DE213592C - - Google Patents

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Publication number

DE213592C

DE213592C DENDAT213592D DE213592DA DE213592C DE 213592 C DE213592 C DE 213592C DE NDAT213592 D DENDAT213592 D DE NDAT213592D DE 213592D A DE213592D A DE 213592DA DE 213592 C DE213592 C DE 213592C

Authority

DE

Germany

Prior art keywords

water

amino

melts

dissolved

substituted

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• PLIKAWJENQZMHA-UHFFFAOYSA-N 4-aminophenol Chemical class NC1=CC=C(O)C=C1 PLIKAWJENQZMHA-UHFFFAOYSA-N 0.000 claims description 7
• HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 5
• 150000003934 aromatic aldehydes Chemical class 0.000 claims description 4
• 239000003513 alkali Substances 0.000 claims description 3
• 239000007859 condensation product Substances 0.000 claims description 3
• 238000000034 method Methods 0.000 claims description 3
• 125000003710 aryl alkyl group Chemical group 0.000 claims description 2
• 239000011701 zinc Substances 0.000 claims description 2
• 229910052725 zinc Inorganic materials 0.000 claims description 2
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 7
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
• 239000000155 melt Substances 0.000 description 5
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
• HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 4
• SCVFZCLFOSHCOH-UHFFFAOYSA-M potassium acetate Chemical compound [K+].CC([O-])=O SCVFZCLFOSHCOH-UHFFFAOYSA-M 0.000 description 4
• GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 4
• 239000000243 solution Substances 0.000 description 4
• QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
• -1 N-benzyl-4-amino-3-chlorophenol Chemical compound 0.000 description 3
• 239000002585 base Substances 0.000 description 3
• 239000000203 mixture Substances 0.000 description 3
• 235000011121 sodium hydroxide Nutrition 0.000 description 3
• 239000003929 acidic solution Substances 0.000 description 2
• 239000007864 aqueous solution Substances 0.000 description 2
• 239000003610 charcoal Substances 0.000 description 2
• 238000001816 cooling Methods 0.000 description 2
• 238000000354 decomposition reaction Methods 0.000 description 2
• QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 2
• 235000011056 potassium acetate Nutrition 0.000 description 2
• 239000000047 product Substances 0.000 description 2
• 150000003839 salts Chemical class 0.000 description 2
• 235000010265 sodium sulphite Nutrition 0.000 description 2
• 238000006467 substitution reaction Methods 0.000 description 2
• QTDCIMUWVJXQBD-UHFFFAOYSA-N 4-Aminophenol sulfate Chemical compound OS([O-])(=O)=O.[NH3+]C1=CC=C(O)C=C1 QTDCIMUWVJXQBD-UHFFFAOYSA-N 0.000 description 1
• QDHHCQZDFGDHMP-UHFFFAOYSA-N Chloramine Chemical compound ClN QDHHCQZDFGDHMP-UHFFFAOYSA-N 0.000 description 1
• DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
• CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
• 230000002378 acidificating effect Effects 0.000 description 1
• 125000003118 aryl group Chemical group 0.000 description 1
• 125000000649 benzylidene group Chemical group [H]C(=[*])C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 150000001875 compounds Chemical class 0.000 description 1
• 239000013078 crystal Substances 0.000 description 1
• 230000029142 excretion Effects 0.000 description 1
• ACXCKRZOISAYHH-UHFFFAOYSA-N molecular chlorine hydrate Chemical compound O.ClCl ACXCKRZOISAYHH-UHFFFAOYSA-N 0.000 description 1
• 239000003208 petroleum Substances 0.000 description 1
• 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 238000000746 purification Methods 0.000 description 1
• 239000011734 sodium Substances 0.000 description 1
• 229910052708 sodium Inorganic materials 0.000 description 1
• 239000007787 solid Substances 0.000 description 1
• 125000003107 substituted aryl group Chemical group 0.000 description 1