DE2526851C3 - Verfahren zur Herstellung von Ketoisophoron - Google Patents

Verfahren zur Herstellung von Ketoisophoron

Info

Publication number
DE2526851C3
DE2526851C3 DE2526851A DE2526851A DE2526851C3 DE 2526851 C3 DE2526851 C3 DE 2526851C3 DE 2526851 A DE2526851 A DE 2526851A DE 2526851 A DE2526851 A DE 2526851A DE 2526851 C3 DE2526851 C3 DE 2526851C3
Authority
DE
Germany
Prior art keywords
catalyst
weight
ketoisophorone
isophorone
copper
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE2526851A
Other languages
German (de)
English (en)
Other versions
DE2526851A1 (de
DE2526851B2 (de
Inventor
Marcel Dr. East Brighton Vic. Seuret (Australien)
Erich Dr. Muenchenstein Widmer (Schweiz)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
F Hoffmann La Roche AG
Original Assignee
F Hoffmann La Roche AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by F Hoffmann La Roche AG filed Critical F Hoffmann La Roche AG
Publication of DE2526851A1 publication Critical patent/DE2526851A1/de
Publication of DE2526851B2 publication Critical patent/DE2526851B2/de
Application granted granted Critical
Publication of DE2526851C3 publication Critical patent/DE2526851C3/de
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/885—Molybdenum and copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/22—Organic complexes
    • B01J31/2204—Organic complexes the ligands containing oxygen or sulfur as complexing atoms
    • B01J31/2208—Oxygen, e.g. acetylacetonates
    • B01J31/2226—Anionic ligands, i.e. the overall ligand carries at least one formal negative charge
    • B01J31/223—At least two oxygen atoms present in one at least bidentate or bridging ligand
    • B01J31/2234—Beta-dicarbonyl ligands, e.g. acetylacetonates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • B01J31/28—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24 of the platinum group metals, iron group metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • B01J31/34—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24 of chromium, molybdenum or tungsten
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/70—Oxidation reactions, e.g. epoxidation, (di)hydroxylation, dehydrogenation and analogues
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/50—Complexes comprising metals of Group V (VA or VB) as the central metal
    • B01J2531/56—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/60—Complexes comprising metals of Group VI (VIA or VIB) as the central metal
    • B01J2531/64—Molybdenum

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE2526851A 1974-06-28 1975-06-16 Verfahren zur Herstellung von Ketoisophoron Expired DE2526851C3 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH892774A CH611590A5 (en) 1974-06-28 1974-06-28 Process for the preparation of a diketo compound

Publications (3)

Publication Number Publication Date
DE2526851A1 DE2526851A1 (de) 1976-01-08
DE2526851B2 DE2526851B2 (de) 1979-11-08
DE2526851C3 true DE2526851C3 (de) 1980-07-24

Family

ID=4346385

Family Applications (1)

Application Number Title Priority Date Filing Date
DE2526851A Expired DE2526851C3 (de) 1974-06-28 1975-06-16 Verfahren zur Herstellung von Ketoisophoron

Country Status (10)

Country Link
US (1) US3960966A (enExample)
JP (1) JPS5134129A (enExample)
AT (1) AT338232B (enExample)
BE (1) BE830723A (enExample)
CH (1) CH611590A5 (enExample)
DE (1) DE2526851C3 (enExample)
FR (1) FR2278667A1 (enExample)
GB (1) GB1448976A (enExample)
IT (1) IT1038795B (enExample)
NL (1) NL179723C (enExample)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH605535A5 (enExample) * 1974-04-11 1978-09-29 Hoffmann La Roche
FR2303785A1 (fr) * 1975-03-11 1976-10-08 Rhone Poulenc Ind Procede d'oxydation de cetones b-ethyleniques
FR2335487A1 (fr) * 1975-12-19 1977-07-15 Rhone Poulenc Ind Procede de preparation de trimethyl-3,5,5 cyclohexene-2 dione-1,4
JPS5912831U (ja) * 1982-07-19 1984-01-26 日本板硝子株式会社 焼付装置
DE3842547A1 (de) * 1988-12-17 1990-06-21 Huels Chemische Werke Ag Verfahren zur herstellung von 2,6,6-trimethyl-cyclohex-2-en-1,4-dion
US5545761A (en) * 1994-11-14 1996-08-13 Aristech Chemical Corporation Method of making ketoisophorone via oxidation of isophorone with tert-butyl hydroperoxide
JPH11342342A (ja) 1998-06-01 1999-12-14 Daicel Chem Ind Ltd 酸化触媒及びそれを用いた酸化方法
JP2000034255A (ja) 1998-07-16 2000-02-02 Daicel Chem Ind Ltd ケトイソホロンの製造方法および製造装置
JP2000247921A (ja) 1998-12-28 2000-09-12 Daicel Chem Ind Ltd ケトイソホロン誘導体の製造方法及び製造装置
ATE541941T1 (de) 1999-08-02 2012-02-15 Dsm Ip Assets Bv Mikrobielle herstellung von levodione
CN110721696B (zh) * 2019-10-01 2020-06-05 山东新和成维生素有限公司 一种采用钙钛矿型复合氧化物催化合成茶香酮的方法
CN111269949B (zh) * 2020-03-06 2022-01-07 万华化学集团股份有限公司 一种利用固定化漆酶催化制备4-氧代异佛尔酮的方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH559156A5 (enExample) * 1972-11-16 1975-02-28 Firmenich & Cie

Also Published As

Publication number Publication date
DE2526851A1 (de) 1976-01-08
AT338232B (de) 1977-08-10
JPS5134129A (en) 1976-03-23
FR2278667A1 (fr) 1976-02-13
US3960966A (en) 1976-06-01
IT1038795B (it) 1979-11-30
GB1448976A (en) 1976-09-08
DE2526851B2 (de) 1979-11-08
CH611590A5 (en) 1979-06-15
NL179723B (nl) 1986-06-02
NL7507153A (nl) 1975-12-30
FR2278667B1 (enExample) 1978-10-13
BE830723A (fr) 1975-12-29
ATA497475A (de) 1976-12-15
JPS5530696B2 (enExample) 1980-08-13
NL179723C (nl) 1986-11-03

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Legal Events

Date Code Title Description
C3 Grant after two publication steps (3rd publication)
8327 Change in the person/name/address of the patent owner

Owner name: F. HOFFMANN-LA ROCHE AG, BASEL, CH

8328 Change in the person/name/address of the agent

Free format text: LEDERER, F., DIPL.-CHEM. DR., 8000 MUENCHEN RIEDERER FRHR. VON PAAR ZU SCHOENAU, A., DIPL.-ING., PAT.-ANWAELTE, 8300 LANDSHUT

8339 Ceased/non-payment of the annual fee