DK1660231T3 - Fremgangsmåde og anordning til fremstilling og tilförsel af katalysatoropslemning til en polymeriseringsreaktor - Google Patents
Fremgangsmåde og anordning til fremstilling og tilförsel af katalysatoropslemning til en polymeriseringsreaktorInfo
- Publication number
- DK1660231T3 DK1660231T3 DK05716677T DK05716677T DK1660231T3 DK 1660231 T3 DK1660231 T3 DK 1660231T3 DK 05716677 T DK05716677 T DK 05716677T DK 05716677 T DK05716677 T DK 05716677T DK 1660231 T3 DK1660231 T3 DK 1660231T3
- Authority
- DK
- Denmark
- Prior art keywords
- reactor
- preparing
- polymerization reactor
- catalyst
- catalyst slurry
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
- B01J8/0035—Periodical feeding or evacuation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
- B01J8/003—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor in a downward flow
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/005—Separating solid material from the gas/liquid stream
- B01J8/007—Separating solid material from the gas/liquid stream by sedimentation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
- B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
- B01J8/224—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement
- B01J8/226—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement internally, i.e. the particles rotate within the vessel
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F10/02—Ethene
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
- B01J2208/00212—Plates; Jackets; Cylinders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00548—Flow
- B01J2208/00557—Flow controlling the residence time inside the reactor vessel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00619—Controlling the weight
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00743—Feeding or discharging of solids
- B01J2208/00752—Feeding
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F110/00—Homopolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F110/02—Ethene
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S526/00—Synthetic resins or natural rubbers -- part of the class 520 series
- Y10S526/919—Catalyst injection technique in addition polymerization processes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/8593—Systems
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- Polymerisation Methods In General (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
- Treatment Of Sludge (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP04100597 | 2004-02-13 | ||
EP04100570A EP1563902A1 (en) | 2004-02-13 | 2004-02-13 | Method and apparatus for preparing and supplying catalyst slurry to a polymerization reactor. |
PCT/EP2005/050625 WO2005077522A1 (en) | 2004-02-13 | 2005-02-14 | Method and apparatus for preparing and supplying catalyst slurry to a polymerisation reactor. |
Publications (1)
Publication Number | Publication Date |
---|---|
DK1660231T3 true DK1660231T3 (da) | 2007-08-13 |
Family
ID=34863115
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DK05716677T DK1660231T3 (da) | 2004-02-13 | 2005-02-14 | Fremgangsmåde og anordning til fremstilling og tilförsel af katalysatoropslemning til en polymeriseringsreaktor |
Country Status (11)
Country | Link |
---|---|
US (1) | US7906597B2 (da) |
EP (1) | EP1660231B1 (da) |
JP (2) | JP5074771B2 (da) |
KR (1) | KR101081670B1 (da) |
AT (1) | ATE359864T1 (da) |
DE (1) | DE602005000922T2 (da) |
DK (1) | DK1660231T3 (da) |
EA (1) | EA010549B1 (da) |
ES (1) | ES2285686T3 (da) |
PT (1) | PT1660231E (da) |
WO (1) | WO2005077522A1 (da) |
Families Citing this family (47)
Publication number | Priority date | Publication date | Assignee | Title |
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US8492489B2 (en) * | 2004-02-13 | 2013-07-23 | Total Petrochemicals Research Feluy | Double loop technology |
EP1832338A1 (en) * | 2006-03-07 | 2007-09-12 | Total Petrochemicals Research Feluy | Method and system for determining catalyst activity |
US7847042B2 (en) * | 2006-03-30 | 2010-12-07 | Total Petrochemicals Research Feluy | Slurry polymerisation process of ethylene in the presence of low amount of scavenger |
US20080087336A1 (en) * | 2006-10-11 | 2008-04-17 | Canon Kabushiki Kaisha | Fluid-processing apparatus and fluid-processing system |
BRPI0807128B1 (pt) * | 2007-02-05 | 2018-05-29 | Basell Poliolefine Italia S.R.L. | Aparelho para a polimerização de olefinas em fase líquida |
TWI433855B (zh) * | 2008-06-04 | 2014-04-11 | Univation Tech Llc | 漿液觸媒流分流器及其使用方法 |
KR20110097788A (ko) * | 2008-11-18 | 2011-08-31 | 토탈 페트로케미칼스 리서치 펠루이 | 중합 반응기로의 촉매 슬러리의 공급을 최적화하는 방법 |
EP2319616A1 (en) | 2009-11-09 | 2011-05-11 | Ineos Usa Llc | Particulate flow control process |
CN102762607B (zh) * | 2009-12-18 | 2015-02-04 | 道达尔研究技术弗吕公司 | 用于生产催化剂淤浆共混物的方法 |
EP2513165B1 (en) | 2009-12-18 | 2015-07-22 | Total Research & Technology Feluy | Method for neutralizing polymerization catalyst |
ES2524827T3 (es) * | 2009-12-18 | 2014-12-12 | Total Research & Technology Feluy | Procedimiento de supervisión del nivel de una suspensión de catalizador de polimerización de etileno |
MX2012006793A (es) * | 2009-12-18 | 2012-10-05 | Total Petrochemicals Res Feluy | Metodos para remplazar catalizadores de polimerizacion de etileno imcompatibles. |
BR112012014866B1 (pt) * | 2009-12-18 | 2020-12-01 | Total Petrochemicals Research Feluy | método para otimizar a alimentação sequencial de pelo menos dois catalisadores de polimerização de etileno em um reator de polimerização de etileno |
EP2383298A1 (en) | 2010-04-30 | 2011-11-02 | Ineos Europe Limited | Polymerization process |
EP2386352A1 (en) | 2010-05-12 | 2011-11-16 | Ineos Europe Limited | Reactor |
DE102010056133B4 (de) | 2010-05-22 | 2023-02-16 | Audi Ag | Verfahren zur Herstellung von Elektrodenmaterial mit ein oder mehreren Katalysatorschichten oder funktionellen Schichten für eine PEM-Brennstoffzelle |
CN103038261B (zh) * | 2010-07-30 | 2015-05-06 | 道达尔研究技术弗吕公司 | 催化剂淤浆制备系统的用途 |
US8846831B2 (en) | 2010-07-30 | 2014-09-30 | Total Research & Technology Feluy | Process for supplying catalyst to a polymerization reactor |
US8728971B2 (en) | 2010-07-30 | 2014-05-20 | Total Research & Technology Feluy | Pressure control of the catalyst mixing vessel |
CA2740755C (en) * | 2011-05-25 | 2019-01-15 | Nova Chemicals Corporation | Chromium catalysts for olefin polymerization |
CA2749835C (en) | 2011-08-23 | 2018-08-21 | Nova Chemicals Corporation | Feeding highly active phosphinimine catalysts to a gas phase reactor |
BR112014016325A8 (pt) * | 2011-12-28 | 2017-07-04 | Ineos Europe Ag | processo de polimerização |
US8821800B2 (en) * | 2012-10-18 | 2014-09-02 | Chevron Phillips Chemical Company Lp | System and method for catalyst preparation |
JP5981865B2 (ja) * | 2013-03-14 | 2016-08-31 | 日本ポリエチレン株式会社 | オレフィン重合用固体触媒の保存方法及びその触媒を用いたオレフィン重合体の製造方法 |
JP6022976B2 (ja) * | 2013-03-14 | 2016-11-09 | 日本ポリエチレン株式会社 | オレフィン重合用固体触媒の保存方法及びその触媒を用いたオレフィン重合体の製造方法 |
KR101523568B1 (ko) * | 2013-05-16 | 2015-05-28 | 대림산업 주식회사 | 반응성 폴리부텐 및 비반응성 폴리부텐의 선택적 제조장치 및 방법 |
CN105324399B (zh) | 2013-06-05 | 2017-09-08 | 大林产业株式会社 | 制备具有多种分子量的聚丁烯的装置和方法 |
US10464071B2 (en) | 2013-09-18 | 2019-11-05 | Schlumberger Technology Corporation | System and method for preparing a treatment fluid |
US9295964B2 (en) * | 2013-09-19 | 2016-03-29 | Chevron Phillips Chemical Company, Lp | Pressure relief for multiple polyolefin polymerization reactors |
CN104043315B (zh) * | 2014-05-23 | 2016-06-01 | 四川天采科技有限责任公司 | 一种从高低压炼厂干气中回收氢气、乙烯的方法 |
AR102845A1 (es) * | 2015-03-18 | 2017-03-29 | Schlumberger Technology Bv | Sistema y método para preparar un fluido de tratamiento |
WO2017151694A1 (en) | 2016-03-01 | 2017-09-08 | Schlumberger Technology Corporation | Well treatment methods |
WO2018193031A1 (en) * | 2017-04-19 | 2018-10-25 | Ashe Morris Ltd | Method and apparatus for handling slurries in flow systems |
US10697889B2 (en) | 2017-07-21 | 2020-06-30 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
US10030086B1 (en) | 2017-07-21 | 2018-07-24 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
US10679734B2 (en) | 2018-03-29 | 2020-06-09 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
US10507445B2 (en) | 2018-03-29 | 2019-12-17 | Chevron Phillips Chemical Company Lp | Methods for determining transition metal compound concentrations in multicomponent liquid systems |
CN108379881B (zh) * | 2018-05-04 | 2023-10-03 | 常州合全药业有限公司 | 一种脱氧连续加料装置及加料方法 |
JP6437153B1 (ja) * | 2018-06-26 | 2018-12-12 | 住友化学株式会社 | スラリーの移送方法、ポリオレフィンの製造方法、およびその利用 |
EP4065277A1 (en) * | 2019-11-26 | 2022-10-05 | ExxonMobil Chemical Patents Inc. | Systems and methods for producing a supported catalyst |
US11833479B2 (en) * | 2020-03-26 | 2023-12-05 | Chevron Phillips Chemical Company Lp | Catalyst slurry mixing process and system |
CN111890146B (zh) * | 2020-07-16 | 2022-02-11 | 徐州徐工液压件有限公司 | 用于无心磨床的磨削液自动循环和物化沉淀压滤净化装置 |
US11512150B2 (en) | 2020-11-17 | 2022-11-29 | Ineos Usa Llc | Polymerization process |
MX2023006101A (es) * | 2020-11-27 | 2023-06-06 | Borealis Ag | Sistema de alimentacion de catalizador. |
CN112387238A (zh) * | 2020-12-11 | 2021-02-23 | 新乡贝诺电子信息技术有限公司 | 一种可快速清理输料管的化学品制作用反应装置 |
CN116917353A (zh) | 2021-03-05 | 2023-10-20 | 埃克森美孚化学专利公司 | 制备和使用淤浆催化剂混合物的方法 |
KR20220141477A (ko) * | 2021-04-13 | 2022-10-20 | 한화솔루션 주식회사 | 슬러리 용액의 촉매 농도 측정 방법 및 이를 이용한 수첨 석유 수지의 연속적 제조 방법 |
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US2917465A (en) * | 1956-04-27 | 1959-12-15 | Phillips Petroleum Co | Polymerization catalyst feed control |
US3726845A (en) * | 1971-03-22 | 1973-04-10 | Exxon Research Engineering Co | Supplying catalyst to a reaction zone |
JPS5879533A (ja) * | 1981-11-05 | 1983-05-13 | Mitsui Petrochem Ind Ltd | 触媒の供給方法 |
US4619901A (en) * | 1985-02-21 | 1986-10-28 | Phillips Petroleum Company | Control of polymerization reaction |
US5098667A (en) * | 1989-05-05 | 1992-03-24 | Phillips Petroleum Company | Particulate flow control |
US5098677A (en) | 1991-04-05 | 1992-03-24 | The United States Of America As Represented By The Department Of Energy | Actinide metal processing |
US5644007A (en) * | 1996-04-26 | 1997-07-01 | Minnesota Mining And Manufacturing Company | Continuous process for the production of poly(1-alkenes) |
US6399722B1 (en) * | 1999-12-01 | 2002-06-04 | Univation Technologies, Llc | Solution feed of multiple catalysts |
JP2001220405A (ja) * | 2000-02-09 | 2001-08-14 | Chisso Corp | プロピレン/オレフィンランダム共重合体およびその製造方法 |
US6916892B2 (en) * | 2001-12-03 | 2005-07-12 | Fina Technology, Inc. | Method for transitioning between Ziegler-Natta and metallocene catalysts in a bulk loop reactor for the production of polypropylene |
JP2004011514A (ja) * | 2002-06-06 | 2004-01-15 | Sumitomo Electric Ind Ltd | マイクロポンプ、その製造方法および使用方法 |
-
2005
- 2005-02-14 WO PCT/EP2005/050625 patent/WO2005077522A1/en active IP Right Grant
- 2005-02-14 AT AT05716677T patent/ATE359864T1/de not_active IP Right Cessation
- 2005-02-14 EP EP05716677A patent/EP1660231B1/en not_active Revoked
- 2005-02-14 ES ES05716677T patent/ES2285686T3/es active Active
- 2005-02-14 EA EA200601489A patent/EA010549B1/ru not_active IP Right Cessation
- 2005-02-14 DK DK05716677T patent/DK1660231T3/da active
- 2005-02-14 US US10/589,315 patent/US7906597B2/en not_active Expired - Fee Related
- 2005-02-14 JP JP2006552631A patent/JP5074771B2/ja not_active Expired - Fee Related
- 2005-02-14 PT PT05716677T patent/PT1660231E/pt unknown
- 2005-02-14 DE DE602005000922T patent/DE602005000922T2/de active Active
-
2006
- 2006-09-05 KR KR1020067018026A patent/KR101081670B1/ko not_active IP Right Cessation
-
2011
- 2011-10-06 JP JP2011222055A patent/JP2012001739A/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
EP1660231A1 (en) | 2006-05-31 |
US7906597B2 (en) | 2011-03-15 |
WO2005077522A1 (en) | 2005-08-25 |
KR20060126591A (ko) | 2006-12-07 |
US20080039596A1 (en) | 2008-02-14 |
EA200601489A1 (ru) | 2007-02-27 |
PT1660231E (pt) | 2007-06-12 |
JP2007525577A (ja) | 2007-09-06 |
DE602005000922D1 (de) | 2007-05-31 |
EP1660231B1 (en) | 2007-04-18 |
EA010549B1 (ru) | 2008-10-30 |
JP5074771B2 (ja) | 2012-11-14 |
KR101081670B1 (ko) | 2011-11-09 |
JP2012001739A (ja) | 2012-01-05 |
ES2285686T3 (es) | 2007-11-16 |
ATE359864T1 (de) | 2007-05-15 |
DE602005000922T2 (de) | 2008-01-17 |
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