DE2441014C3 - Verfahren zur Herstellung von Natriumpercarbonat durch Zerstäubung - Google Patents
Verfahren zur Herstellung von Natriumpercarbonat durch ZerstäubungInfo
- Publication number
- DE2441014C3 DE2441014C3 DE2441014A DE2441014A DE2441014C3 DE 2441014 C3 DE2441014 C3 DE 2441014C3 DE 2441014 A DE2441014 A DE 2441014A DE 2441014 A DE2441014 A DE 2441014A DE 2441014 C3 DE2441014 C3 DE 2441014C3
- Authority
- DE
- Germany
- Prior art keywords
- sodium percarbonate
- hydrogen peroxide
- atomization
- active oxygen
- fluidized bed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- VTIIJXUACCWYHX-UHFFFAOYSA-L disodium;carboxylatooxy carbonate Chemical compound [Na+].[Na+].[O-]C(=O)OOC([O-])=O VTIIJXUACCWYHX-UHFFFAOYSA-L 0.000 title claims description 17
- 229940045872 sodium percarbonate Drugs 0.000 title claims description 17
- 238000000034 method Methods 0.000 title claims description 15
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 238000000889 atomisation Methods 0.000 title description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 31
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 24
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 12
- 239000001569 carbon dioxide Substances 0.000 claims description 6
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 6
- 239000007921 spray Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 239000007789 gas Substances 0.000 claims description 5
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 150000002484 inorganic compounds Chemical class 0.000 claims 1
- 229910010272 inorganic material Inorganic materials 0.000 claims 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 13
- 239000001301 oxygen Substances 0.000 description 13
- 229910052760 oxygen Inorganic materials 0.000 description 13
- 235000011121 sodium hydroxide Nutrition 0.000 description 10
- 239000000243 solution Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical class [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 4
- 239000003599 detergent Substances 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000003513 alkali Substances 0.000 description 3
- MWNQXXOSWHCCOZ-UHFFFAOYSA-L sodium;oxido carbonate Chemical compound [Na+].[O-]OC([O-])=O MWNQXXOSWHCCOZ-UHFFFAOYSA-L 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- 239000007844 bleaching agent Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 235000017550 sodium carbonate Nutrition 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 239000003381 stabilizer Substances 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000010410 dusting Methods 0.000 description 1
- 229940071106 ethylenediaminetetraacetate Drugs 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 description 1
- 239000000391 magnesium silicate Substances 0.000 description 1
- 229910052919 magnesium silicate Inorganic materials 0.000 description 1
- 235000019792 magnesium silicate Nutrition 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 239000006199 nebulizer Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
- 229940048086 sodium pyrophosphate Drugs 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/10—Peroxyhydrates; Peroxyacids or salts thereof containing carbon
- C01B15/103—Peroxyhydrates; Peroxyacids or salts thereof containing carbon containing only alkali metals as metals
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7331041A FR2242328B1 (OSRAM) | 1973-08-28 | 1973-08-28 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2441014A1 DE2441014A1 (de) | 1975-03-27 |
| DE2441014B2 DE2441014B2 (de) | 1978-10-19 |
| DE2441014C3 true DE2441014C3 (de) | 1979-06-07 |
Family
ID=9124381
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2441014A Expired DE2441014C3 (de) | 1973-08-28 | 1974-08-27 | Verfahren zur Herstellung von Natriumpercarbonat durch Zerstäubung |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US4018874A (OSRAM) |
| JP (1) | JPS544359B2 (OSRAM) |
| AT (1) | AT349433B (OSRAM) |
| BE (1) | BE816421A (OSRAM) |
| BR (1) | BR7407099A (OSRAM) |
| CA (1) | CA1033534A (OSRAM) |
| CH (1) | CH593864A5 (OSRAM) |
| DE (1) | DE2441014C3 (OSRAM) |
| DK (1) | DK139263B (OSRAM) |
| ES (1) | ES429567A1 (OSRAM) |
| FR (1) | FR2242328B1 (OSRAM) |
| GB (1) | GB1479896A (OSRAM) |
| IE (1) | IE39728B1 (OSRAM) |
| IT (1) | IT1016893B (OSRAM) |
| LU (1) | LU70798A1 (OSRAM) |
| NL (1) | NL180094C (OSRAM) |
| NO (1) | NO138086C (OSRAM) |
| SE (1) | SE400541B (OSRAM) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS51135900A (en) * | 1975-05-19 | 1976-11-25 | Kao Corp | Method for prod uction of the stable sodium percarbonate |
| FR2380221A1 (fr) * | 1977-02-11 | 1978-09-08 | Ugine Kuhlmann | Perfectionnement au procede de preparation du percarbonate de sodium |
| JPS5833164B2 (ja) * | 1980-07-04 | 1983-07-18 | 花王株式会社 | 中空顆粒状過炭酸塩及びその製造方法 |
| US4966762A (en) * | 1988-10-06 | 1990-10-30 | Fmc Corporation | Process for manufacturing a soda ash peroxygen carrier |
| US4970058A (en) * | 1988-10-06 | 1990-11-13 | Fmc Corporation | Soda ash peroxygen carrier |
| US4970019A (en) * | 1988-10-27 | 1990-11-13 | Fmc Corporation | Particulate composition containing bleach and optical brightener and process for its manufacture |
| JPH0649086B2 (ja) * | 1989-08-05 | 1994-06-29 | 三井・デュポンフロロケミカル株式会社 | 塩弗化アルカンの接触分解法 |
| FI94618C (fi) † | 1993-11-30 | 1995-10-10 | Kemira Oy | Menetelmä stabiilisuudeltaan parempien natriumperkarbonaattipartikkelien valmistamiseksi |
| CA2204727A1 (en) * | 1994-10-04 | 1996-04-11 | Charles E. Sizer | Method of disinfecting the food contact surfaces of food packaging machines and disinfecting solution therefor |
| CN103002878B (zh) | 2010-04-09 | 2015-07-01 | 帕西拉制药有限公司 | 用于配制大直径合成膜囊泡的方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2167997A (en) * | 1938-02-16 | 1939-08-01 | Du Pont | Preparation of metal percarbonates |
| US2541733A (en) * | 1947-05-22 | 1951-02-13 | Du Pont | Production of alkali metal carbonate perhydrates |
| SU141853A1 (ru) * | 1960-10-10 | 1960-11-30 | Т.П. Фирсова | Способ получени истинных перкарбонатов щелочных металлов |
| GB1165154A (en) * | 1965-12-10 | 1969-09-24 | Laporte Chemical | Peroxygen Compounds |
| GB1312514A (en) * | 1970-07-06 | 1973-04-04 | Laporte Industries Ltd | Process for the preparation of peroxygen compounds |
-
1973
- 1973-08-28 FR FR7331041A patent/FR2242328B1/fr not_active Expired
-
1974
- 1974-06-17 BE BE145497A patent/BE816421A/xx not_active IP Right Cessation
- 1974-06-25 GB GB28164/74A patent/GB1479896A/en not_active Expired
- 1974-07-29 IE IE1603/74A patent/IE39728B1/xx unknown
- 1974-08-15 US US05/497,537 patent/US4018874A/en not_active Expired - Lifetime
- 1974-08-19 AT AT673474A patent/AT349433B/de not_active IP Right Cessation
- 1974-08-20 CA CA207,429A patent/CA1033534A/en not_active Expired
- 1974-08-26 SE SE7410818A patent/SE400541B/xx not_active IP Right Cessation
- 1974-08-26 LU LU70798A patent/LU70798A1/xx unknown
- 1974-08-27 NL NLAANVRAGE7411397,A patent/NL180094C/xx not_active IP Right Cessation
- 1974-08-27 IT IT69621/74A patent/IT1016893B/it active
- 1974-08-27 ES ES429567A patent/ES429567A1/es not_active Expired
- 1974-08-27 BR BR7099/74A patent/BR7407099A/pt unknown
- 1974-08-27 CH CH1166874A patent/CH593864A5/xx not_active IP Right Cessation
- 1974-08-27 DK DK454874AA patent/DK139263B/da not_active IP Right Cessation
- 1974-08-27 DE DE2441014A patent/DE2441014C3/de not_active Expired
- 1974-08-28 NO NO743074A patent/NO138086C/no unknown
- 1974-08-28 JP JP9800874A patent/JPS544359B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CA1033534A (en) | 1978-06-27 |
| ES429567A1 (es) | 1976-08-16 |
| NO743074L (OSRAM) | 1975-03-24 |
| DE2441014B2 (de) | 1978-10-19 |
| LU70798A1 (OSRAM) | 1975-01-02 |
| AT349433B (de) | 1979-04-10 |
| IE39728L (en) | 1975-02-28 |
| SE7410818L (OSRAM) | 1975-03-03 |
| NL7411397A (nl) | 1975-03-04 |
| ATA673474A (de) | 1978-09-15 |
| IT1016893B (it) | 1977-06-20 |
| BR7407099A (pt) | 1975-11-04 |
| DK139263B (da) | 1979-01-22 |
| GB1479896A (en) | 1977-07-13 |
| US4018874A (en) | 1977-04-19 |
| SE400541B (sv) | 1978-04-03 |
| NO138086B (no) | 1978-03-20 |
| NL180094C (nl) | 1987-01-02 |
| DK454874A (OSRAM) | 1975-04-28 |
| DE2441014A1 (de) | 1975-03-27 |
| BE816421A (fr) | 1974-10-16 |
| IE39728B1 (en) | 1978-12-20 |
| FR2242328B1 (OSRAM) | 1976-05-07 |
| JPS544359B2 (OSRAM) | 1979-03-06 |
| JPS5051099A (OSRAM) | 1975-05-07 |
| DK139263C (OSRAM) | 1979-06-18 |
| NL180094B (nl) | 1986-08-01 |
| CH593864A5 (OSRAM) | 1977-12-15 |
| NO138086C (no) | 1978-06-28 |
| FR2242328A1 (OSRAM) | 1975-03-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) |