DE602004013436D1 - Verfahren zur herstellung von ester durch umesterung mit einem festen sauren katalysator - Google Patents
Verfahren zur herstellung von ester durch umesterung mit einem festen sauren katalysatorInfo
- Publication number
- DE602004013436D1 DE602004013436D1 DE602004013436T DE602004013436T DE602004013436D1 DE 602004013436 D1 DE602004013436 D1 DE 602004013436D1 DE 602004013436 T DE602004013436 T DE 602004013436T DE 602004013436 T DE602004013436 T DE 602004013436T DE 602004013436 D1 DE602004013436 D1 DE 602004013436D1
- Authority
- DE
- Germany
- Prior art keywords
- ester
- acid catalyst
- solid acid
- alcohol
- starting material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000003054 catalyst Substances 0.000 title abstract 3
- 239000011973 solid acid Substances 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 5
- 150000002148 esters Chemical class 0.000 abstract 5
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- 239000007858 starting material Substances 0.000 abstract 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 abstract 2
- 238000005809 transesterification reaction Methods 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 229910052786 argon Inorganic materials 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
- 239000012808 vapor phase Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
- C11C3/10—Ester interchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/24—Chromium, molybdenum or tungsten
- B01J23/30—Tungsten
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
- B01J27/053—Sulfates
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Fats And Perfumes (AREA)
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2003083979 | 2003-03-26 | ||
JP2003083979 | 2003-03-26 | ||
PCT/JP2003/015323 WO2004085583A1 (ja) | 2003-03-26 | 2003-12-01 | 固体酸触媒を用いたエステル交換反応によるエステルの製造方法 |
WOPCT/JP03/15323 | 2003-12-01 | ||
PCT/JP2004/003731 WO2004085584A1 (ja) | 2003-03-26 | 2004-03-19 | 固体酸触媒を用いたエステル交換反応によるエステルの製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
DE602004013436D1 true DE602004013436D1 (de) | 2008-06-12 |
DE602004013436T2 DE602004013436T2 (de) | 2009-06-04 |
Family
ID=33094982
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE602004013436T Expired - Lifetime DE602004013436T2 (de) | 2003-03-26 | 2004-03-19 | Verfahren zur herstellung von ester durch umesterung mit einem festen sauren katalysator |
Country Status (8)
Country | Link |
---|---|
US (1) | US7211681B2 (de) |
EP (1) | EP1607467B1 (de) |
JP (1) | JP4994664B2 (de) |
AT (1) | ATE393808T1 (de) |
AU (1) | AU2003304018A1 (de) |
DE (1) | DE602004013436T2 (de) |
MY (1) | MY140824A (de) |
WO (2) | WO2004085583A1 (de) |
Families Citing this family (39)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1632290A4 (de) * | 2003-04-23 | 2007-06-13 | Japan Energy Corp | Zinnhaltiger fester säurekatalysator und herstellungsverfahren dafür |
US7842653B2 (en) * | 2005-06-16 | 2010-11-30 | Council Of Scientific & Industrial Research | Process for the preparation of lubricants |
JP2007022973A (ja) * | 2005-07-19 | 2007-02-01 | Kao Corp | エステルの製造方法 |
US7754643B2 (en) * | 2005-10-07 | 2010-07-13 | Council Of Scientific & Industrial Research | Transesterification catalyst and a process for the preparation thereof |
ATE440815T1 (de) * | 2005-10-10 | 2009-09-15 | Council Scient Ind Res | Verfahren zur herstellung von dialkylcarbonaten |
US7482480B2 (en) * | 2005-10-10 | 2009-01-27 | Council Of Scientific & Industrial Research | Process for the preparation of hydrocarbon fuel |
JP4976016B2 (ja) * | 2006-01-17 | 2012-07-18 | Jx日鉱日石エネルギー株式会社 | エステル交換反応によるエステルの製造方法 |
JPWO2007105306A1 (ja) * | 2006-03-14 | 2009-07-30 | 東レ株式会社 | 太陽電池用ポリエステル樹脂シート、それを用いてなる積層品、太陽電池裏面保護シート、およびモジュール |
US7795460B2 (en) * | 2006-05-05 | 2010-09-14 | Tda Research, Inc. | Method of making alkyl esters |
MX2009001280A (es) * | 2006-08-04 | 2009-06-19 | Mcneff Res Consultants Inc | Metodos y aparatos para producir esteres de alquilo a partir de cargas de alimentacion con lipidos y sistemas que incluyen los mismos. |
US7897798B2 (en) | 2006-08-04 | 2011-03-01 | Mcneff Research Consultants, Inc. | Methods and apparatus for producing alkyl esters from lipid feed stocks and systems including same |
US8445709B2 (en) | 2006-08-04 | 2013-05-21 | Mcneff Research Consultants, Inc. | Systems and methods for refining alkyl ester compositions |
MX2009008612A (es) * | 2007-02-13 | 2009-11-10 | Mcneff Res Consultants Inc | Dispositivos y metodos para la remocion selectiva de contaminantes de una composicion. |
US8017796B2 (en) | 2007-02-13 | 2011-09-13 | Mcneff Research Consultants, Inc. | Systems for selective removal of contaminants from a composition and methods of regenerating the same |
US7833931B2 (en) * | 2007-03-27 | 2010-11-16 | Dic Corporation | Solid acid catalyst for production of polyester, process for production of the catalyst, and process for production of polyester using the catalyst |
WO2008122790A2 (en) * | 2007-04-05 | 2008-10-16 | University Of York | Heteropolyacid catalysts and biodiesel manufacturing methods using such catalysts |
US7767837B2 (en) * | 2007-05-04 | 2010-08-03 | Tda Research, Inc. | Methods of making alkyl esters |
US7943791B2 (en) * | 2007-09-28 | 2011-05-17 | Mcneff Research Consultants, Inc. | Methods and compositions for refining lipid feed stocks |
EP2303827B1 (de) | 2008-06-25 | 2019-10-16 | Benefuel Inc. | Verfahren zur herstellung von fettsäurealkylestern |
JP5470382B2 (ja) | 2008-06-25 | 2014-04-16 | ベネヒューエル・インコーポレーテッド | 脂肪酸アルキルエステルの製法 |
WO2010020998A2 (en) * | 2008-07-30 | 2010-02-25 | Indian Oil Corporation Limited | A catalyst composition for transesterification of organically/naturally derived oils and fats to produce alkyl esters and process for preparing the same |
CN102015808B (zh) * | 2008-09-26 | 2012-12-12 | Dic株式会社 | 氨基甲酸酯化反应催化剂以及氨基甲酸酯化物的制造方法 |
US8361174B2 (en) | 2008-10-07 | 2013-01-29 | Sartec Corporation | Catalysts, systems, and methods for producing fuels and fuel additives from polyols |
US9102877B2 (en) * | 2008-11-12 | 2015-08-11 | Sartec Corporation | Systems and methods for producing fuels from biomass |
US8188305B2 (en) * | 2009-02-03 | 2012-05-29 | David Miller | Method of producing biodiesel with supercritical alcohol and apparatus for same |
SG178891A1 (en) * | 2009-09-04 | 2012-04-27 | Exxonmobil Res & Eng Co | Stable alkoxylated fatty acid alkyl esters from transesterification-alkoxylation of vegetable oils |
WO2011089253A1 (en) * | 2010-01-25 | 2011-07-28 | Albemarle Europe Sprl | Zirconium-based catalyst compositions and their use for biodiesel production |
MY163273A (en) | 2011-03-09 | 2017-08-30 | Benefuel Inc | Systems and methods for making bioproducts |
US9080480B2 (en) | 2011-07-01 | 2015-07-14 | Toyota Jidosha Kabushiki Kaisha | Exhaust purification system for internal combustion engine |
WO2013006968A1 (en) * | 2011-07-08 | 2013-01-17 | Nrg Biofuels Inc. | Catalysts and methods for the production of biodiesel |
GB201119871D0 (en) | 2011-11-17 | 2011-12-28 | Davy Process Techn Ltd | Process |
GB201218078D0 (en) | 2012-10-09 | 2012-11-21 | Davy Process Techn Ltd | Process |
US9328054B1 (en) | 2013-09-27 | 2016-05-03 | Travis Danner | Method of alcoholisis of fatty acids and fatty acid gyicerides |
JP5832678B1 (ja) * | 2015-02-25 | 2015-12-16 | 日本ケッチェン株式会社 | 脂肪酸アルキルエステル製造触媒、その製造方法及び当該触媒を用いた脂肪酸アルキルエステルの製造方法 |
MX2016004133A (es) * | 2016-03-31 | 2017-09-29 | Inst Mexicano Del Petróleo | Uso de catalizadores acidos heterogeneos a base de sales metalicas mxtas para producir biodiesel. |
US10239812B2 (en) | 2017-04-27 | 2019-03-26 | Sartec Corporation | Systems and methods for synthesis of phenolics and ketones |
US10696923B2 (en) | 2018-02-07 | 2020-06-30 | Sartec Corporation | Methods and apparatus for producing alkyl esters from lipid feed stocks, alcohol feedstocks, and acids |
US10544381B2 (en) | 2018-02-07 | 2020-01-28 | Sartec Corporation | Methods and apparatus for producing alkyl esters from a reaction mixture containing acidified soap stock, alcohol feedstock, and acid |
CN110152647B (zh) * | 2018-02-12 | 2022-01-04 | 中国石油化工股份有限公司 | 一种催化剂及其制备方法和应用 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH06313188A (ja) * | 1993-04-28 | 1994-11-08 | Kao Corp | 脂肪酸エステルの製造方法 |
JPH07197047A (ja) | 1993-12-30 | 1995-08-01 | Someya Shoten:Kk | ディーゼル燃料およびその製造方法 |
US6376701B1 (en) * | 1995-12-29 | 2002-04-23 | Council Of Scientific & Industrial Research | Process for the transesterification of keto esters using solid acids as catalysts |
JP3028282B2 (ja) | 1996-02-28 | 2000-04-04 | 有限会社染谷商店 | 廃食用油を原資源として精製する重油バーナー用燃料および廃食用油を原資源としての再利用方法 |
GB2332155B (en) | 1997-12-12 | 2001-09-12 | Sec Dep Of Science And Technol | Highly acidic mesoporous synergystic solid catalyst and its applications |
JP3837950B2 (ja) | 1998-09-09 | 2006-10-25 | 住友化学株式会社 | 脂肪酸エステルの製造方法および脂肪酸エステルを含む燃料 |
EP1409622A1 (de) * | 2000-05-15 | 2004-04-21 | Dragan Nimcevic | Umesterung von fetten |
-
2003
- 2003-12-01 WO PCT/JP2003/015323 patent/WO2004085583A1/ja active Application Filing
- 2003-12-01 AU AU2003304018A patent/AU2003304018A1/en not_active Abandoned
-
2004
- 2004-03-19 JP JP2005504022A patent/JP4994664B2/ja not_active Expired - Fee Related
- 2004-03-19 EP EP04722015A patent/EP1607467B1/de not_active Expired - Lifetime
- 2004-03-19 DE DE602004013436T patent/DE602004013436T2/de not_active Expired - Lifetime
- 2004-03-19 WO PCT/JP2004/003731 patent/WO2004085584A1/ja active IP Right Grant
- 2004-03-19 US US10/544,822 patent/US7211681B2/en not_active Expired - Fee Related
- 2004-03-19 AT AT04722015T patent/ATE393808T1/de not_active IP Right Cessation
- 2004-03-25 MY MYPI20041066A patent/MY140824A/en unknown
Also Published As
Publication number | Publication date |
---|---|
WO2004085584A1 (ja) | 2004-10-07 |
MY140824A (en) | 2010-01-29 |
US7211681B2 (en) | 2007-05-01 |
DE602004013436T2 (de) | 2009-06-04 |
JPWO2004085584A1 (ja) | 2006-06-29 |
AU2003304018A1 (en) | 2004-10-18 |
EP1607467A4 (de) | 2006-05-17 |
EP1607467A1 (de) | 2005-12-21 |
WO2004085583A1 (ja) | 2004-10-07 |
EP1607467B1 (de) | 2008-04-30 |
JP4994664B2 (ja) | 2012-08-08 |
US20060149087A1 (en) | 2006-07-06 |
ATE393808T1 (de) | 2008-05-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition |