DE60039923D1 - Herstellungsverfahren für Feuerfestpulver mit niedrigen Sauerstoffgehalt zur Verwendung in der Pulvermetallurgie - Google Patents

Herstellungsverfahren für Feuerfestpulver mit niedrigen Sauerstoffgehalt zur Verwendung in der Pulvermetallurgie

Info

Publication number
DE60039923D1
DE60039923D1 DE60039923T DE60039923T DE60039923D1 DE 60039923 D1 DE60039923 D1 DE 60039923D1 DE 60039923 T DE60039923 T DE 60039923T DE 60039923 T DE60039923 T DE 60039923T DE 60039923 D1 DE60039923 D1 DE 60039923D1
Authority
DE
Germany
Prior art keywords
powder
production process
low oxygen
metal
target level
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60039923T
Other languages
English (en)
Inventor
Prabhat Kumar
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Materion Newton Inc
Original Assignee
HC Starck Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=23487672&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE60039923(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by HC Starck Inc filed Critical HC Starck Inc
Application granted granted Critical
Publication of DE60039923D1 publication Critical patent/DE60039923D1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
    • H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
    • H01G9/004—Details
    • H01G9/04—Electrodes or formation of dielectric layers thereon
    • H01G9/042—Electrodes or formation of dielectric layers thereon characterised by the material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/30—Making metallic powder or suspensions thereof using chemical processes with decomposition of metal compounds, e.g. by pyrolysis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/14—Treatment of metallic powder
    • B22F1/145—Chemical treatment, e.g. passivation or decarburisation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/12—Both compacting and sintering
    • B22F3/16—Both compacting and sintering in successive or repeated steps
    • B22F3/162—Machining, working after consolidation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/02—Making metallic powder or suspensions thereof using physical processes
    • B22F9/023—Hydrogen absorption
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/20—Obtaining niobium, tantalum or vanadium
    • C22B34/24—Obtaining niobium or tantalum
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
    • C22B9/14—Refining in the solid state
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C1/00—Making non-ferrous alloys
    • C22C1/04—Making non-ferrous alloys by powder metallurgy
    • C22C1/045—Alloys based on refractory metals
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22C—ALLOYS
    • C22C32/00—Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ
    • C22C32/001—Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ with only oxides
    • C22C32/0015—Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ with only oxides with only single oxides as main non-metallic constituents
    • C22C32/0031—Matrix based on refractory metals, W, Mo, Nb, Hf, Ta, Zr, Ti, V or alloys thereof
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
    • H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
    • H01G9/004—Details
    • H01G9/04—Electrodes or formation of dielectric layers thereon
    • H01G9/048—Electrodes or formation of dielectric layers thereon characterised by their structure
    • H01G9/052—Sintered electrodes
    • H01G9/0525—Powder therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/20—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces by extruding
    • B22F2003/208—Warm or hot extruding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
    • B22F2998/10—Processes characterised by the sequence of their steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Organic Chemistry (AREA)
  • Power Engineering (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Powder Metallurgy (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Preventing Corrosion Or Incrustation Of Metals (AREA)
  • Inorganic Insulating Materials (AREA)
DE60039923T 1999-08-19 2000-08-18 Herstellungsverfahren für Feuerfestpulver mit niedrigen Sauerstoffgehalt zur Verwendung in der Pulvermetallurgie Expired - Lifetime DE60039923D1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US09/377,077 US6261337B1 (en) 1999-08-19 1999-08-19 Low oxygen refractory metal powder for powder metallurgy

Publications (1)

Publication Number Publication Date
DE60039923D1 true DE60039923D1 (de) 2008-09-25

Family

ID=23487672

Family Applications (2)

Application Number Title Priority Date Filing Date
DE60021579T Expired - Lifetime DE60021579T2 (de) 1999-08-19 2000-08-18 Verfahren zur herstellung von feuerfestpulver mit niedrigen sauerstoffgehalt zur verwendung in der pulvermetallurgie
DE60039923T Expired - Lifetime DE60039923D1 (de) 1999-08-19 2000-08-18 Herstellungsverfahren für Feuerfestpulver mit niedrigen Sauerstoffgehalt zur Verwendung in der Pulvermetallurgie

Family Applications Before (1)

Application Number Title Priority Date Filing Date
DE60021579T Expired - Lifetime DE60021579T2 (de) 1999-08-19 2000-08-18 Verfahren zur herstellung von feuerfestpulver mit niedrigen sauerstoffgehalt zur verwendung in der pulvermetallurgie

Country Status (18)

Country Link
US (1) US6261337B1 (de)
EP (3) EP1200218B1 (de)
KR (2) KR100436108B1 (de)
CN (1) CN1272125C (de)
AT (2) ATE300377T1 (de)
AU (1) AU766574B2 (de)
BR (1) BR0007018A (de)
CA (1) CA2346957A1 (de)
CY (1) CY1108564T1 (de)
CZ (1) CZ20011740A3 (de)
DE (2) DE60021579T2 (de)
DK (1) DK1541261T3 (de)
EA (1) EA002736B1 (de)
ES (1) ES2313136T3 (de)
HK (1) HK1040501B (de)
IL (1) IL142601A (de)
PT (2) PT1541261E (de)
WO (1) WO2001012364A1 (de)

Families Citing this family (39)

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US6521173B2 (en) * 1999-08-19 2003-02-18 H.C. Starck, Inc. Low oxygen refractory metal powder for powder metallurgy
IL132291A0 (en) * 1999-10-08 2001-03-19 Advanced Alloys Technologies L A method for production of tantalum powder with highly developed surface
US6358625B1 (en) * 1999-10-11 2002-03-19 H. C. Starck, Inc. Refractory metals with improved adhesion strength
RU2246376C2 (ru) 2000-03-01 2005-02-20 Кабот Корпорейшн Азотированные вентильные металлы и способы их получения
AU1851002A (en) * 2000-11-30 2002-06-11 Showa Denko Kk Powder for capacitor, sintered body thereof and capacitor using the sintered body
US20030002043A1 (en) * 2001-04-10 2003-01-02 Kla-Tencor Corporation Periodic patterns and technique to control misalignment
AU2002307722B2 (en) 2001-05-15 2007-10-18 Showa Denko K.K. Niobium powder, niobium sintered body and capacitor using the sintered body
AU2008200187B2 (en) * 2001-05-15 2010-02-18 Showa Denko K.K. Niobium powder, niobium sintered body and capacitor using the sintered body
US6780218B2 (en) * 2001-06-20 2004-08-24 Showa Denko Kabushiki Kaisha Production process for niobium powder
US7081148B2 (en) * 2001-09-18 2006-07-25 Praxair S.T. Technology, Inc. Textured-grain-powder metallurgy tantalum sputter target
US6770154B2 (en) 2001-09-18 2004-08-03 Praxair S.T. Technology, Inc. Textured-grain-powder metallurgy tantalum sputter target
MXPA04007104A (es) * 2002-01-23 2004-10-29 Starck H C Inc Productos laminados de pulvimetalurgia de metal refractario de tamano de grano estabilizado.
WO2004003949A1 (en) * 2002-01-24 2004-01-08 H.C. Starck Inc. Capacitor-grade lead wires with increased tensile strength and hardness
TWI341337B (en) * 2003-01-07 2011-05-01 Cabot Corp Powder metallurgy sputtering targets and methods of producing same
US20060162822A1 (en) * 2003-01-21 2006-07-27 Richard Malen Capacitor-grade lead wires with increased tensile strength and hardness
DE10304756B4 (de) * 2003-02-05 2005-04-07 W.C. Heraeus Gmbh Sauerstoffangereicherter Niob-Draht
CN1541792B (zh) * 2003-03-28 2012-05-09 三菱综合材料株式会社 不重磨刀片的制造方法以及压粉体的排列装置
US7135141B2 (en) * 2003-03-31 2006-11-14 Hitachi Metals, Ltd. Method of manufacturing a sintered body
US20050279630A1 (en) * 2004-06-16 2005-12-22 Dynamic Machine Works, Inc. Tubular sputtering targets and methods of flowforming the same
AU2006243448B2 (en) * 2005-05-05 2011-09-01 H.C. Starck Inc. Coating process for manufacture or reprocessing of sputter targets and X-ray anodes
MX2007013600A (es) 2005-05-05 2008-01-24 Starck H C Gmbh Metodo para revestir una superficie de bustrato y producto revestido.
US20080078268A1 (en) * 2006-10-03 2008-04-03 H.C. Starck Inc. Process for preparing metal powders having low oxygen content, powders so-produced and uses thereof
CN101730757B (zh) * 2006-11-07 2015-09-30 H.C.施塔克有限公司 涂覆基材表面的方法和经过涂覆的产品
US20080145688A1 (en) 2006-12-13 2008-06-19 H.C. Starck Inc. Method of joining tantalum clade steel structures
US8197894B2 (en) 2007-05-04 2012-06-12 H.C. Starck Gmbh Methods of forming sputtering targets
CN101808770A (zh) * 2007-10-15 2010-08-18 高温特殊金属公司 利用回收的废料作为源材料制备钽粉末的方法
US8246903B2 (en) 2008-09-09 2012-08-21 H.C. Starck Inc. Dynamic dehydriding of refractory metal powders
US8043655B2 (en) * 2008-10-06 2011-10-25 H.C. Starck, Inc. Low-energy method of manufacturing bulk metallic structures with submicron grain sizes
CN102189261A (zh) * 2011-05-30 2011-09-21 华中科技大学 一种多孔制件的致密化方法
US9108273B2 (en) 2011-09-29 2015-08-18 H.C. Starck Inc. Methods of manufacturing large-area sputtering targets using interlocking joints
CN102672181A (zh) * 2012-06-07 2012-09-19 太仓市锦立得粉末冶金有限公司 一种粉末冶金制品的生产工艺
EP3112059B1 (de) 2014-02-27 2020-01-15 Ningxia Orient Tantalum Industry Co., Ltd. Herstellung von hochreinem tantalpulver
CN103920880A (zh) * 2014-03-11 2014-07-16 宁夏东方钽业股份有限公司 钽及钽合金棒材的制备方法
EP3129176B1 (de) * 2014-04-11 2024-10-09 Materion Newton Inc. Hochreine refraktärmetallsputter-targets mit gleichmässigem zufallsgefüge hergestellt durch heissisostatisches verpressen von hochreinen refraktärmetallpulvern
KR101488703B1 (ko) * 2014-10-29 2015-02-04 국방과학연구소 탄탈륨 분말 소결체 라이너 및 그 제조방법
TWI692382B (zh) 2016-01-27 2020-05-01 史達克公司 高熵合金絲及多主元合金絲，及其預形成物、製造方法和應用
US10730089B2 (en) 2016-03-03 2020-08-04 H.C. Starck Inc. Fabrication of metallic parts by additive manufacturing
CN111940745B (zh) * 2019-12-30 2024-01-19 宁夏东方钽业股份有限公司 大松装冶金级钽粉的制造方法
CN111560531B (zh) * 2020-04-15 2021-07-09 河南中钻新材料有限公司 一种低氧化物夹杂高性能粉末冶金镍基高温合金的制备方法

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US4722756A (en) * 1987-02-27 1988-02-02 Cabot Corp Method for deoxidizing tantalum material
US5242481A (en) * 1989-06-26 1993-09-07 Cabot Corporation Method of making powders and products of tantalum and niobium
US5082491A (en) * 1989-09-28 1992-01-21 V Tech Corporation Tantalum powder with improved capacitor anode processing characteristics
DE69128692T2 (de) * 1990-11-09 1998-06-18 Toyoda Chuo Kenkyusho Kk Titanlegierung aus Sinterpulver und Verfahren zu deren Herstellung
US5954856A (en) * 1996-04-25 1999-09-21 Cabot Corporation Method of making tantalum metal powder with controlled size distribution and products made therefrom

Also Published As

Publication number Publication date
ATE404308T1 (de) 2008-08-15
KR20030087087A (ko) 2003-11-12
DE60021579T2 (de) 2006-05-24
HK1040501A1 (en) 2002-06-14
AU766574B2 (en) 2003-10-16
WO2001012364A1 (en) 2001-02-22
PT1541261E (pt) 2008-11-12
CY1108564T1 (el) 2014-04-09
CA2346957A1 (en) 2001-02-22
CN1322157A (zh) 2001-11-14
EP1200218A4 (de) 2004-04-14
AU7063600A (en) 2001-03-13
EP1995005B1 (de) 2015-02-25
DK1541261T3 (da) 2008-12-01
KR100436108B1 (ko) 2004-06-14
HK1040501B (zh) 2007-04-20
ATE300377T1 (de) 2005-08-15
BR0007018A (pt) 2001-07-03
EP1200218B1 (de) 2005-07-27
EA002736B1 (ru) 2002-08-29
CZ20011740A3 (cs) 2002-02-13
EA200100441A1 (ru) 2001-10-22
EP1200218A1 (de) 2002-05-02
EP1995005A1 (de) 2008-11-26
EP1541261B1 (de) 2008-08-13
EP1541261A1 (de) 2005-06-15
PT1200218E (pt) 2005-11-30
DE60021579D1 (de) 2005-09-01
IL142601A (en) 2006-10-05
KR100431095B1 (ko) 2004-05-12
CN1272125C (zh) 2006-08-30
US6261337B1 (en) 2001-07-17
ES2313136T3 (es) 2009-03-01
KR20010099702A (ko) 2001-11-09

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