
ES91116121T 1990-10-05 1991-09-23 Metodo para la produccion de acido citrico granular y sales del mismo. Expired - Lifetime ES2074620T3 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/594,548 US5045459A (en) 1990-10-05 1990-10-05 Method for the production of granular citric acid
US07/692,616 US5104799A (en) 1990-10-05 1991-04-29 Method for the production of granular citric acid and salts thereof

Publications (1)

Publication Number Publication Date
ES2074620T3 true ES2074620T3 (es) 1995-09-16

Family

ID=27082008

Family Applications (1)

Application Number Title Priority Date Filing Date
ES91116121T Expired - Lifetime ES2074620T3 (es) 1990-10-05 1991-09-23 Metodo para la produccion de acido citrico granular y sales del mismo.

Country Status (9)

Country Link
US (1) US5104799A (es)
EP (1) EP0479084B1 (es)
JP (1) JPH04262786A (es)
AT (1) ATE125249T1 (es)
CA (1) CA2051366A1 (es)
DE (1) DE69111355T2 (es)
ES (1) ES2074620T3 (es)
GR (1) GR3017363T3 (es)
MX (1) MX9101283A (es)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4027927A1 (de) * 1990-09-04 1992-03-05 Bayer Ag Brausekomponente und verfahren zu ihrer herstellung
US5268283A (en) * 1990-10-05 1993-12-07 Miles Inc. Method for the production of detergent builder formulations utilizing spray granulated citric acid and salts thereof
US5352825A (en) * 1993-07-06 1994-10-04 Hoarmann & Reimer Corp. Recovery of organic acid salts from impure process streams by addition of bases
AU7471694A (en) * 1993-07-12 1995-02-13 Avraham Baniel A process for the production of water-soluble salts of carboxylic and amino acids
ES2173976T3 (es) * 1994-09-12 2002-11-01 Aeci Ltd Procedimiento para recuperar acido citrico.
US5965028A (en) * 1994-09-12 1999-10-12 Reilly Industries, Inc. Process for treating a liquid
AT402923B (de) * 1995-06-06 1997-09-25 Jungbunzlauer Ag Wasserfreies trinatriumcitrat, verfahren zu seiner herstellung und seine verwendung als trägermaterial
US5532148A (en) * 1995-08-30 1996-07-02 Ntec, Inc. Process for producing of citric acid and monovalent citrate salts
SK279219B6 (sk) * 1995-10-27 1998-08-05 Likospol Spôsob koncentračnej purifikácie kyseliny citrónov
US20040081735A1 (en) * 1998-12-18 2004-04-29 Birgit Schleifenbaum Encapsulated flavor and/or fragrance preparations
DE19956604A1 (de) * 1998-12-18 2000-11-02 Haarmann & Reimer Gmbh Eingekapselte Aroma- und/oder Riechstoffzubereitungen
DE102005056669A1 (de) * 2005-11-28 2007-05-31 Basf Ag Fermentative Herstellung organischer Verbindungen unter Einsatz Dextrin-haltiger Medien
DE102006004833A1 (de) * 2006-02-02 2007-08-16 Holger Mannweiler Verfahren zum Trocknen von Saft
CA2615150A1 (en) * 2006-12-20 2008-06-20 Kraft Foods Holdings, Inc. Instant acidified milk beverages
CN106146292B (zh) * 2015-04-02 2018-09-11 中粮生物化学（安徽）股份有限公司 一种无水柠檬酸晶体的生产方法
CN105111070B (zh) * 2015-08-28 2017-01-11 安徽丰原马鞍山生物化学有限公司 一种柠檬酸钾的制备方法
CN115572222B (zh) * 2022-08-11 2024-05-10 山东金禾保健品有限公司 一种柠檬酸钙球形晶体的制备方法及其应用

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3086928A (en) * 1958-08-09 1963-04-23 Benckiser Gmbh Joh A Process of producing citric acid
US4391908A (en) * 1967-06-07 1983-07-05 Takeda Chemical Industries, Ltd. Method for producing citric acids
US3936352A (en) * 1970-06-01 1976-02-03 Aktiengesellschaft Jungbunzlauer Spiritus- Und Chemische Fabrik Process for the production of citric acid
IL39710A (en) * 1972-06-19 1975-04-25 Imi Inst For Res & Dev Recovery of acids from aqueous solutions by solvent extraction
DE2360091A1 (de) * 1972-12-06 1974-07-04 Erap Verfahren zur herstellung von zitronensaeure durch fermentation
US4178211A (en) * 1977-03-03 1979-12-11 Ethyl Corporation Process for producing citric acid
JPS53144526A (en) * 1977-05-19 1978-12-15 Tokuyama Soda Co Ltd Recovery of organic acid
IT1099546B (it) * 1978-10-27 1985-09-18 Euteco Spa Procedimento per la preparazione di acido citrico
JPS5886091A (ja) * 1981-11-18 1983-05-23 Showa Shell Sekiyu Kk クエン酸の製法
JPS58118538A (ja) * 1981-12-29 1983-07-14 Toray Eng Co Ltd 有機酸の回収方法
DE3570866D1 (en) * 1984-02-03 1989-07-13 Ladenburg Biochemie Process for the isolation of citric acid
DE3502924A1 (de) * 1984-02-03 1985-08-08 Joh. A. Benckiser Gmbh, 6700 Ludwigshafen Verfahren zur gewinnung von citronensaeure
DE3808277A1 (de) * 1988-03-12 1989-09-21 Bayer Ag Verfahren und vorrichtung zur wirbelschichtspruehgranulation
EP0163836B1 (de) * 1984-04-07 1988-10-12 Bayer Ag Verfahren und Vorrichtung zur Herstellung von Granulaten
DE3425358A1 (de) * 1984-07-10 1986-02-20 Hoechst Ag, 6230 Frankfurt Verfahren zur isolierung wasserloeslicher saurer verbindungen
US4851573A (en) * 1986-12-18 1989-07-25 Uop Separation of citric acid from fermentation broth with a weakly basic anionic exchange resin adsorbent
KR890005273A (ko) * 1987-09-09 1989-05-13 이정오 2중 실관 반응기에 의한 구연산의 연속 생산방법

Also Published As

Publication number Publication date
DE69111355T2 (de) 1996-01-04
ATE125249T1 (de) 1995-08-15
DE69111355D1 (de) 1995-08-24
CA2051366A1 (en) 1992-04-06
EP0479084A2 (en) 1992-04-08
EP0479084A3 (en) 1992-12-02
JPH04262786A (ja) 1992-09-18
EP0479084B1 (en) 1995-07-19
MX9101283A (es) 1994-05-31
US5104799A (en) 1992-04-14
GR3017363T3 (en) 1995-12-31

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