DE1543173C3 - Verfahren zur Herstellung und Gewinnung von Propenoxid, Essigsäure und anderen wertvollen Oxidationsprodukten - Google Patents

Verfahren zur Herstellung und Gewinnung von Propenoxid, Essigsäure und anderen wertvollen Oxidationsprodukten

Info

Publication number
DE1543173C3
DE1543173C3 DE1543173A DE1543173A DE1543173C3 DE 1543173 C3 DE1543173 C3 DE 1543173C3 DE 1543173 A DE1543173 A DE 1543173A DE 1543173 A DE1543173 A DE 1543173A DE 1543173 C3 DE1543173 C3 DE 1543173C3
Authority
DE
Germany
Prior art keywords
propene
solvent
product
column
oxidation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE1543173A
Other languages
German (de)
English (en)
Other versions
DE1543173A1 (de
DE1543173B2 (de
Inventor
Robert Christie Dayton Ohio Binning
Harold Raymond Florissant Null
Stanley Lyle Creve Coeur Reid
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Monsanto Co
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Co filed Critical Monsanto Co
Publication of DE1543173A1 publication Critical patent/DE1543173A1/de
Publication of DE1543173B2 publication Critical patent/DE1543173B2/de
Application granted granted Critical
Publication of DE1543173C3 publication Critical patent/DE1543173C3/de
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
    • C07D295/027—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements containing only one hetero ring
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/06—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the liquid phase
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/32—Separation; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Epoxy Compounds (AREA)
DE1543173A 1964-02-12 1965-02-11 Verfahren zur Herstellung und Gewinnung von Propenoxid, Essigsäure und anderen wertvollen Oxidationsprodukten Expired DE1543173C3 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US344222A US3337620A (en) 1964-02-12 1964-02-12 Preparation and recovery of acetic acid
US344389A US3350416A (en) 1964-02-12 1964-02-12 Production and recovery of oxygenated hydrocarbons by plural distillation
US344366A US3350415A (en) 1964-02-12 1964-02-12 Production and recovery of oxygenated hydrocarbons by plural distillation

Publications (3)

Publication Number Publication Date
DE1543173A1 DE1543173A1 (de) 1969-07-31
DE1543173B2 DE1543173B2 (de) 1975-01-09
DE1543173C3 true DE1543173C3 (de) 1975-08-21

Family

ID=27407601

Family Applications (2)

Application Number Title Priority Date Filing Date
DE1543173A Expired DE1543173C3 (de) 1964-02-12 1965-02-11 Verfahren zur Herstellung und Gewinnung von Propenoxid, Essigsäure und anderen wertvollen Oxidationsprodukten
DE19651543175 Withdrawn DE1543175A1 (de) 1964-02-12 1965-02-11 Verfahren zur Erzeugung von Essigsaeure

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE19651543175 Withdrawn DE1543175A1 (de) 1964-02-12 1965-02-11 Verfahren zur Erzeugung von Essigsaeure

Country Status (8)

Country Link
US (3) US3350416A (enExample)
AT (3) AT277192B (enExample)
BE (1) BE659660A (enExample)
DE (2) DE1543173C3 (enExample)
GB (2) GB1082572A (enExample)
IL (2) IL22967A (enExample)
LU (1) LU47979A1 (enExample)
NL (2) NL144574B (enExample)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3464897A (en) * 1967-06-02 1969-09-02 Atlantic Richfield Co Separation of propylene oxide from other hydrocarbons
DE2225657C2 (de) * 1972-05-26 1974-05-22 Basf Ag, 6700 Ludwigshafen Verfahren zur Gewinnung von Propylenoxid
US3923882A (en) * 1974-04-17 1975-12-02 Union Carbide Corp Production of acetic acid
JPS606687B2 (ja) * 1977-10-26 1985-02-20 株式会社日本触媒 ガス混合方法およびガス混合装置
US5094724A (en) * 1991-04-19 1992-03-10 Lloyd Berg Separation of methylene chloride from the lower formates by extractive distillation
KR20170023804A (ko) * 2014-06-20 2017-03-06 비피 케미칼즈 리미티드 메틸 아세테이트 혼합물의 정제 방법
CN107488464B (zh) * 2017-04-27 2019-04-30 中国石油大学(北京) 一种超清洁高辛烷值汽油的生产方法及生产系统
WO2019105451A1 (zh) * 2017-11-30 2019-06-06 中国石油化工股份有限公司 一种环氧烷烃生产方法和生产系统

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3153058A (en) * 1964-10-13 Direct oxidation of olefins in a solvent
US1534752A (en) * 1920-05-21 1925-04-21 Carbide & Carbon Chem Corp Production of glycol esters
US1813636A (en) * 1928-02-07 1931-07-07 Ig Farbenindustrie Ag Process of separating formic acid from acetic acid
US2224984A (en) * 1936-08-19 1940-12-17 Armour & Co Fatty acid distillation
US2627489A (en) * 1949-01-11 1953-02-03 Nathan L Drake Insect repellents
US2985668A (en) * 1957-01-30 1961-05-23 Shingu Haruo Preparation of olefin oxides
US3071601A (en) * 1957-04-05 1963-01-01 Robert S Aries Oxidation of propylene
US3024170A (en) * 1959-06-15 1962-03-06 Donald F Othmer Process of azeotropic distillation of formic acid from acetic acid

Also Published As

Publication number Publication date
BE659660A (enExample) 1965-08-12
DE1543175A1 (de) 1969-07-31
DE1543173A1 (de) 1969-07-31
NL6501797A (enExample) 1965-08-13
US3350415A (en) 1967-10-31
GB1082572A (en) 1967-09-06
AT292650B (de) 1971-09-10
US3337620A (en) 1967-08-22
US3350416A (en) 1967-10-31
NL6501794A (enExample) 1965-08-13
LU47979A1 (enExample) 1965-08-12
IL22967A (en) 1968-12-26
AT291209B (de) 1971-07-12
NL144574B (nl) 1975-01-15
DE1543173B2 (de) 1975-01-09
GB1097134A (en) 1967-12-29
IL22966A (en) 1968-11-27
AT277192B (de) 1969-12-10

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Legal Events

Date Code Title Description
SH Request for examination between 03.10.1968 and 22.04.1971
C3 Grant after two publication steps (3rd publication)
E77 Valid patent as to the heymanns-index 1977
EHJ Ceased/non-payment of the annual fee