DE602005000922T2 - Verfahren und vorrichtung zur steuerung der zufuhr von katalysatorschlamm in einen polymerisationsreaktor - Google Patents
Verfahren und vorrichtung zur steuerung der zufuhr von katalysatorschlamm in einen polymerisationsreaktor Download PDFInfo
- Publication number
- DE602005000922T2 DE602005000922T2 DE602005000922T DE602005000922T DE602005000922T2 DE 602005000922 T2 DE602005000922 T2 DE 602005000922T2 DE 602005000922 T DE602005000922 T DE 602005000922T DE 602005000922 T DE602005000922 T DE 602005000922T DE 602005000922 T2 DE602005000922 T2 DE 602005000922T2
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- catalyst
- reactor
- catalyst slurry
- slurry
- cocatalyst
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- MCULRUJILOGHCJ-UHFFFAOYSA-N triisobutylaluminium Chemical compound CC(C)C[Al](CC(C)C)CC(C)C MCULRUJILOGHCJ-UHFFFAOYSA-N 0.000 description 19
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- 238000001704 evaporation Methods 0.000 description 2
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- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
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- SIPUZPBQZHNSDW-UHFFFAOYSA-N bis(2-methylpropyl)aluminum Chemical compound CC(C)C[Al]CC(C)C SIPUZPBQZHNSDW-UHFFFAOYSA-N 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
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- YNLAOSYQHBDIKW-UHFFFAOYSA-M diethylaluminium chloride Chemical compound CC[Al](Cl)CC YNLAOSYQHBDIKW-UHFFFAOYSA-M 0.000 description 1
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- GCPCLEKQVMKXJM-UHFFFAOYSA-N ethoxy(diethyl)alumane Chemical compound CCO[Al](CC)CC GCPCLEKQVMKXJM-UHFFFAOYSA-N 0.000 description 1
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- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 description 1
- 125000004836 hexamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
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- 238000011068 loading method Methods 0.000 description 1
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 1
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- 150000003608 titanium Chemical class 0.000 description 1
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- ORYGRKHDLWYTKX-UHFFFAOYSA-N trihexylalumane Chemical compound CCCCCC[Al](CCCCCC)CCCCCC ORYGRKHDLWYTKX-UHFFFAOYSA-N 0.000 description 1
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- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
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- B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
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- B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
- B01J8/003—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor in a downward flow
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- B01J8/005—Separating solid material from the gas/liquid stream
- B01J8/007—Separating solid material from the gas/liquid stream by sedimentation
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- B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
- B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
- B01J8/224—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement
- B01J8/226—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement internally, i.e. the particles rotate within the vessel
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
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- B01J2208/00008—Controlling the process
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- B01J2208/00557—Flow controlling the residence time inside the reactor vessel
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F110/00—Homopolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S526/00—Synthetic resins or natural rubbers -- part of the class 520 series
- Y10S526/919—Catalyst injection technique in addition polymerization processes
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/8593—Systems
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- Polymerisation Methods In General (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
- Treatment Of Sludge (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP04100570A EP1563902A1 (en) | 2004-02-13 | 2004-02-13 | Method and apparatus for preparing and supplying catalyst slurry to a polymerization reactor. |
| EP04100570 | 2004-02-13 | ||
| EP04100597 | 2004-02-13 | ||
| EP04100597 | 2004-02-13 | ||
| PCT/EP2005/050625 WO2005077522A1 (en) | 2004-02-13 | 2005-02-14 | Method and apparatus for preparing and supplying catalyst slurry to a polymerisation reactor. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE602005000922D1 DE602005000922D1 (de) | 2007-05-31 |
| DE602005000922T2 true DE602005000922T2 (de) | 2008-01-17 |
Family
ID=34863115
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE602005000922T Expired - Lifetime DE602005000922T2 (de) | 2004-02-13 | 2005-02-14 | Verfahren und vorrichtung zur steuerung der zufuhr von katalysatorschlamm in einen polymerisationsreaktor |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US7906597B2 (enExample) |
| EP (1) | EP1660231B1 (enExample) |
| JP (2) | JP5074771B2 (enExample) |
| KR (1) | KR101081670B1 (enExample) |
| AT (1) | ATE359864T1 (enExample) |
| DE (1) | DE602005000922T2 (enExample) |
| DK (1) | DK1660231T3 (enExample) |
| EA (1) | EA010549B1 (enExample) |
| ES (1) | ES2285686T3 (enExample) |
| PT (1) | PT1660231E (enExample) |
| WO (1) | WO2005077522A1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102010056133B4 (de) | 2010-05-22 | 2023-02-16 | Audi Ag | Verfahren zur Herstellung von Elektrodenmaterial mit ein oder mehreren Katalysatorschichten oder funktionellen Schichten für eine PEM-Brennstoffzelle |
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| EP1999161B1 (en) * | 2006-03-30 | 2013-02-13 | Total Research & Technology Feluy | Slurry polymerisation process of ethylene in the presence of low amount of scavenger. |
| US20080087336A1 (en) * | 2006-10-11 | 2008-04-17 | Canon Kabushiki Kaisha | Fluid-processing apparatus and fluid-processing system |
| CN101674880B (zh) * | 2007-02-05 | 2015-05-27 | 巴塞尔聚烯烃意大利有限责任公司 | 用于烯烃液相聚合的设备 |
| TWI433855B (zh) * | 2008-06-04 | 2014-04-11 | Univation Tech Llc | 漿液觸媒流分流器及其使用方法 |
| KR20110097788A (ko) * | 2008-11-18 | 2011-08-31 | 토탈 페트로케미칼스 리서치 펠루이 | 중합 반응기로의 촉매 슬러리의 공급을 최적화하는 방법 |
| EP2319616A1 (en) | 2009-11-09 | 2011-05-11 | Ineos Usa Llc | Particulate flow control process |
| RS53659B1 (sr) * | 2009-12-18 | 2015-04-30 | Total Research & Technology Feluy | Postupak za kontrolisanje nivoa suspenzije katalizatora pri polimerizaciji etilena |
| EP2387590B2 (en) † | 2009-12-18 | 2019-12-25 | Total Research & Technology Feluy | Method for replacing compatible ethylene polymerization catalysts |
| CN102762608B (zh) * | 2009-12-18 | 2014-08-20 | 道达尔研究技术弗吕公司 | 用于中和聚合催化剂的方法 |
| KR101522080B1 (ko) * | 2009-12-18 | 2015-05-20 | 토탈 리서치 앤드 테크놀로지 펠루이 | 비호환성 에틸렌 중합 촉매 대체 방법 |
| KR20120115326A (ko) * | 2009-12-18 | 2012-10-17 | 토탈 리서치 앤드 테크놀로지 펠루이 | 촉매 슬러리 블렌드의 제조 방법 |
| EP2383298A1 (en) † | 2010-04-30 | 2011-11-02 | Ineos Europe Limited | Polymerization process |
| EP2386352A1 (en) | 2010-05-12 | 2011-11-16 | Ineos Europe Limited | Reactor |
| WO2012013800A1 (en) * | 2010-07-30 | 2012-02-02 | Total Petrochemicals Research Feluy | Process for supplying catalyst to a polymerization reactor |
| US8728971B2 (en) | 2010-07-30 | 2014-05-20 | Total Research & Technology Feluy | Pressure control of the catalyst mixing vessel |
| EA027699B1 (ru) * | 2010-07-30 | 2017-08-31 | Тотал Рисерч Энд Текнолоджи Фелюй | Применение установки приготовления суспензии катализатора |
| CA2740755C (en) * | 2011-05-25 | 2019-01-15 | Nova Chemicals Corporation | Chromium catalysts for olefin polymerization |
| CA2749835C (en) | 2011-08-23 | 2018-08-21 | Nova Chemicals Corporation | Feeding highly active phosphinimine catalysts to a gas phase reactor |
| US9376517B2 (en) * | 2011-12-28 | 2016-06-28 | Ineos Europe Ag | Polymerisation process |
| US8821800B2 (en) * | 2012-10-18 | 2014-09-02 | Chevron Phillips Chemical Company Lp | System and method for catalyst preparation |
| JP6022976B2 (ja) * | 2013-03-14 | 2016-11-09 | 日本ポリエチレン株式会社 | オレフィン重合用固体触媒の保存方法及びその触媒を用いたオレフィン重合体の製造方法 |
| JP5981865B2 (ja) * | 2013-03-14 | 2016-08-31 | 日本ポリエチレン株式会社 | オレフィン重合用固体触媒の保存方法及びその触媒を用いたオレフィン重合体の製造方法 |
| KR101523568B1 (ko) | 2013-05-16 | 2015-05-28 | 대림산업 주식회사 | 반응성 폴리부텐 및 비반응성 폴리부텐의 선택적 제조장치 및 방법 |
| BR112015030132B1 (pt) * | 2013-06-05 | 2022-02-22 | Daelim Industrial Co., Ltd | Aparelho e método para preparar polibuteno com vários pesos moleculares |
| US10464071B2 (en) | 2013-09-18 | 2019-11-05 | Schlumberger Technology Corporation | System and method for preparing a treatment fluid |
| US9295964B2 (en) * | 2013-09-19 | 2016-03-29 | Chevron Phillips Chemical Company, Lp | Pressure relief for multiple polyolefin polymerization reactors |
| CN104043315B (zh) * | 2014-05-23 | 2016-06-01 | 四川天采科技有限责任公司 | 一种从高低压炼厂干气中回收氢气、乙烯的方法 |
| AR102845A1 (es) * | 2015-03-18 | 2017-03-29 | Schlumberger Technology Bv | Sistema y método para preparar un fluido de tratamiento |
| WO2017151694A1 (en) | 2016-03-01 | 2017-09-08 | Schlumberger Technology Corporation | Well treatment methods |
| WO2018193031A1 (en) * | 2017-04-19 | 2018-10-25 | Ashe Morris Ltd | Method and apparatus for handling slurries in flow systems |
| US10697889B2 (en) | 2017-07-21 | 2020-06-30 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
| US10030086B1 (en) | 2017-07-21 | 2018-07-24 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
| US10679734B2 (en) | 2018-03-29 | 2020-06-09 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
| US10507445B2 (en) | 2018-03-29 | 2019-12-17 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
| CN108379881B (zh) * | 2018-05-04 | 2023-10-03 | 常州合全药业有限公司 | 一种脱氧连续加料装置及加料方法 |
| JP6437153B1 (ja) | 2018-06-26 | 2018-12-12 | 住友化学株式会社 | スラリーの移送方法、ポリオレフィンの製造方法、およびその利用 |
| FR3083526B1 (fr) | 2018-07-04 | 2020-07-31 | Crealyst Group | Systeme de remplissage perfectionne |
| CN114901391B (zh) * | 2019-11-26 | 2024-11-26 | 埃克森美孚化学专利公司 | 生产负载型催化剂的系统和方法 |
| US11833479B2 (en) * | 2020-03-26 | 2023-12-05 | Chevron Phillips Chemical Company Lp | Catalyst slurry mixing process and system |
| CN111890146B (zh) * | 2020-07-16 | 2022-02-11 | 徐州徐工液压件有限公司 | 用于无心磨床的磨削液自动循环和物化沉淀压滤净化装置 |
| US11512150B2 (en) | 2020-11-17 | 2022-11-29 | Ineos Usa Llc | Polymerization process |
| JP7698718B2 (ja) * | 2020-11-27 | 2025-06-25 | ボレアリス・アクチェンゲゼルシャフト | 触媒供給システム |
| CN112387238A (zh) * | 2020-12-11 | 2021-02-23 | 新乡贝诺电子信息技术有限公司 | 一种可快速清理输料管的化学品制作用反应装置 |
| EP4301792A2 (en) | 2021-03-05 | 2024-01-10 | ExxonMobil Chemical Patents Inc. | Processes for making and using slurry catalyst mixtures |
| KR102702921B1 (ko) * | 2021-04-13 | 2024-09-03 | 한화솔루션 주식회사 | 슬러리 용액의 촉매 농도 측정 방법 및 이를 이용한 수첨 석유 수지의 연속적 제조 방법 |
| WO2025090149A1 (en) * | 2023-10-23 | 2025-05-01 | ExxonMobil Technology and Engineering Company | Methods for modifying a supported catalyst during olefin polymerization through pressurized delivery of a catalyst solution |
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| US2917465A (en) * | 1956-04-27 | 1959-12-15 | Phillips Petroleum Co | Polymerization catalyst feed control |
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| JPS5879533A (ja) * | 1981-11-05 | 1983-05-13 | Mitsui Petrochem Ind Ltd | 触媒の供給方法 |
| US4619901A (en) * | 1985-02-21 | 1986-10-28 | Phillips Petroleum Company | Control of polymerization reaction |
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| US5098677A (en) | 1991-04-05 | 1992-03-24 | The United States Of America As Represented By The Department Of Energy | Actinide metal processing |
| US5644007A (en) * | 1996-04-26 | 1997-07-01 | Minnesota Mining And Manufacturing Company | Continuous process for the production of poly(1-alkenes) |
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| US6916892B2 (en) * | 2001-12-03 | 2005-07-12 | Fina Technology, Inc. | Method for transitioning between Ziegler-Natta and metallocene catalysts in a bulk loop reactor for the production of polypropylene |
| JP2004011514A (ja) * | 2002-06-06 | 2004-01-15 | Sumitomo Electric Ind Ltd | マイクロポンプ、その製造方法および使用方法 |
-
2005
- 2005-02-14 DK DK05716677T patent/DK1660231T3/da active
- 2005-02-14 EP EP05716677A patent/EP1660231B1/en not_active Revoked
- 2005-02-14 JP JP2006552631A patent/JP5074771B2/ja not_active Expired - Fee Related
- 2005-02-14 DE DE602005000922T patent/DE602005000922T2/de not_active Expired - Lifetime
- 2005-02-14 PT PT05716677T patent/PT1660231E/pt unknown
- 2005-02-14 ES ES05716677T patent/ES2285686T3/es not_active Expired - Lifetime
- 2005-02-14 WO PCT/EP2005/050625 patent/WO2005077522A1/en not_active Ceased
- 2005-02-14 AT AT05716677T patent/ATE359864T1/de not_active IP Right Cessation
- 2005-02-14 EA EA200601489A patent/EA010549B1/ru not_active IP Right Cessation
- 2005-02-14 US US10/589,315 patent/US7906597B2/en not_active Expired - Fee Related
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2006
- 2006-09-05 KR KR1020067018026A patent/KR101081670B1/ko not_active Expired - Fee Related
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2011
- 2011-10-06 JP JP2011222055A patent/JP2012001739A/ja active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102010056133B4 (de) | 2010-05-22 | 2023-02-16 | Audi Ag | Verfahren zur Herstellung von Elektrodenmaterial mit ein oder mehreren Katalysatorschichten oder funktionellen Schichten für eine PEM-Brennstoffzelle |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20060126591A (ko) | 2006-12-07 |
| ATE359864T1 (de) | 2007-05-15 |
| US7906597B2 (en) | 2011-03-15 |
| JP2012001739A (ja) | 2012-01-05 |
| WO2005077522A1 (en) | 2005-08-25 |
| US20080039596A1 (en) | 2008-02-14 |
| JP2007525577A (ja) | 2007-09-06 |
| EP1660231A1 (en) | 2006-05-31 |
| EA010549B1 (ru) | 2008-10-30 |
| JP5074771B2 (ja) | 2012-11-14 |
| DE602005000922D1 (de) | 2007-05-31 |
| EA200601489A1 (ru) | 2007-02-27 |
| DK1660231T3 (da) | 2007-08-13 |
| PT1660231E (pt) | 2007-06-12 |
| KR101081670B1 (ko) | 2011-11-09 |
| EP1660231B1 (en) | 2007-04-18 |
| ES2285686T3 (es) | 2007-11-16 |
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