DE2231988C2 - Galvanisches Bad für die Abscheidung von glänzendem Zinn - Google Patents
Galvanisches Bad für die Abscheidung von glänzendem ZinnInfo
- Publication number
- DE2231988C2 DE2231988C2 DE2231988A DE2231988A DE2231988C2 DE 2231988 C2 DE2231988 C2 DE 2231988C2 DE 2231988 A DE2231988 A DE 2231988A DE 2231988 A DE2231988 A DE 2231988A DE 2231988 C2 DE2231988 C2 DE 2231988C2
- Authority
- DE
- Germany
- Prior art keywords
- tin
- bath
- deposition
- aldehyde
- shiny
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 title claims description 10
- 230000008021 deposition Effects 0.000 title claims description 7
- OJVAMHKKJGICOG-UHFFFAOYSA-N 2,5-hexanedione Chemical compound CC(=O)CCC(C)=O OJVAMHKKJGICOG-UHFFFAOYSA-N 0.000 claims description 24
- 239000007795 chemical reaction product Substances 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 11
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 10
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 10
- 239000000654 additive Substances 0.000 claims description 10
- 239000000080 wetting agent Substances 0.000 claims description 10
- 125000003545 alkoxy group Chemical group 0.000 claims description 8
- 230000000996 additive effect Effects 0.000 claims description 7
- -1 tin (II) ions Chemical class 0.000 claims description 5
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 3
- 238000005282 brightening Methods 0.000 claims description 3
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 claims 1
- 150000001299 aldehydes Chemical group 0.000 description 12
- 239000000203 mixture Substances 0.000 description 11
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 10
- 125000004432 carbon atom Chemical group C* 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 5
- 125000000217 alkyl group Chemical group 0.000 description 5
- 238000000151 deposition Methods 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 4
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000002244 precipitate Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 125000002373 5 membered heterocyclic group Chemical group 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 238000007792 addition Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000004094 surface-active agent Substances 0.000 description 3
- ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical compound CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 description 2
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 description 2
- 229960000583 acetic acid Drugs 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 230000001464 adherent effect Effects 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 238000004070 electrodeposition Methods 0.000 description 2
- 238000009713 electroplating Methods 0.000 description 2
- 150000002462 imidazolines Chemical class 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 description 2
- 239000006259 organic additive Substances 0.000 description 2
- QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 2
- 230000000737 periodic effect Effects 0.000 description 2
- 238000007747 plating Methods 0.000 description 2
- 229920000570 polyether Polymers 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 1
- 229910001369 Brass Inorganic materials 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- 206010037867 Rash macular Diseases 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 125000003172 aldehyde group Chemical group 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 239000010951 brass Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 230000008451 emotion Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- SYSQUGFVNFXIIT-UHFFFAOYSA-N n-[4-(1,3-benzoxazol-2-yl)phenyl]-4-nitrobenzenesulfonamide Chemical class C1=CC([N+](=O)[O-])=CC=C1S(=O)(=O)NC1=CC=C(C=2OC3=CC=CC=C3N=2)C=C1 SYSQUGFVNFXIIT-UHFFFAOYSA-N 0.000 description 1
- 238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000012044 organic layer Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 125000006353 oxyethylene group Chemical group 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- OBBXFSIWZVFYJR-UHFFFAOYSA-L tin(2+);sulfate Chemical compound [Sn+2].[O-]S([O-])(=O)=O OBBXFSIWZVFYJR-UHFFFAOYSA-L 0.000 description 1
- 229910000375 tin(II) sulfate Inorganic materials 0.000 description 1
- 239000005028 tinplate Substances 0.000 description 1
- 210000002105 tongue Anatomy 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/30—Electroplating: Baths therefor from solutions of tin
- C25D3/32—Electroplating: Baths therefor from solutions of tin characterised by the organic bath constituents used
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Electroplating And Plating Baths Therefor (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US15903571A | 1971-07-01 | 1971-07-01 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2231988A1 DE2231988A1 (de) | 1973-01-18 |
| DE2231988C2 true DE2231988C2 (de) | 1982-04-01 |
Family
ID=22570808
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2231988A Expired DE2231988C2 (de) | 1971-07-01 | 1972-06-29 | Galvanisches Bad für die Abscheidung von glänzendem Zinn |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US3755096A (enExample) |
| JP (1) | JPS5632397B1 (enExample) |
| AU (1) | AU472304B2 (enExample) |
| CA (1) | CA1035315A (enExample) |
| DE (1) | DE2231988C2 (enExample) |
| ES (1) | ES404332A1 (enExample) |
| FR (1) | FR2143922B1 (enExample) |
| GB (1) | GB1373293A (enExample) |
| IT (1) | IT959485B (enExample) |
| NL (1) | NL7209231A (enExample) |
| SE (1) | SE385920B (enExample) |
| ZA (1) | ZA723658B (enExample) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3977949A (en) * | 1975-07-07 | 1976-08-31 | Columbia Chemical Corporation | Acidic plating bath and additives for electrodeposition of bright tin |
| NZ190645A (en) * | 1978-06-16 | 1980-11-14 | M & T Chemicals Inc | Aqueous acid tin plating bath containing 2,5-dimethoxy-benzaldehyde as brightening agent |
| US4242182A (en) * | 1978-07-21 | 1980-12-30 | Francine Popescu | Bright tin electroplating bath |
| PL120216B1 (en) * | 1979-01-11 | 1982-02-27 | Politechnika Warszawska | Process for electrochemical manufacture of bright tin coatingsovjannykh pokrytijj |
| JPS5843797U (ja) * | 1981-09-17 | 1983-03-24 | シャープ株式会社 | 電子レンジ |
| JPS5864765U (ja) * | 1981-10-27 | 1983-05-02 | 三和シヤツタ−工業株式会社 | 折戸の閉鎖保持装置 |
| US4530741A (en) * | 1984-07-12 | 1985-07-23 | Columbia Chemical Corporation | Aqueous acid plating bath and brightener composition for producing bright electrodeposits of tin |
| US4844780A (en) * | 1988-02-17 | 1989-07-04 | Maclee Chemical Company, Inc. | Brightener and aqueous plating bath for tin and/or lead |
| AU2927392A (en) * | 1991-11-01 | 1993-06-07 | National-Standard Company | Age resistant solder coatings |
| US5394084A (en) * | 1991-12-23 | 1995-02-28 | The Boeing Company | Method and apparatus for reducing errors in eddy-current conductivity measurements due to lift-off by interpolating between a plurality of reference conductivity measurements |
| US5814202A (en) * | 1997-10-14 | 1998-09-29 | Usx Corporation | Electrolytic tin plating process with reduced sludge production |
| WO2007088600A1 (ja) * | 2006-02-01 | 2007-08-09 | Murata Manufacturing Co., Ltd. | セラミック電子部品の製造方法及びめっき浴 |
| GB2564149A (en) | 2017-07-05 | 2019-01-09 | Skf Ab | Electroplated cage for rolling element bearing |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL134963C (enExample) * | 1963-08-28 | |||
| NL128321C (enExample) * | 1965-02-13 | |||
| NL151449B (nl) * | 1966-09-14 | 1976-11-15 | Philips Nv | Werkwijze voor de bereiding van een zuur bad voor het elektrolytisch neerslaan van tin. |
| US3577328A (en) * | 1968-11-07 | 1971-05-04 | Conversion Chem Corp | Method and bath for electroplating tin |
| NL6910903A (enExample) * | 1969-07-16 | 1971-01-19 | ||
| US3616306A (en) * | 1969-11-19 | 1971-10-26 | Conversion Chem Corp | Tin plating bath and method |
| US3669854A (en) * | 1970-08-03 | 1972-06-13 | M & T Chemicals Inc | Zinc electroplating electrolyte and process |
-
1971
- 1971-07-01 US US00159035A patent/US3755096A/en not_active Expired - Lifetime
-
1972
- 1972-05-29 ZA ZA723658A patent/ZA723658B/xx unknown
- 1972-06-20 GB GB2884972A patent/GB1373293A/en not_active Expired
- 1972-06-21 AU AU43661/72A patent/AU472304B2/en not_active Expired
- 1972-06-26 SE SE7208364A patent/SE385920B/xx unknown
- 1972-06-28 ES ES404332A patent/ES404332A1/es not_active Expired
- 1972-06-29 DE DE2231988A patent/DE2231988C2/de not_active Expired
- 1972-06-30 FR FR7223710A patent/FR2143922B1/fr not_active Expired
- 1972-06-30 NL NL7209231A patent/NL7209231A/xx not_active Application Discontinuation
- 1972-06-30 IT IT9569/72A patent/IT959485B/it active
- 1972-06-30 CA CA146,105A patent/CA1035315A/en not_active Expired
- 1972-07-01 JP JP6618972A patent/JPS5632397B1/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| CA1035315A (en) | 1978-07-25 |
| SE385920B (sv) | 1976-07-26 |
| DE2231988A1 (de) | 1973-01-18 |
| US3755096A (en) | 1973-08-28 |
| JPS5632397B1 (enExample) | 1981-07-27 |
| ZA723658B (en) | 1973-03-28 |
| NL7209231A (enExample) | 1973-01-03 |
| AU472304B2 (en) | 1976-05-20 |
| FR2143922B1 (enExample) | 1977-04-01 |
| IT959485B (it) | 1973-11-10 |
| ES404332A1 (es) | 1976-01-01 |
| AU4366172A (en) | 1974-01-03 |
| FR2143922A1 (enExample) | 1973-02-09 |
| GB1373293A (en) | 1974-11-06 |
Similar Documents
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|---|---|---|
| DE2231988C2 (de) | Galvanisches Bad für die Abscheidung von glänzendem Zinn | |
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| DE3447813C2 (enExample) | ||
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| OI | Miscellaneous see part 1 | ||
| OI | Miscellaneous see part 1 | ||
| D2 | Grant after examination | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: M & T CHEMICALS, INC., WOODBRIDGE, N.J., US |
|
| 8339 | Ceased/non-payment of the annual fee |