DE1596755A1 - Glas-Kristall-Mischkoerper und Verfahren zu seiner Herstellung - Google Patents
Glas-Kristall-Mischkoerper und Verfahren zu seiner HerstellungInfo
- Publication number
- DE1596755A1 DE1596755A1 DE19661596755 DE1596755A DE1596755A1 DE 1596755 A1 DE1596755 A1 DE 1596755A1 DE 19661596755 DE19661596755 DE 19661596755 DE 1596755 A DE1596755 A DE 1596755A DE 1596755 A1 DE1596755 A1 DE 1596755A1
- Authority
- DE
- Germany
- Prior art keywords
- glass
- percent
- weight
- crystallization
- crystal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000013078 crystal Substances 0.000 title claims description 81
- 238000000034 method Methods 0.000 title claims description 12
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- 230000008569 process Effects 0.000 title description 4
- 239000011521 glass Substances 0.000 claims description 53
- 238000002425 crystallisation Methods 0.000 claims description 38
- 230000008025 crystallization Effects 0.000 claims description 38
- 239000000203 mixture Substances 0.000 claims description 29
- 238000010899 nucleation Methods 0.000 claims description 15
- 230000006911 nucleation Effects 0.000 claims description 15
- 239000002667 nucleating agent Substances 0.000 claims description 12
- 229910052700 potassium Inorganic materials 0.000 claims description 12
- 238000007496 glass forming Methods 0.000 claims description 11
- 239000000155 melt Substances 0.000 claims description 9
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 8
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 6
- 229910006404 SnO 2 Inorganic materials 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 239000000470 constituent Substances 0.000 claims description 4
- 238000011065 in-situ storage Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 229910052664 nepheline Inorganic materials 0.000 description 42
- 239000010434 nepheline Substances 0.000 description 42
- 238000010438 heat treatment Methods 0.000 description 38
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 13
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 10
- 239000011591 potassium Substances 0.000 description 10
- 239000011734 sodium Substances 0.000 description 9
- 230000009466 transformation Effects 0.000 description 7
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 230000035939 shock Effects 0.000 description 5
- 239000006104 solid solution Substances 0.000 description 5
- 238000001816 cooling Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000006066 glass batch Substances 0.000 description 3
- 238000005342 ion exchange Methods 0.000 description 3
- 229910001462 kalsilite Inorganic materials 0.000 description 3
- 229910044991 metal oxide Inorganic materials 0.000 description 3
- 150000004706 metal oxides Chemical class 0.000 description 3
- 230000000704 physical effect Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000002441 X-ray diffraction Methods 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 229910001676 gahnite Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 229910052573 porcelain Inorganic materials 0.000 description 2
- 239000012629 purifying agent Substances 0.000 description 2
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Chemical compound [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 description 2
- 230000002269 spontaneous effect Effects 0.000 description 2
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 2
- 238000011179 visual inspection Methods 0.000 description 2
- 210000004127 vitreous body Anatomy 0.000 description 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 239000006105 batch ingredient Substances 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052792 caesium Inorganic materials 0.000 description 1
- 241001233037 catfish Species 0.000 description 1
- 229910001597 celsian Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 239000011222 crystalline ceramic Substances 0.000 description 1
- 229910002106 crystalline ceramic Inorganic materials 0.000 description 1
- 239000010987 cubic zirconia Substances 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000004031 devitrification Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 239000002241 glass-ceramic Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 239000006193 liquid solution Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012768 molten material Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 229910001415 sodium ion Inorganic materials 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 229910001928 zirconium oxide Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C10/00—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
- C03C10/0018—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition containing SiO2, Al2O3 and monovalent metal oxide as main constituents
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C10/00—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
- C03C10/0054—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition containing PbO, SnO2, B2O3
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Glass Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US45238865A | 1965-04-30 | 1965-04-30 | |
| US17134371A | 1971-08-12 | 1971-08-12 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1596755A1 true DE1596755A1 (de) | 1971-02-25 |
Family
ID=26866996
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19661596755 Pending DE1596755A1 (de) | 1965-04-30 | 1966-04-26 | Glas-Kristall-Mischkoerper und Verfahren zu seiner Herstellung |
Country Status (7)
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3528828A (en) * | 1964-05-28 | 1970-09-15 | Owens Illinois Inc | Glass,ceramics,and method |
| DE1596905C3 (de) * | 1965-01-27 | 1975-05-07 | Nippon Electric Glass Co., Ltd., Otsu, Shiga (Japan) | Thermisch kristallisierbares, Nephelin als Hauptkristallphase abscheidendes Glas auf der Basis des Systems SiO tief 2-AI tief 2 0 tief 3 - Na tief 2 0 und eine durch thermische Kristallisation daraus hergestellte Glaskeramik |
| US4000998A (en) * | 1975-03-19 | 1977-01-04 | Corning Glass Works | Spontaneously-formed nepheline-carnegieite glass-ceramics |
| US4341544A (en) * | 1980-10-31 | 1982-07-27 | Corning Glass Works | Method of making peraluminous nepheline/kalsilite glass-ceramics |
| US4341872A (en) * | 1981-06-05 | 1982-07-27 | Corning Glass Works | Microwave-compatible nepheline glass-ceramics |
| US4467039A (en) * | 1983-05-09 | 1984-08-21 | Corning Glass Works | Potassium fluorrichterite glass ceramics and method |
| US7470640B2 (en) * | 2006-04-11 | 2008-12-30 | Corning Incorporated | Glass-ceramic seals for use in solid oxide fuel cells |
| US7867932B2 (en) * | 2007-08-28 | 2011-01-11 | Corning Incorporated | Refractory glass ceramics |
| US8158261B2 (en) * | 2009-04-22 | 2012-04-17 | National Taipei University Technology | Glass-ceramic composite encapsulation material |
| CA2918056C (en) | 2013-07-22 | 2021-09-21 | Morgan Advanced Materials Plc. | Inorganic fibre compositions |
| US9409815B2 (en) * | 2014-04-04 | 2016-08-09 | Corning Incorporated | Opaque colored glass-ceramics comprising nepheline crystal phases |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3146114A (en) * | 1958-12-30 | 1964-08-25 | Corning Glass Works | Method of making semicrystalline ceramic bodies and the composition thereof |
| US3236662A (en) * | 1962-03-19 | 1966-02-22 | Corning Glass Works | Semicrystalline body and method of making it |
| NL129123C (US20090163788A1-20090625-C00002.png) * | 1962-05-16 | |||
| NL295249A (US20090163788A1-20090625-C00002.png) * | 1962-07-23 | |||
| US3528828A (en) * | 1964-05-28 | 1970-09-15 | Owens Illinois Inc | Glass,ceramics,and method |
-
1966
- 1966-04-21 GB GB17579/66A patent/GB1137976A/en not_active Expired
- 1966-04-26 NL NL6605578A patent/NL6605578A/xx unknown
- 1966-04-26 DE DE19661596755 patent/DE1596755A1/de active Pending
- 1966-04-29 BE BE680361D patent/BE680361A/xx unknown
- 1966-04-29 SE SE5914/66A patent/SE302505B/xx unknown
- 1966-04-29 CH CH622766A patent/CH454372A/fr unknown
-
1971
- 1971-08-12 US US00171343A patent/US3720526A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| CH454372A (fr) | 1968-04-15 |
| US3720526A (en) | 1973-03-13 |
| GB1137976A (en) | 1968-12-27 |
| NL6605578A (US20090163788A1-20090625-C00002.png) | 1966-10-31 |
| BE680361A (US20090163788A1-20090625-C00002.png) | 1966-10-31 |
| SE302505B (US20090163788A1-20090625-C00002.png) | 1968-07-22 |
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