DE1944457A1 - Verfahren und Vorrichtung fuer die Umsetzung zwischen Gasen und Fluessigkeiten - Google Patents
Verfahren und Vorrichtung fuer die Umsetzung zwischen Gasen und FluessigkeitenInfo
- Publication number
- DE1944457A1 DE1944457A1 DE19691944457 DE1944457A DE1944457A1 DE 1944457 A1 DE1944457 A1 DE 1944457A1 DE 19691944457 DE19691944457 DE 19691944457 DE 1944457 A DE1944457 A DE 1944457A DE 1944457 A1 DE1944457 A1 DE 1944457A1
- Authority
- DE
- Germany
- Prior art keywords
- liquid
- gas
- baffle plate
- disc
- reactor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007788 liquid Substances 0.000 title claims description 87
- 238000006243 chemical reaction Methods 0.000 title claims description 52
- 238000000034 method Methods 0.000 title claims description 26
- 239000007789 gas Substances 0.000 title description 70
- 230000008569 process Effects 0.000 title description 7
- 239000000463 material Substances 0.000 claims description 33
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 20
- 150000001336 alkenes Chemical class 0.000 claims description 18
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims description 14
- 239000010409 thin film Substances 0.000 claims description 13
- 239000003701 inert diluent Substances 0.000 claims description 10
- 238000012546 transfer Methods 0.000 claims description 8
- 239000003085 diluting agent Substances 0.000 claims description 7
- 230000007480 spreading Effects 0.000 claims description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 1
- 239000000047 product Substances 0.000 description 33
- 235000019441 ethanol Nutrition 0.000 description 22
- 239000000498 cooling water Substances 0.000 description 14
- 239000010408 film Substances 0.000 description 14
- 239000002253 acid Substances 0.000 description 12
- 150000004996 alkyl benzenes Chemical class 0.000 description 12
- 239000003086 colorant Substances 0.000 description 12
- 230000000694 effects Effects 0.000 description 11
- 238000002474 experimental method Methods 0.000 description 8
- 239000002585 base Substances 0.000 description 7
- 238000007865 diluting Methods 0.000 description 7
- 239000002245 particle Substances 0.000 description 7
- 239000003921 oil Substances 0.000 description 6
- 230000003287 optical effect Effects 0.000 description 6
- 238000005192 partition Methods 0.000 description 6
- 238000006277 sulfonation reaction Methods 0.000 description 6
- 239000003599 detergent Substances 0.000 description 5
- 239000012530 fluid Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- 239000007795 chemical reaction product Substances 0.000 description 4
- 230000003301 hydrolyzing effect Effects 0.000 description 4
- 238000007654 immersion Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 230000004048 modification Effects 0.000 description 4
- 238000012986 modification Methods 0.000 description 4
- 238000010186 staining Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- MWUXSHHQAYIFBG-UHFFFAOYSA-N Nitric oxide Chemical compound O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 3
- 230000003247 decreasing effect Effects 0.000 description 3
- 230000003472 neutralizing effect Effects 0.000 description 3
- 150000002894 organic compounds Chemical class 0.000 description 3
- 150000003138 primary alcohols Chemical class 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000004711 α-olefin Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000004040 coloring Methods 0.000 description 2
- 239000004020 conductor Substances 0.000 description 2
- PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical compound NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 description 2
- 239000011552 falling film Substances 0.000 description 2
- 150000002191 fatty alcohols Chemical class 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- WQYVRQLZKVEZGA-UHFFFAOYSA-N hypochlorite Chemical compound Cl[O-] WQYVRQLZKVEZGA-UHFFFAOYSA-N 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 2
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- 241001225841 Besa Species 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 206010010219 Compulsions Diseases 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 238000005219 brazing Methods 0.000 description 1
- 230000031709 bromination Effects 0.000 description 1
- 238000005893 bromination reaction Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 238000004440 column chromatography Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000000625 cyclamic acid and its Na and Ca salt Substances 0.000 description 1
- HCAJEUSONLESMK-UHFFFAOYSA-N cyclohexylsulfamic acid Chemical compound OS(=O)(=O)NC1CCCCC1 HCAJEUSONLESMK-UHFFFAOYSA-N 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000007038 hydrochlorination reaction Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 230000000802 nitrating effect Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 150000003018 phosphorus compounds Chemical class 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 230000036632 reaction speed Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 150000003333 secondary alcohols Chemical class 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- COEZWFYORILMOM-UHFFFAOYSA-N sodium 4-[(2,4-dihydroxyphenyl)diazenyl]benzenesulfonic acid Chemical compound [Na+].OC1=CC(O)=CC=C1N=NC1=CC=C(S(O)(=O)=O)C=C1 COEZWFYORILMOM-UHFFFAOYSA-N 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- UYTGDDAPMOSNND-UHFFFAOYSA-N sulfane sulfur trioxide Chemical compound S.O=S(=O)=O UYTGDDAPMOSNND-UHFFFAOYSA-N 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- XTHPWXDJESJLNJ-UHFFFAOYSA-N sulfurochloridic acid Chemical compound OS(Cl)(=O)=O XTHPWXDJESJLNJ-UHFFFAOYSA-N 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000004809 thin layer chromatography Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 208000012312 yellow dropping Diseases 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1887—Stationary reactors having moving elements inside forming a thin film
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/20—Mixing gases with liquids
- B01F23/21—Mixing gases with liquids by introducing liquids into gaseous media
- B01F23/213—Mixing gases with liquids by introducing liquids into gaseous media by spraying or atomising of the liquids
- B01F23/2131—Mixing gases with liquids by introducing liquids into gaseous media by spraying or atomising of the liquids using rotating elements, e.g. rolls or brushes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
- B01J10/02—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor of the thin-film type
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00085—Plates; Jackets; Cylinders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00189—Controlling or regulating processes controlling the stirring velocity
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB41862/68A GB1282097A (en) | 1968-09-03 | 1968-09-03 | Process and reactor for reacting a gas and a liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1944457A1 true DE1944457A1 (de) | 1970-03-12 |
Family
ID=10421692
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19691944457 Pending DE1944457A1 (de) | 1968-09-03 | 1969-09-02 | Verfahren und Vorrichtung fuer die Umsetzung zwischen Gasen und Fluessigkeiten |
Country Status (7)
| Country | Link |
|---|---|
| JP (1) | JPS4814547B1 (enrdf_load_stackoverflow) |
| BE (1) | BE738383A (enrdf_load_stackoverflow) |
| DE (1) | DE1944457A1 (enrdf_load_stackoverflow) |
| FR (1) | FR2017305B1 (enrdf_load_stackoverflow) |
| GB (1) | GB1282097A (enrdf_load_stackoverflow) |
| NL (1) | NL6913466A (enrdf_load_stackoverflow) |
| ZA (1) | ZA696188B (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010081600A3 (de) * | 2009-01-13 | 2011-01-20 | Construction Research & Technology Gmbh | Rotierende oberflächen für sdr |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS52779A (en) * | 1972-08-30 | 1977-01-06 | Allied Chem | Method and apparatus for reacting thin film of organic liquid with gas medium |
| AU4446979A (en) | 1978-02-21 | 1979-08-30 | Imperial Chemical Industries Limited | Chemical process on the surface of a rotating body |
| CA1125995A (en) | 1978-02-21 | 1982-06-22 | Imperial Chemical Industries Limited | Chemical process in a medium connected to a rotating body |
| GB2185422B (en) * | 1986-01-15 | 1990-08-15 | David Victor Gent | Apparatus for removing contaminants from a gas using a washing liquid |
| GB2417215B (en) * | 2004-08-18 | 2009-06-10 | Protensive Ltd | Spinning disc reactor with enhanced spreader plate features |
| SE536493C2 (sv) * | 2009-03-10 | 2013-12-27 | Alfa Laval Corp Ab | En modul innefattande en reaktorenhet |
| EP2408548A1 (en) | 2009-03-16 | 2012-01-25 | Gabae Technologies, Llc | Apparatus, systems and methods for producing particles using rotating capillaries |
| US20120067427A1 (en) * | 2009-03-16 | 2012-03-22 | Koslow Evan E | Apparatus, systems and methods for mass transfer of gases into liquids |
| US11696766B2 (en) | 2009-09-11 | 2023-07-11 | Tbi Innovations, Llc | Methods and devices to reduce damaging effects of concussive or blast forces on a subject |
| KR20140038438A (ko) * | 2011-05-02 | 2014-03-28 | 테크니쉐 유니버시테이트 아인트호벤 | 다중상 및 단일상 접촉을 위한 디바이스 |
| US8900169B2 (en) | 2013-03-15 | 2014-12-02 | Tbi Innovations, Llc | Methods and devices to reduce the likelihood of injury from concussive or blast forces |
| EA201891055A1 (ru) | 2015-11-16 | 2018-11-30 | Кью30 Спортс Сайенс, Ллк | Устройства для защиты от травматического повреждения головного мозга |
| CA3016454A1 (en) | 2016-03-02 | 2017-09-08 | Q30 Sports Science, Llc | Methods and devices to reduce damaging effects of concussive or blast forces on a subject |
| CN112933866B (zh) * | 2021-03-22 | 2022-07-22 | 哈尔滨工程大学 | 一种可用于有害气体净化处理的气液两相引射器 |
| CN113398852B (zh) * | 2021-06-21 | 2023-03-28 | 许昌学院 | 一种板式塔的内调温装置 |
| CN113731346A (zh) * | 2021-09-23 | 2021-12-03 | 孙建惠 | 一种具有溶剂直接吸结构的无水甲醛加工装置 |
| CN115041120B (zh) * | 2022-06-22 | 2024-04-12 | 华厦镓碳科技(深圳)有限公司 | 一种镓基金属热还原二氧化碳装置及方法 |
-
1968
- 1968-09-03 GB GB41862/68A patent/GB1282097A/en not_active Expired
-
1969
- 1969-08-29 ZA ZA696188*A patent/ZA696188B/xx unknown
- 1969-09-02 DE DE19691944457 patent/DE1944457A1/de active Pending
- 1969-09-03 BE BE738383D patent/BE738383A/xx unknown
- 1969-09-03 NL NL6913466A patent/NL6913466A/xx unknown
- 1969-09-03 JP JP44069402A patent/JPS4814547B1/ja active Pending
- 1969-09-03 FR FR6930081A patent/FR2017305B1/fr not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010081600A3 (de) * | 2009-01-13 | 2011-01-20 | Construction Research & Technology Gmbh | Rotierende oberflächen für sdr |
Also Published As
| Publication number | Publication date |
|---|---|
| BE738383A (enrdf_load_stackoverflow) | 1970-03-03 |
| FR2017305B1 (enrdf_load_stackoverflow) | 1974-08-09 |
| FR2017305A1 (enrdf_load_stackoverflow) | 1970-05-22 |
| NL6913466A (enrdf_load_stackoverflow) | 1970-03-05 |
| GB1282097A (en) | 1972-07-19 |
| JPS4814547B1 (enrdf_load_stackoverflow) | 1973-05-08 |
| ZA696188B (en) | 1971-04-28 |
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