DE1568583A1 - Verfahren zur Herstellung von Dichloraethan - Google Patents
Verfahren zur Herstellung von DichloraethanInfo
- Publication number
- DE1568583A1 DE1568583A1 DE19661568583 DE1568583A DE1568583A1 DE 1568583 A1 DE1568583 A1 DE 1568583A1 DE 19661568583 DE19661568583 DE 19661568583 DE 1568583 A DE1568583 A DE 1568583A DE 1568583 A1 DE1568583 A1 DE 1568583A1
- Authority
- DE
- Germany
- Prior art keywords
- chlorine
- ethylene
- bed
- catalyst
- oxygen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 24
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 title claims description 11
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 46
- 239000000460 chlorine Substances 0.000 claims description 46
- 229910052801 chlorine Inorganic materials 0.000 claims description 46
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical class C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 32
- 239000005977 Ethylene Substances 0.000 claims description 31
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 24
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 23
- 239000001301 oxygen Substances 0.000 claims description 22
- 229910052760 oxygen Inorganic materials 0.000 claims description 22
- 239000003085 diluting agent Substances 0.000 claims description 19
- 239000003054 catalyst Substances 0.000 claims description 17
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 16
- 239000000203 mixture Substances 0.000 claims description 15
- 239000002245 particle Substances 0.000 claims description 14
- 239000011780 sodium chloride Substances 0.000 claims description 14
- 235000011164 potassium chloride Nutrition 0.000 claims description 8
- 239000001103 potassium chloride Substances 0.000 claims description 8
- 241001122767 Theaceae Species 0.000 claims 1
- GZETWZZNDACBTQ-UHFFFAOYSA-N [Cl].C=C Chemical group [Cl].C=C GZETWZZNDACBTQ-UHFFFAOYSA-N 0.000 claims 1
- 229940072033 potash Drugs 0.000 claims 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims 1
- 235000015320 potassium carbonate Nutrition 0.000 claims 1
- 230000035484 reaction time Effects 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 description 29
- 239000000047 product Substances 0.000 description 16
- 235000002639 sodium chloride Nutrition 0.000 description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 239000007789 gas Substances 0.000 description 7
- 230000003197 catalytic effect Effects 0.000 description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
- 229910052799 carbon Inorganic materials 0.000 description 5
- JCLFHZLOKITRCE-UHFFFAOYSA-N 4-pentoxyphenol Chemical compound CCCCCOC1=CC=C(O)C=C1 JCLFHZLOKITRCE-UHFFFAOYSA-N 0.000 description 4
- 241001233037 catfish Species 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 2
- 150000001805 chlorine compounds Chemical class 0.000 description 2
- 229960003750 ethyl chloride Drugs 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- 239000012808 vapor phase Substances 0.000 description 2
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 1
- FMFKNGWZEQOWNK-UHFFFAOYSA-N 1-butoxypropan-2-yl 2-(2,4,5-trichlorophenoxy)propanoate Chemical compound CCCCOCC(C)OC(=O)C(C)OC1=CC(Cl)=C(Cl)C=C1Cl FMFKNGWZEQOWNK-UHFFFAOYSA-N 0.000 description 1
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
- 241000447437 Gerreidae Species 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 description 1
- 206010035148 Plague Diseases 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 description 1
- 125000003963 dichloro group Chemical group Cl* 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 229950011008 tetrachloroethylene Drugs 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
- C07C17/02—Preparation of halogenated hydrocarbons by addition of halogens to unsaturated hydrocarbons
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US48731665A | 1965-09-14 | 1965-09-14 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1568583A1 true DE1568583A1 (de) | 1970-03-05 |
Family
ID=23935245
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19661568583 Pending DE1568583A1 (de) | 1965-09-14 | 1966-09-08 | Verfahren zur Herstellung von Dichloraethan |
Country Status (6)
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0111203A1 (de) * | 1982-12-08 | 1984-06-20 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von 1,2-Dichlorethan |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB8330714D0 (en) * | 1982-12-24 | 1983-12-29 | Ici Plc | 1 2-dichloroethane |
| DE4103281A1 (de) * | 1991-02-04 | 1992-08-06 | Buna Ag | Verfahren zur herstellung von 1,2-dichlorethan |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2099231A (en) * | 1935-06-10 | 1937-11-16 | Shell Dev | Halogenation of unsaturated compounds |
| US2284482A (en) * | 1940-02-13 | 1942-05-26 | Shell Dev | Halo-substitution of mixtures containing saturated organic compounds |
| US2520712A (en) * | 1948-08-10 | 1950-08-29 | Shell Dev | Catalytic purification of unsaturated hydrocarbons |
| US2966525A (en) * | 1959-05-19 | 1960-12-27 | Monsanto Chemicals | Preparation of allyl chloride |
| US3079445A (en) * | 1960-01-04 | 1963-02-26 | Monsanto Chemicals | Production of chloroprene |
| US3215509A (en) * | 1963-08-08 | 1965-11-02 | Int Minerals & Chem Corp | Leaching halite values from langbeinite |
-
1965
- 1965-09-14 US US487316A patent/US3496244A/en not_active Expired - Lifetime
-
1966
- 1966-08-22 NL NL6611822A patent/NL6611822A/xx unknown
- 1966-09-05 GB GB39558/66A patent/GB1145912A/en not_active Expired
- 1966-09-08 DE DE19661568583 patent/DE1568583A1/de active Pending
- 1966-09-09 BE BE686685D patent/BE686685A/xx unknown
- 1966-09-14 ES ES0331187A patent/ES331187A1/es not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0111203A1 (de) * | 1982-12-08 | 1984-06-20 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von 1,2-Dichlorethan |
Also Published As
| Publication number | Publication date |
|---|---|
| US3496244A (en) | 1970-02-17 |
| GB1145912A (en) | 1969-03-19 |
| ES331187A1 (es) | 1967-12-01 |
| NL6611822A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1967-03-15 |
| BE686685A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1967-02-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2659046A1 (de) | Verfahren zur herstellung von 1-chlor- 1,1-difluoraethan und/oder 1,1,1-trifluoraethan | |
| EP0291860B1 (de) | Verfahren zur Herstellung von CF3I | |
| DE1468679C3 (de) | Chlorfluorierung von Acetylen | |
| DE2751434C3 (de) | Verfahren zur Wiedergewinnung von Chlorwerte | |
| CH650499A5 (de) | Verfahren zur herstellung von 3-chlor-5-trifluormethylpyridinen. | |
| DE1468680C3 (de) | Verfahren zur Herstellung chlorfluorierter Derivate des Äthylens oder des Äthans | |
| DE1568583A1 (de) | Verfahren zur Herstellung von Dichloraethan | |
| DE2631658C2 (de) | Verfahren zur Herstellung von Vinylidenfluorid | |
| DE2005259C3 (de) | Verfahren zur Herstellung von p-Bromphenol | |
| DE3640383A1 (de) | Kohlenwasserstoff-loesliche metallorganische komplexe von magnesium und alkalimetallen sowie ein verfahren zu deren herstellung | |
| DE2702932A1 (de) | Verfahren zur herstellung von fluorreichen, organischen, ein oder zwei kohlenstoffatome enthaltenden verbindungen | |
| DE1618779B2 (de) | Perfluoralkyljodide, Verfahren zu ihrer Herstellung und ihre Verwendung als Telomerisationsinitiatoren | |
| DE2257107A1 (de) | Verfahren zur herstellung von vinylidenchlorid | |
| DE1592368C3 (de) | Verfahren zur Gewinnung von Ammoniak und Chlor aus Ammoniumchlorid | |
| DE2123989A1 (de) | Verfahren zur Herstellung von C tief 1bis C tief 10-Alkylestern der Chrysanthemsäure | |
| DD215528A5 (de) | Verfahren zur herstellung von 1,2-dichlorethan | |
| DE1232129B (de) | Verfahren zur kontinuierlichen Herstellung von Monochloressigsaeure | |
| DE1568583C (de) | Verfahren zur Herstellung von reinem Dichlorathan | |
| DE2837690C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| DE3000277A1 (de) | Verfahren zur herstellung von allylchlorid | |
| DE2509517C3 (de) | Verfahren zur Herstellung einer bromfreien Alkali oder Erdalkalichloridlösung | |
| DE1240842B (de) | Verfahren zur Aufbereitung von hochchlorierten, spezifisch schweren Rueckstaenden, die bei der industriellen Herstellung von chlorierten Kohlenwasserstoffen anfallen | |
| DE736884C (de) | Verfahren zur Herstellung von Hexachlorbutadien | |
| DE1044777B (de) | Verfahren zur Herstellung von Phosphorpentafluorid | |
| DE888701C (de) | Verfahren zur Herstellung von Pentachlorphenol |