DE2807816A1 - Extraktionsverfahren - Google Patents

Extraktionsverfahren

Info

Publication number
DE2807816A1
DE2807816A1 DE19782807816 DE2807816A DE2807816A1 DE 2807816 A1 DE2807816 A1 DE 2807816A1 DE 19782807816 DE19782807816 DE 19782807816 DE 2807816 A DE2807816 A DE 2807816A DE 2807816 A1 DE2807816 A1 DE 2807816A1
Authority
DE
Germany
Prior art keywords
pentenenitrile
hydrocyanation
line
nitriles
stream
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
DE19782807816
Other languages
German (de)
English (en)
Other versions
DE2807816C2 (en, 2012
Inventor
John William Corn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of DE2807816A1 publication Critical patent/DE2807816A1/de
Application granted granted Critical
Publication of DE2807816C2 publication Critical patent/DE2807816C2/de
Granted legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/12—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides
    • B01J31/14—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides of aluminium or boron
    • B01J31/146—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides of aluminium or boron of boron
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B01J31/1845—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
    • B01J31/185—Phosphites ((RO)3P), their isomeric phosphonates (R(RO)2P=O) and RO-substitution derivatives thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/40—Regeneration or reactivation
    • B01J31/4015—Regeneration or reactivation of catalysts containing metals
    • B01J31/4023—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper
    • B01J31/403—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper containing iron group metals or copper
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
    • B01J2231/34—Other additions, e.g. Monsanto-type carbonylations, addition to 1,2-C=X or 1,2-C-X triplebonds, additions to 1,4-C=C-C=X or 1,4-C=-C-X triple bonds with X, e.g. O, S, NH/N
    • B01J2231/341—1,2-additions, e.g. aldol or Knoevenagel condensations
    • B01J2231/342—Aldol type reactions, i.e. nucleophilic addition of C-H acidic compounds, their R3Si- or metal complex analogues, to aldehydes or ketones
    • B01J2231/343—Aldol type reactions, i.e. nucleophilic addition of C-H acidic compounds, their R3Si- or metal complex analogues, to aldehydes or ketones to prepare cyanhydrines, e.g. by adding HCN or TMSCN
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/20—Complexes comprising metals of Group II (IIA or IIB) as the central metal
    • B01J2531/26—Zinc
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/84—Metals of the iron group
    • B01J2531/847—Nickel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/06—Halogens; Compounds thereof
    • B01J27/08—Halides
    • B01J27/10—Chlorides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24—Nitrogen compounds
    • B01J27/26—Cyanides
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
DE19782807816 1977-02-23 1978-02-23 Extraktionsverfahren Granted DE2807816A1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/771,065 US4080374A (en) 1977-02-23 1977-02-23 Product recovery

Publications (2)

Publication Number Publication Date
DE2807816A1 true DE2807816A1 (de) 1978-08-24
DE2807816C2 DE2807816C2 (en, 2012) 1989-01-12

Family

ID=25090587

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19782807816 Granted DE2807816A1 (de) 1977-02-23 1978-02-23 Extraktionsverfahren

Country Status (9)

Country Link
US (1) US4080374A (en, 2012)
JP (1) JPS53105424A (en, 2012)
BE (1) BE864203A (en, 2012)
CA (1) CA1119195A (en, 2012)
DE (1) DE2807816A1 (en, 2012)
FR (1) FR2381749A1 (en, 2012)
GB (1) GB1560720A (en, 2012)
IT (1) IT1158653B (en, 2012)
NL (1) NL188800C (en, 2012)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3037336A1 (de) * 1979-10-02 1981-04-23 Aktiebolaget Bofors, 69180 Bofors Laufrohr-abdichtung

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4328172A (en) * 1981-02-24 1982-05-04 E. I. Du Pont De Nemours And Company Hydrocyanation of olefins
US4339395A (en) * 1981-04-15 1982-07-13 E. I. Du Pont De Nemours And Company Treatment of olefin hydrocyanation products
US4382038A (en) * 1981-10-01 1983-05-03 E. I. Du Pont De Nemours And Company Hydrocyanation of olefins
US4990645A (en) * 1990-06-27 1991-02-05 E. I. Du Pont De Nemours And Company Hydrocyanation process
FR2849027B1 (fr) * 2002-12-23 2005-01-21 Rhodia Polyamide Intermediates Procede de synthese de composes comprenant des fonctions nitriles a partir de composes a insaturations ethyleniques
FR2850966B1 (fr) 2003-02-10 2005-03-18 Rhodia Polyamide Intermediates Procede de fabrication de composes dinitriles
FR2854892B1 (fr) * 2003-05-12 2005-06-24 Rhodia Polyamide Intermediates Procede de fabrication de dinitriles
FR2854891B1 (fr) 2003-05-12 2006-07-07 Rhodia Polyamide Intermediates Procede de preparation de dinitriles
DE102004004683A1 (de) * 2004-01-29 2005-08-18 Basf Ag Verfahren zur Herstellung von Dinitrilen
FR2878848B1 (fr) * 2004-12-07 2007-01-05 Rhodia Chimie Sa Procede de fabrication de composes dinitriles
BRPI0709313A2 (pt) * 2006-03-17 2011-07-05 Invista Tech Sarl método de separação e método para a preparação de triorganofosfitos
US7709674B2 (en) * 2006-07-14 2010-05-04 Invista North America S.A R.L Hydrocyanation process with reduced yield losses
WO2008028843A1 (de) * 2006-09-04 2008-03-13 Basf Aktiengesellschaft Verfahren zur herstellung von dinitrilen
US9133226B2 (en) 2011-12-21 2015-09-15 Invista North America S.A.R.L. Extraction solvent control for reducing stable emulsions
CN103547349B (zh) 2011-12-21 2016-03-16 因温斯特北美公司 用于减少稳定乳液的萃取溶剂控制
US9133223B2 (en) 2011-12-21 2015-09-15 Invista North America S.A.R.L. Extraction solvent control for reducing stable emulsions
EP2928597B1 (en) 2012-12-07 2019-07-17 INVISTA Textiles (U.K.) Limited Improved process for producing pentenenitriles
JP2020112730A (ja) 2019-01-15 2020-07-27 キヤノン株式会社 表示装置及びその制御方法、プログラム、記憶媒体
CN111995547B (zh) 2020-01-19 2021-07-09 浙江新和成股份有限公司 己二腈的制备方法和装置

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2154501A1 (de) * 1970-11-03 1972-05-04 EI du Pont de Nemours and Co, Wilmington, Del (V St A ) Abtrennung organischer Phosphorverbin düngen und ihrer Metallkomplexe von organi sehen Dmitrilen

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3496215A (en) * 1965-11-23 1970-02-17 Du Pont Hydrocyanation of olefins using selected nickel phosphite catalysts
US3526654A (en) * 1968-05-17 1970-09-01 Du Pont Isomerization of 2-pentenenitrile to 3-pentenenitrile
US3538142A (en) * 1969-08-04 1970-11-03 Du Pont Process of isomerizing 3-pentenenitrile to 4-pentenenitrile
US3542847A (en) * 1969-09-15 1970-11-24 Du Pont Process for isomerizing 3-pentenenitrile to 4-pentenenitrile
BE760119A (fr) * 1969-12-17 1971-06-09 Montedison Spa Procede de preparation du pentene-3-nitrile
US3752839A (en) * 1970-07-02 1973-08-14 Du Pont Hydrocyanation olefins
US3676475A (en) * 1970-07-06 1972-07-11 Du Pont Hydrides of nickel coordination compounds
BE791339A (fr) * 1971-11-15 1973-05-14 Halcon International Inc Procédé de préparation de cyano-composés
US3773809A (en) * 1972-06-28 1973-11-20 Du Pont Separation of organic phosphorus compounds and their metal complexes from organic nitriles in the hydrocyanation of olefins
US3859327A (en) * 1972-10-25 1975-01-07 Du Pont Process for recovery of nickel from a deactivated hydrocyanation catalyst
US3818068A (en) * 1973-01-19 1974-06-18 Du Pont Removal of deactivated catalyst species from a hydrocyanation product fluid

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2154501A1 (de) * 1970-11-03 1972-05-04 EI du Pont de Nemours and Co, Wilmington, Del (V St A ) Abtrennung organischer Phosphorverbin düngen und ihrer Metallkomplexe von organi sehen Dmitrilen

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3037336A1 (de) * 1979-10-02 1981-04-23 Aktiebolaget Bofors, 69180 Bofors Laufrohr-abdichtung

Also Published As

Publication number Publication date
JPS53105424A (en) 1978-09-13
NL188800C (nl) 1992-10-01
US4080374A (en) 1978-03-21
IT7820534A0 (it) 1978-02-22
CA1119195A (en) 1982-03-02
NL7801975A (nl) 1978-08-25
NL188800B (nl) 1992-05-06
GB1560720A (en) 1980-02-06
JPS6141345B2 (en, 2012) 1986-09-13
DE2807816C2 (en, 2012) 1989-01-12
IT1158653B (it) 1987-02-25
FR2381749A1 (fr) 1978-09-22
BE864203A (fr) 1978-08-22
FR2381749B1 (en, 2012) 1984-07-06

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Legal Events

Date Code Title Description
8110 Request for examination paragraph 44
D2 Grant after examination
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee