DE2445156A1 - Verfahren zur gewinnung von fettsaeuren und/oder harzsaeuren - Google Patents
Verfahren zur gewinnung von fettsaeuren und/oder harzsaeurenInfo
- Publication number
- DE2445156A1 DE2445156A1 DE19742445156 DE2445156A DE2445156A1 DE 2445156 A1 DE2445156 A1 DE 2445156A1 DE 19742445156 DE19742445156 DE 19742445156 DE 2445156 A DE2445156 A DE 2445156A DE 2445156 A1 DE2445156 A1 DE 2445156A1
- Authority
- DE
- Germany
- Prior art keywords
- soaps
- melting point
- tall oil
- film evaporator
- acids
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000014113 dietary fatty acids Nutrition 0.000 title claims description 36
- 239000000194 fatty acid Substances 0.000 title claims description 36
- 229930195729 fatty acid Natural products 0.000 title claims description 36
- 150000004665 fatty acids Chemical class 0.000 title claims description 36
- 239000002253 acid Substances 0.000 title claims description 33
- 150000007513 acids Chemical class 0.000 title claims description 27
- 238000000034 method Methods 0.000 title claims description 21
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- 239000000463 material Substances 0.000 claims description 50
- 239000000344 soap Substances 0.000 claims description 47
- 239000010409 thin film Substances 0.000 claims description 23
- 239000011347 resin Substances 0.000 claims description 22
- 229920005989 resin Polymers 0.000 claims description 22
- 239000003784 tall oil Substances 0.000 claims description 20
- 230000008018 melting Effects 0.000 claims description 18
- 238000002844 melting Methods 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 238000007127 saponification reaction Methods 0.000 claims description 14
- 238000011282 treatment Methods 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 4
- 238000000605 extraction Methods 0.000 claims description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- 238000010438 heat treatment Methods 0.000 description 10
- 229930182558 Sterol Natural products 0.000 description 8
- 150000003432 sterols Chemical class 0.000 description 8
- 235000003702 sterols Nutrition 0.000 description 8
- 239000003921 oil Substances 0.000 description 7
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- 238000004821 distillation Methods 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 238000000354 decomposition reaction Methods 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- 150000003505 terpenes Chemical class 0.000 description 5
- 235000007586 terpenes Nutrition 0.000 description 5
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 4
- 239000003513 alkali Substances 0.000 description 4
- 238000001704 evaporation Methods 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 4
- 150000002148 esters Chemical class 0.000 description 3
- 238000011049 filling Methods 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 229940076810 beta sitosterol Drugs 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 229950005143 sitosterol Drugs 0.000 description 2
- 239000006200 vaporizer Substances 0.000 description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 description 1
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 1
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 1
- LGJMUZUPVCAVPU-UHFFFAOYSA-N beta-Sitostanol Natural products C1CC2CC(O)CCC2(C)C2C1C1CCC(C(C)CCC(CC)C(C)C)C1(C)CC2 LGJMUZUPVCAVPU-UHFFFAOYSA-N 0.000 description 1
- NJKOMDUNNDKEAI-UHFFFAOYSA-N beta-sitosterol Natural products CCC(CCC(C)C1CCC2(C)C3CC=C4CC(O)CCC4C3CCC12C)C(C)C NJKOMDUNNDKEAI-UHFFFAOYSA-N 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 235000020778 linoleic acid Nutrition 0.000 description 1
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 150000002888 oleic acid derivatives Chemical class 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- KZJWDPNRJALLNS-VJSFXXLFSA-N sitosterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CC[C@@H](CC)C(C)C)[C@@]1(C)CC2 KZJWDPNRJALLNS-VJSFXXLFSA-N 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 1
- 150000003648 triterpenes Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B13/00—Recovery of fats, fatty oils or fatty acids from waste materials
- C11B13/005—Recovery of fats, fatty oils or fatty acids from waste materials of residues of the fabrication of wood-cellulose (in particular tall-oil)
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10525873A JPS5512080B2 (enExample) | 1973-09-18 | 1973-09-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2445156A1 true DE2445156A1 (de) | 1975-04-03 |
Family
ID=14402615
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19742445156 Pending DE2445156A1 (de) | 1973-09-18 | 1974-09-18 | Verfahren zur gewinnung von fettsaeuren und/oder harzsaeuren |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3887537A (enExample) |
| JP (1) | JPS5512080B2 (enExample) |
| AT (1) | AT345950B (enExample) |
| CA (1) | CA1012964A (enExample) |
| DE (1) | DE2445156A1 (enExample) |
| GB (1) | GB1481567A (enExample) |
| NL (1) | NL155532B (enExample) |
| SE (1) | SE419639B (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2642414A1 (de) * | 1975-09-22 | 1977-04-07 | Japan Synthetic Rubber Co Ltd | Verfahren zur gewinnung von hochreinen fettsaeuren, harzsaeuren und sterinen |
Families Citing this family (34)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4060800A (en) * | 1971-04-21 | 1977-11-29 | Philip Stern | Fire alarm device |
| US4263103A (en) * | 1977-06-24 | 1981-04-21 | Henkel Corporation | Process for thermally stabilizing sterols by degassing and flash distilling |
| US4483791A (en) * | 1983-06-22 | 1984-11-20 | Sylvachem Corporation | Recovery of fatty acids from tall oil heads |
| JPS606810U (ja) * | 1983-06-27 | 1985-01-18 | 三菱電機株式会社 | 二次空気制御弁 |
| US5097012A (en) * | 1990-01-23 | 1992-03-17 | Clemson University | Solvent extraction of fatty acid stream with liquid water and elevated temperatures and pressures |
| CA2230373A1 (en) * | 1998-02-20 | 1999-08-20 | Forbes Medi-Tech Inc. | Method for the preparation of phytosterols from tall oil pitch |
| US20040024175A1 (en) * | 1998-02-10 | 2004-02-05 | Alfred Wong | Method for the preparation of phytosterols from tall oil pitch |
| US20050107582A1 (en) * | 2003-07-30 | 2005-05-19 | Alfred Wong | Method for the preparation of phytosterols from tall oil pitch |
| WO2000009535A1 (en) * | 1998-08-17 | 2000-02-24 | Westvaco Corporation | Isolation and purification of sterols from neutrals fraction of tall oil pitch by direct crystallization, single phase |
| WO2000012533A1 (en) * | 1998-08-27 | 2000-03-09 | Westvaco Corporation | Isolation and purification of sterols from neutrals fraction of tall oil pitch by direct crystallization, dual phase |
| US6107456A (en) * | 1998-08-31 | 2000-08-22 | Arizona Chemical Corporation | Method for separating sterols from tall oil |
| US6057462A (en) * | 1998-11-06 | 2000-05-02 | Westvaco Corporation | Isolation and purification of sterols from neutrals fraction of tall oil pitch by single decantation crystallization |
| AU4958599A (en) * | 1998-12-07 | 2000-06-26 | Westvaco Corporation | Isolation and purification of sterols from neutrals fraction of tall oil pitch by dual decantation crystallization |
| NZ515158A (en) * | 1999-04-27 | 2003-06-30 | Sterol Technologies Ltd | Process for the purification of sterols from hydrocarbon extracts using evaporative fractionation |
| EP1389622A3 (en) * | 1999-04-27 | 2004-12-15 | Sterol Technologies Ltd. | Process for the purification of sterols from hydrocarborn extracts using evaporative fractionation |
| US7371876B2 (en) * | 1999-04-27 | 2008-05-13 | Sterol Technologies Ltd. | Process for the purification of sterols from hydrocarbon extracts using evaporative fractionation |
| DE60020914T2 (de) * | 1999-09-03 | 2005-12-01 | Cabby Business Inc., Road Town | Effizientes Verfahren zur Herstellung sehr reiner Sterinen |
| US20090191243A9 (en) * | 2000-01-03 | 2009-07-30 | Hill John C | High unsaponifiables and methods of using the same and its derivatives and uses thereof |
| US7955611B2 (en) * | 2000-01-03 | 2011-06-07 | International Flora Technologies Ltd. | Binding and rinse-off of quaternary ammonium compounds for cosmetic and personal care applications |
| US6780831B2 (en) * | 2001-02-02 | 2004-08-24 | Raisio Benecol, Ltd. | Process for separating unsaponifiable valuable substances from sulphate soap based materials |
| DE60133460D1 (de) * | 2001-09-07 | 2008-05-15 | Raisio Staest Oy | Verfahren zur Isolierung von Sterinen und/oder Wachsalkoholen aus Talölprodukten |
| DE60332053D1 (de) * | 2003-02-21 | 2010-05-20 | Cognis Ip Man Gmbh | Verfahren zur gewinnung von fettsäurealkylestern, harzsäuren und sterinen aus rohtallöl |
| EP1586624B1 (en) | 2004-02-06 | 2013-04-03 | Härting Glade, Thomas Francis | Process of refinement of crude tall oil using short path distillation |
| FI20070137A0 (fi) * | 2007-02-15 | 2007-02-15 | Raisio Benecol Oy | Menetelmä rasvahappojen, hartsihappojen ja sterolien eristämiseksi mäntyöljypiestä |
| FI20080174A0 (fi) | 2008-02-29 | 2008-02-29 | Raisio Nutrition Ltd | Menetelmä sterolien ja happojen erottamiseksi mäntyöljypiestä |
| US9221869B2 (en) * | 2008-03-10 | 2015-12-29 | Sunpine Ab | Recovery of phytosterols from residual vegetable oil streams |
| SI2635592T2 (sl) | 2010-11-03 | 2025-09-30 | Verbio Se | Postopek za pridobivanje fitosterolov in/ali tokoferolov iz ostankov destilacije estrov rastlinskih olj, prednostno iz destilacijskih ostankov iz transesterifikacije rastlinskih olj |
| FI20106252A0 (fi) | 2010-11-26 | 2010-11-26 | Upm Kymmene Corp | Menetelmä ja systeemi polttoainekomponenttien valmistamiseksi |
| FI124101B (en) * | 2012-05-14 | 2014-03-14 | Hankkija Maatalous Oy | Modified tall oil fatty acid |
| FI124918B (fi) | 2013-05-14 | 2015-03-31 | Hankkija Maatalous Oy | Mäntyöljyrasvahappo |
| FI125051B (fi) | 2013-10-24 | 2015-05-15 | Hankkija Oy | Mäntyöljyrasvahappo |
| HUE050907T2 (hu) | 2013-11-13 | 2021-01-28 | Hankkija Oy | Gyantasavakat tartalmazó takarmány-kiegészítõ |
| BR102015031936B1 (pt) * | 2015-12-18 | 2023-04-11 | Universidade Estadual De Campinas - Unicamp | Sistema e processo integrado de purificação do limoneno |
| CN105647385B (zh) * | 2016-02-03 | 2021-03-23 | 广西金秀松源林产有限公司 | 一种松脂废渣高效翻炒、蒸馏回收系统 |
-
1973
- 1973-09-18 JP JP10525873A patent/JPS5512080B2/ja not_active Expired
-
1974
- 1974-09-06 US US50387374 patent/US3887537A/en not_active Expired - Lifetime
- 1974-09-09 SE SE7411364A patent/SE419639B/xx unknown
- 1974-09-11 CA CA208,991A patent/CA1012964A/en not_active Expired
- 1974-09-12 GB GB3977774A patent/GB1481567A/en not_active Expired
- 1974-09-16 AT AT745874A patent/AT345950B/de not_active IP Right Cessation
- 1974-09-18 NL NL7412370A patent/NL155532B/xx not_active IP Right Cessation
- 1974-09-18 DE DE19742445156 patent/DE2445156A1/de active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2642414A1 (de) * | 1975-09-22 | 1977-04-07 | Japan Synthetic Rubber Co Ltd | Verfahren zur gewinnung von hochreinen fettsaeuren, harzsaeuren und sterinen |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5055602A (enExample) | 1975-05-15 |
| NL155532B (nl) | 1978-01-16 |
| SE7411364L (enExample) | 1975-03-19 |
| NL7412370A (nl) | 1975-03-20 |
| AT345950B (de) | 1978-10-10 |
| CA1012964A (en) | 1977-06-28 |
| US3887537A (en) | 1975-06-03 |
| GB1481567A (en) | 1977-08-03 |
| ATA745874A (de) | 1978-02-15 |
| JPS5512080B2 (enExample) | 1980-03-29 |
| SE419639B (sv) | 1981-08-17 |
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