DE1271695B - Verfahren zur Herstellung von 2, 2, 3, 3-Tetrachlorbutan - Google Patents
Verfahren zur Herstellung von 2, 2, 3, 3-TetrachlorbutanInfo
- Publication number
- DE1271695B DE1271695B DEP1271A DE1271695A DE1271695B DE 1271695 B DE1271695 B DE 1271695B DE P1271 A DEP1271 A DE P1271A DE 1271695 A DE1271695 A DE 1271695A DE 1271695 B DE1271695 B DE 1271695B
- Authority
- DE
- Germany
- Prior art keywords
- tetrachlorobutane
- chlorine
- trichlorobutane
- chlorobutane
- hydrogen chloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- WSPZFVOCHITLIY-UHFFFAOYSA-N 2,2,3,3-tetrachlorobutane Chemical compound CC(Cl)(Cl)C(C)(Cl)Cl WSPZFVOCHITLIY-UHFFFAOYSA-N 0.000 title claims description 24
- 238000000034 method Methods 0.000 title claims description 16
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- UNTJXPFYXVCMFE-UHFFFAOYSA-N 2,2,3-trichlorobutane Chemical compound CC(Cl)C(C)(Cl)Cl UNTJXPFYXVCMFE-UHFFFAOYSA-N 0.000 claims description 14
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 12
- 239000000460 chlorine Substances 0.000 claims description 12
- 229910052801 chlorine Inorganic materials 0.000 claims description 12
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 9
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 9
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 8
- 238000006243 chemical reaction Methods 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 6
- 238000005660 chlorination reaction Methods 0.000 claims description 5
- 239000013078 crystal Substances 0.000 claims description 4
- 238000003776 cleavage reaction Methods 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 239000000706 filtrate Substances 0.000 claims description 2
- 230000007017 scission Effects 0.000 claims description 2
- VFWCMGCRMGJXDK-UHFFFAOYSA-N 1-chlorobutane Chemical group CCCCCl VFWCMGCRMGJXDK-UHFFFAOYSA-N 0.000 claims 4
- 238000006467 substitution reaction Methods 0.000 claims 2
- GEKSDZPTJSTVQV-UHFFFAOYSA-N 1-chlorobutane;hydrochloride Chemical compound Cl.CCCCCl GEKSDZPTJSTVQV-UHFFFAOYSA-N 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 239000011521 glass Substances 0.000 claims 1
- 239000005457 ice water Substances 0.000 claims 1
- 238000001556 precipitation Methods 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 238000003786 synthesis reaction Methods 0.000 claims 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 5
- UOCLXMDMGBRAIB-UHFFFAOYSA-N 1,1,1-trichloroethane Chemical compound CC(Cl)(Cl)Cl UOCLXMDMGBRAIB-UHFFFAOYSA-N 0.000 description 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- NGAAIHKWQFLRDY-UHFFFAOYSA-N 1,2,3,3-tetrachlorobutane Chemical compound CC(Cl)(Cl)C(Cl)CCl NGAAIHKWQFLRDY-UHFFFAOYSA-N 0.000 description 1
- IXZVKECRTHXEEW-UHFFFAOYSA-N 1,2,3,4-tetrachlorobutane Chemical compound ClCC(Cl)C(Cl)CCl IXZVKECRTHXEEW-UHFFFAOYSA-N 0.000 description 1
- LIFLRQVHKGGNSG-UHFFFAOYSA-N 2,3-dichlorobuta-1,3-diene Chemical compound ClC(=C)C(Cl)=C LIFLRQVHKGGNSG-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
- B01J19/122—Incoherent waves
- B01J19/123—Ultraviolet light
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEK0055910 | 1965-04-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1271695B true DE1271695B (de) | 1968-07-04 |
Family
ID=7227638
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEP1271A Pending DE1271695B (de) | 1965-04-24 | 1965-04-24 | Verfahren zur Herstellung von 2, 2, 3, 3-Tetrachlorbutan |
Country Status (7)
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2571901A (en) * | 1945-12-12 | 1951-10-16 | Niagara Alkali Company | Chlorinating process |
| US2459767A (en) * | 1946-03-19 | 1949-01-18 | Allied Chem & Dye Corp | Manufacture of chlorofluoro methanes |
-
1965
- 1965-04-24 DE DEP1271A patent/DE1271695B/de active Pending
-
1966
- 1966-03-29 US US538191A patent/US3413207A/en not_active Expired - Lifetime
- 1966-04-13 NL NL6604928A patent/NL6604928A/xx unknown
- 1966-04-14 FR FR57541A patent/FR1475581A/fr not_active Expired
- 1966-04-20 GB GB17265/66A patent/GB1085489A/en not_active Expired
- 1966-04-22 BE BE679911D patent/BE679911A/xx unknown
- 1966-04-22 AT AT380666A patent/AT260192B/de active
Also Published As
| Publication number | Publication date |
|---|---|
| NL6604928A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1966-10-25 |
| BE679911A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1966-10-03 |
| GB1085489A (en) | 1967-10-04 |
| US3413207A (en) | 1968-11-26 |
| FR1475581A (fr) | 1967-03-31 |
| AT260192B (de) | 1968-02-12 |
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