DE2938115A1 - Verfahren zur herstellung von alkylenglykolen - Google Patents

Verfahren zur herstellung von alkylenglykolen

Info

Publication number
DE2938115A1
DE2938115A1 DE19792938115 DE2938115A DE2938115A1 DE 2938115 A1 DE2938115 A1 DE 2938115A1 DE 19792938115 DE19792938115 DE 19792938115 DE 2938115 A DE2938115 A DE 2938115A DE 2938115 A1 DE2938115 A1 DE 2938115A1
Authority
DE
Germany
Prior art keywords
reaction
catalyst
alkylene oxide
amount
glycol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
DE19792938115
Other languages
German (de)
English (en)
Other versions
DE2938115C2 (fr
Inventor
Toshihiko Kumazawa
Hiroshi Odanaka
Takeshi Yamamoto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Shokubai Co Ltd
Original Assignee
Nippon Shokubai Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP8593579A external-priority patent/JPS5612323A/ja
Priority claimed from JP8751079A external-priority patent/JPS5612324A/ja
Priority claimed from JP9169579A external-priority patent/JPS5616431A/ja
Priority claimed from JP9321879A external-priority patent/JPS5618930A/ja
Priority claimed from JP9615579A external-priority patent/JPS5620529A/ja
Priority claimed from JP9737779A external-priority patent/JPS5622738A/ja
Priority claimed from JP9947179A external-priority patent/JPS5625125A/ja
Application filed by Nippon Shokubai Co Ltd filed Critical Nippon Shokubai Co Ltd
Publication of DE2938115A1 publication Critical patent/DE2938115A1/de
Application granted granted Critical
Publication of DE2938115C2 publication Critical patent/DE2938115C2/de
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
    • C07C29/10—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
    • C07C29/103—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers
    • C07C29/106—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers of oxiranes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
DE19792938115 1979-07-09 1979-09-20 Verfahren zur herstellung von alkylenglykolen Granted DE2938115A1 (de)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
JP8593579A JPS5612323A (en) 1979-07-09 1979-07-09 Preparation of ethylene glycol
JP8751079A JPS5612324A (en) 1979-07-12 1979-07-12 Preparation of ethylene glycol
JP9169579A JPS5616431A (en) 1979-07-20 1979-07-20 Preparation of alkylene glycol
JP9321879A JPS5618930A (en) 1979-07-24 1979-07-24 Production of alkylene glycol
JP9615579A JPS5620529A (en) 1979-07-30 1979-07-30 Preparation of alkylene glycol
JP9737779A JPS5622738A (en) 1979-08-01 1979-08-01 Preparation of alkylene glycol
JP9947179A JPS5625125A (en) 1979-08-06 1979-08-06 Preparation of alkylene glycol

Publications (2)

Publication Number Publication Date
DE2938115A1 true DE2938115A1 (de) 1981-01-29
DE2938115C2 DE2938115C2 (fr) 1990-04-05

Family

ID=27565417

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19792938115 Granted DE2938115A1 (de) 1979-07-09 1979-09-20 Verfahren zur herstellung von alkylenglykolen

Country Status (7)

Country Link
US (1) US4277632A (fr)
BE (1) BE878902A (fr)
CA (1) CA1120955A (fr)
DE (1) DE2938115A1 (fr)
FR (1) FR2460906A1 (fr)
GB (1) GB2053190B (fr)
NL (1) NL7907002A (fr)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4423005A (en) * 1981-09-25 1983-12-27 Baxter Travenol Laboratories, Inc. Determining quantitative degree of ethylene oxide exposure in sterilization processes
US4551566A (en) * 1982-09-30 1985-11-05 Union Carbide Corporation Process for the production of alkylene glycols
US4667045A (en) * 1984-03-28 1987-05-19 Union Carbide Corporation Organosalts of metalate anions and process for the production of alkylene glycols therewith
CA1248143A (fr) * 1984-03-28 1989-01-03 Brian T. Keen Production continue d'alkylene glycol en presence d'un organometallate
US4578524A (en) * 1984-03-28 1986-03-25 Union Carbide Corporation Carbon dioxide-enhanced monoalkylene glycol production
AU580300B2 (en) * 1984-03-28 1989-01-12 Union Carbide Corporation Alcoholates of metalate anions and glycols produced from them
US4560813A (en) * 1984-03-28 1985-12-24 Union Carbide Corporation Processes for the production of alkylene glycol in the presence of organometalate
US4579982A (en) * 1984-03-28 1986-04-01 Union Carbide Corporation Preparation of monoalkylene glycols using two liquid phase reaction menstruum
US4579983A (en) * 1984-03-28 1986-04-01 Union Carbide Corporation Process for the hydrolysis of alkylene oxides using organometalates
US4982021A (en) * 1984-03-28 1991-01-01 Union Carbide Chemicals And Plastics Company Inc. Process for the production of alkylene glycols with metalate-containing solid
US4571440A (en) * 1984-03-28 1986-02-18 Union Carbide Corporation Continuous process for the production of alkylene glycol in the presence of organometalate
CA1314566C (fr) * 1984-03-28 1993-03-16 John Howard Robson Methode de preparation d'alkyleneglycols a l'aide d'une substance solide renfermant un metallate
DE3683264D1 (de) * 1985-11-18 1992-02-13 Mitsui Toatsu Chemicals Verfahren zur herstellung von ethylenglykol und/oder propylenglykol.
US4760200A (en) * 1985-12-31 1988-07-26 Union Carbide Corporation Process for the production of alkylene glycols
EP0318099A3 (fr) * 1987-11-25 1989-11-15 Union Carbide Corporation Production du monoalkylène glycol en utilisant des compositions de réseau de métaux mixtes
US5349110A (en) * 1990-08-20 1994-09-20 Texaco Chemical Company Synthesis of low molecular weight glycol ethers from oxiranes plus olefins
US5250743A (en) * 1992-12-31 1993-10-05 Eastman Kodak Company Method of intercoversion of enantiomers of acyclic 1,2-dihydroxy-3-alkenes
US6211419B1 (en) * 2000-04-24 2001-04-03 The Dow Chemical Company Process for the preparation of alkylene glycols
CN1305820C (zh) * 2003-09-23 2007-03-21 中国石化集团天津石油化工公司 环氧化合物催化水合生产二元醇的工艺方法
ATE420721T1 (de) * 2004-08-05 2009-01-15 Saudi Basic Ind Corp Verfahren mit einem mit katalysator beschichteten wärmetauscher
US8304584B2 (en) * 2007-06-27 2012-11-06 H R D Corporation Method of making alkylene glycols
US7491856B2 (en) 2007-06-27 2009-02-17 H R D Corporation Method of making alkylene glycols
EA019753B1 (ru) * 2008-07-03 2014-06-30 ЭйчАДи КОПЭРЕЙШН Реактор, устройство и способ проведения гетерогенного катализа
CA2742498C (fr) * 2008-11-10 2018-02-27 Dow Technology Investments Llc Procede de production de glycols faiblement colores
DE102009038398A1 (de) 2009-08-24 2011-03-03 Uhde Gmbh Verfahren und Vorrichtung zur Herstellung von Alkylenoxiden und von Alkylenglykolen
CN114716299A (zh) * 2022-05-10 2022-07-08 岳阳昌德新材料有限公司 丙二醇/二丙二醇/三丙二醇的制备方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2807651A (en) * 1956-03-23 1957-09-24 Dow Chemical Co Method of preparing glycols and monoethers of glycols
US2833787A (en) * 1955-03-15 1958-05-06 Shell Dev Epoxidation process using hydrogen peroxide and an acid salt of a heavy metal peracid
US4160116A (en) * 1978-08-28 1979-07-03 Showa Denko K.K. Process for the production of alkylene glycols

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR816690A (fr) * 1936-01-24 1937-08-13 Distillers Co Yeast Ltd Perfectionnements à la fabrication de dérivés du glycol
GB654764A (en) * 1948-02-05 1951-06-27 Distillers Co Yeast Ltd Hydroxylation of olefinic compounds
US2623909A (en) * 1950-07-12 1952-12-30 Celanese Corp Hydrolysis of 1, 2-propylene oxide to 1, 2-propylene glycol
FR1079226A (fr) * 1952-04-28 1954-11-26 Bataafsche Petroleum Procédé de préparation de composés organiques polyhydroxy
US3629343A (en) * 1968-10-11 1971-12-21 Vnii Neftekhim Protsessov Process for the production of alkylene glycols
FR2105292A5 (fr) * 1969-11-26 1972-04-28 Raffinage Cie Francaise
DE2141470A1 (de) * 1971-08-19 1973-02-22 Erdoelchemie Gmbh Verfahren zur herstellung von aethylenglykol
DE2256907C3 (de) * 1972-11-20 1982-03-18 Henkel KGaA, 4000 Düsseldorf Verfahren zur Herstellung von vicinalen Di- und Polyolen
IT971363B (it) * 1972-11-30 1974-04-30 Sir Soc Italiana Resine Spa Procedimento per la preparazione del glicole etilenico
SU558898A1 (ru) * 1973-07-16 1977-05-25 Предприятие П/Я В-8585 Способ получени -гликолей
US4014945A (en) * 1975-08-28 1977-03-29 Standard Oil Company Process for the preparation of ethylene glycol
JPS6045610B2 (ja) * 1978-03-20 1985-10-11 株式会社日本触媒 エチレングリコ−ルの製造方法
JPS6045611B2 (ja) * 1978-03-24 1985-10-11 株式会社日本触媒 エチレングリコ−ルの製造方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2833787A (en) * 1955-03-15 1958-05-06 Shell Dev Epoxidation process using hydrogen peroxide and an acid salt of a heavy metal peracid
US2807651A (en) * 1956-03-23 1957-09-24 Dow Chemical Co Method of preparing glycols and monoethers of glycols
US4160116A (en) * 1978-08-28 1979-07-03 Showa Denko K.K. Process for the production of alkylene glycols

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Chem.Abstr., 87, 1977, 101929 *

Also Published As

Publication number Publication date
BE878902A (fr) 1980-01-16
NL7907002A (nl) 1981-01-13
CA1120955A (fr) 1982-03-30
FR2460906A1 (fr) 1981-01-30
DE2938115C2 (fr) 1990-04-05
GB2053190A (en) 1981-02-04
FR2460906B1 (fr) 1984-05-18
US4277632A (en) 1981-07-07
GB2053190B (en) 1983-09-21

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Legal Events

Date Code Title Description
8110 Request for examination paragraph 44
D2 Grant after examination
8364 No opposition during term of opposition
8330 Complete disclaimer