DE2420765C3 - Verfahren zur Reinigung von Decandicarbonsäure- (l,lo) - Google Patents
Verfahren zur Reinigung von Decandicarbonsäure- (l,lo)Info
- Publication number
- DE2420765C3 DE2420765C3 DE2420765A DE2420765A DE2420765C3 DE 2420765 C3 DE2420765 C3 DE 2420765C3 DE 2420765 A DE2420765 A DE 2420765A DE 2420765 A DE2420765 A DE 2420765A DE 2420765 C3 DE2420765 C3 DE 2420765C3
- Authority
- DE
- Germany
- Prior art keywords
- acid
- weight
- content
- percent
- distillation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 title claims description 44
- 238000000034 method Methods 0.000 title claims description 15
- 238000004140 cleaning Methods 0.000 title 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 26
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 23
- 229910017604 nitric acid Inorganic materials 0.000 claims description 23
- 239000002253 acid Substances 0.000 claims description 20
- 230000003647 oxidation Effects 0.000 claims description 16
- 238000007254 oxidation reaction Methods 0.000 claims description 16
- 229910052757 nitrogen Inorganic materials 0.000 claims description 13
- SXVPOSFURRDKBO-UHFFFAOYSA-N Cyclododecanone Chemical compound O=C1CCCCCCCCCCC1 SXVPOSFURRDKBO-UHFFFAOYSA-N 0.000 claims description 8
- 239000003054 catalyst Substances 0.000 claims description 6
- 239000007800 oxidant agent Substances 0.000 claims description 4
- 238000000746 purification Methods 0.000 claims description 2
- DDTBPAQBQHZRDW-UHFFFAOYSA-N cyclododecane Chemical compound C1CCCCCCCCCCC1 DDTBPAQBQHZRDW-UHFFFAOYSA-N 0.000 claims 1
- 238000004821 distillation Methods 0.000 description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 24
- 241001550224 Apha Species 0.000 description 17
- 239000000047 product Substances 0.000 description 13
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 10
- 238000010438 heat treatment Methods 0.000 description 8
- QJGNSTCICFBACB-UHFFFAOYSA-N 2-octylpropanedioic acid Chemical compound CCCCCCCCC(C(O)=O)C(O)=O QJGNSTCICFBACB-UHFFFAOYSA-N 0.000 description 5
- 239000004952 Polyamide Substances 0.000 description 5
- SFVWPXMPRCIVOK-UHFFFAOYSA-N cyclododecanol Chemical compound OC1CCCCCCCCCCC1 SFVWPXMPRCIVOK-UHFFFAOYSA-N 0.000 description 5
- 230000008014 freezing Effects 0.000 description 5
- 238000007710 freezing Methods 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- 229920002647 polyamide Polymers 0.000 description 5
- 239000011552 falling film Substances 0.000 description 4
- 229910001385 heavy metal Inorganic materials 0.000 description 4
- GQPLMRYTRLFLPF-UHFFFAOYSA-N nitrous oxide Inorganic materials [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 description 4
- 229920000728 polyester Polymers 0.000 description 4
- 230000008018 melting Effects 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 239000012452 mother liquor Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 239000013078 crystal Substances 0.000 description 2
- 150000001991 dicarboxylic acids Chemical class 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000010408 film Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- WQYVRQLZKVEZGA-UHFFFAOYSA-N hypochlorite Chemical compound Cl[O-] WQYVRQLZKVEZGA-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 238000007669 thermal treatment Methods 0.000 description 2
- FWQNYUYRXNWOOM-UHFFFAOYSA-N 2-nonylpropanedioic acid Chemical compound CCCCCCCCCC(C(O)=O)C(O)=O FWQNYUYRXNWOOM-UHFFFAOYSA-N 0.000 description 1
- 241000530268 Lycaena heteronea Species 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical compound [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001944 continuous distillation Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- KBFICOCXSYMXRY-UHFFFAOYSA-N decanedioic acid;nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O.OC(=O)CCCCCCCCC(O)=O KBFICOCXSYMXRY-UHFFFAOYSA-N 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 150000002897 organic nitrogen compounds Chemical class 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 229920006149 polyester-amide block copolymer Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000009183 running Effects 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- 238000000967 suction filtration Methods 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- LSGOVYNHVSXFFJ-UHFFFAOYSA-N vanadate(3-) Chemical compound [O-][V]([O-])([O-])=O LSGOVYNHVSXFFJ-UHFFFAOYSA-N 0.000 description 1
- 150000003681 vanadium Chemical class 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (11)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2420765A DE2420765C3 (de) | 1974-04-29 | 1974-04-29 | Verfahren zur Reinigung von Decandicarbonsäure- (l,lo) |
| FR7511934A FR2268781B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1974-04-29 | 1975-04-17 | |
| IT49257/75A IT1035434B (it) | 1974-04-29 | 1975-04-23 | Procedimento per la depurazione di acido decandicarbossilicoi io |
| JP50049859A JPS582217B2 (ja) | 1974-04-29 | 1975-04-25 | デカンジカルボン酸−（１，１０）の製法 |
| SU752127953A SU623516A3 (ru) | 1974-04-29 | 1975-04-25 | Способ очистки декандикарбоновой -1,10 кислоты |
| DD185738A DD119410A5 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1974-04-29 | 1975-04-28 | |
| BE155883A BE828508A (fr) | 1974-04-29 | 1975-04-28 | Procede de purification de l'acide decane-1,10-dicarboxylique |
| GB17484/75A GB1501997A (en) | 1974-04-29 | 1975-04-28 | Process for the purification of decane dicarboxylic acid-(1,10) |
| CA225,645A CA1051025A (en) | 1974-04-29 | 1975-04-28 | Process for the purification of decane dicarboxylic acid-(1,10) |
| NL7505111A NL7505111A (nl) | 1974-04-29 | 1975-04-29 | Werkwijze voor het zuiveren van decaandicar- bonzuur-(1,10). |
| US05/572,857 US4067779A (en) | 1974-04-29 | 1975-04-29 | Process for the purification of 1,10-decanedicarboxylic acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2420765A DE2420765C3 (de) | 1974-04-29 | 1974-04-29 | Verfahren zur Reinigung von Decandicarbonsäure- (l,lo) |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2420765A1 DE2420765A1 (de) | 1975-10-30 |
| DE2420765B2 DE2420765B2 (de) | 1980-05-29 |
| DE2420765C3 true DE2420765C3 (de) | 1981-02-12 |
Family
ID=5914274
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2420765A Expired DE2420765C3 (de) | 1974-04-29 | 1974-04-29 | Verfahren zur Reinigung von Decandicarbonsäure- (l,lo) |
Country Status (11)
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2486935A1 (fr) * | 1980-07-17 | 1982-01-22 | Du Pont | Traitement d'esters de diacide par des hydroborates, permanganates ou methoxydes alcalins |
| CN103183813A (zh) * | 2005-04-22 | 2013-07-03 | 三菱化学株式会社 | 来自生物质资源的聚酯及其制造方法 |
| CN101525287B (zh) * | 2008-03-04 | 2012-02-08 | 上海芝东商务咨询有限公司 | 一种癸二酸的精制方法 |
| JP2011515411A (ja) * | 2008-03-19 | 2011-05-19 | インビスタ テクノロジーズ エス エイ アール エル | シクロドデカトリエンの製造方法およびラウロラクトンの製造方法 |
| WO2012082617A2 (en) * | 2010-12-14 | 2012-06-21 | Aquatech International Corporation | Method for recycling deoiled water using counterflow falling-film evaporators |
| US12017182B2 (en) | 2019-12-24 | 2024-06-25 | Cathay Biotech Inc. | Method and system for refining long chain dicarboxylic acid |
| CN111138273B (zh) | 2019-12-24 | 2024-11-26 | 上海凯赛生物技术股份有限公司 | 一种长链二元酸的精制工艺及系统 |
| CN113307532B (zh) * | 2021-06-15 | 2022-04-22 | 西南石油大学 | 一种低温固井用控制水泥水化热的微胶囊的制备方法 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2522529A (en) * | 1946-01-08 | 1950-09-19 | Robert W Miller | Distillation of alcohols from dibasic acid diesters |
| US2791551A (en) * | 1952-05-01 | 1957-05-07 | Wyandotte Chemicals Corp | Removal of hno3 from carboxymethyl diethers of ethylene glycols |
| US2771482A (en) * | 1953-08-26 | 1956-11-20 | Gulf Research Development Co | Nitric acid oxidation of hydrocarbons |
| US2791598A (en) * | 1953-08-26 | 1957-05-07 | Gulf Research Development Co | Nitric acid oxidation of hydrocarbons |
| US2878276A (en) * | 1955-05-03 | 1959-03-17 | Gulf Research Development Co | Process for producing dibasic carboxylic acids |
| NL289024A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1962-02-19 | |||
| US3402108A (en) * | 1966-07-07 | 1968-09-17 | Emery Industries Inc | Process for the production of a purified grade of azelaic acid by treatment with ozone during purification |
| US3637832A (en) * | 1968-03-12 | 1972-01-25 | Du Pont | Preparation of straight chain dicarboxylic acids |
| DE1919228C3 (de) * | 1969-04-16 | 1984-04-12 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur kontinuierlichen Herstellung von gesättigten aliphatischen Dicarbonsäuren |
| JPS4834578A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1971-09-07 | 1973-05-19 | ||
| DE2217003C2 (de) * | 1972-04-08 | 1983-12-15 | Chemische Werke Hüls AG, 4370 Marl | Verfahren und Vorrichtung zur kontinuierlichen Herstellung von gesättigten aliphatischen Dicarbonsäuren |
| US3903152A (en) * | 1972-07-04 | 1975-09-02 | Toa Gosei Chem Ind | Process for producing highly pure 1,12-dodecanedioic acid |
| US3979450A (en) * | 1973-02-08 | 1976-09-07 | Jury Leonidovich Moskovich | Method for preparing dicarboxylic acids |
-
1974
- 1974-04-29 DE DE2420765A patent/DE2420765C3/de not_active Expired
-
1975
- 1975-04-17 FR FR7511934A patent/FR2268781B1/fr not_active Expired
- 1975-04-23 IT IT49257/75A patent/IT1035434B/it active
- 1975-04-25 JP JP50049859A patent/JPS582217B2/ja not_active Expired
- 1975-04-25 SU SU752127953A patent/SU623516A3/ru active
- 1975-04-28 CA CA225,645A patent/CA1051025A/en not_active Expired
- 1975-04-28 DD DD185738A patent/DD119410A5/xx unknown
- 1975-04-28 BE BE155883A patent/BE828508A/xx unknown
- 1975-04-28 GB GB17484/75A patent/GB1501997A/en not_active Expired
- 1975-04-29 NL NL7505111A patent/NL7505111A/xx not_active Application Discontinuation
- 1975-04-29 US US05/572,857 patent/US4067779A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| FR2268781A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1975-11-21 |
| FR2268781B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1979-08-24 |
| IT1035434B (it) | 1979-10-20 |
| DE2420765A1 (de) | 1975-10-30 |
| JPS50149616A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1975-11-29 |
| BE828508A (fr) | 1975-08-18 |
| SU623516A3 (ru) | 1978-09-05 |
| NL7505111A (nl) | 1975-10-31 |
| JPS582217B2 (ja) | 1983-01-14 |
| DE2420765B2 (de) | 1980-05-29 |
| CA1051025A (en) | 1979-03-20 |
| DD119410A5 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1976-04-20 |
| US4067779A (en) | 1978-01-10 |
| GB1501997A (en) | 1978-02-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: HUELS AG, 4370 MARL, DE |
|
| 8339 | Ceased/non-payment of the annual fee |