DE1063806B - Verfahren zur Herstellung polyvalenter makromolekularer Saeuren - Google Patents
Verfahren zur Herstellung polyvalenter makromolekularer SaeurenInfo
- Publication number
- DE1063806B DE1063806B DED27321A DED0027321A DE1063806B DE 1063806 B DE1063806 B DE 1063806B DE D27321 A DED27321 A DE D27321A DE D0027321 A DED0027321 A DE D0027321A DE 1063806 B DE1063806 B DE 1063806B
- Authority
- DE
- Germany
- Prior art keywords
- acids
- polyvalent
- production
- macromolecular
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002253 acid Substances 0.000 title claims description 13
- 150000007513 acids Chemical class 0.000 title claims description 12
- 238000000034 method Methods 0.000 title claims description 5
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 claims description 10
- 239000007800 oxidant agent Substances 0.000 claims description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 2
- 238000007254 oxidation reaction Methods 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims 2
- 239000003929 acidic solution Substances 0.000 claims 1
- 238000005349 anion exchange Methods 0.000 claims 1
- 150000001735 carboxylic acids Chemical class 0.000 claims 1
- 239000007789 gas Substances 0.000 claims 1
- 150000004965 peroxy acids Chemical class 0.000 claims 1
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 description 7
- 239000000243 solution Substances 0.000 description 6
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- YEJRWHAVMIAJKC-UHFFFAOYSA-N 4-Butyrolactone Chemical compound O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 description 2
- ZHNUHDYFZUAESO-UHFFFAOYSA-N Formamide Chemical compound NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 description 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000000502 dialysis Methods 0.000 description 2
- 238000004108 freeze drying Methods 0.000 description 2
- 239000012286 potassium permanganate Substances 0.000 description 2
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 2
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 2
- 238000004513 sizing Methods 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- 229920002845 Poly(methacrylic acid) Polymers 0.000 description 1
- 229920002873 Polyethylenimine Polymers 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- 150000001253 acrylic acids Chemical class 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 159000000009 barium salts Chemical class 0.000 description 1
- 159000000007 calcium salts Chemical class 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 150000001879 copper Chemical class 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229940046892 lead acetate Drugs 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000000123 paper Substances 0.000 description 1
- 229920000867 polyelectrolyte Polymers 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000007717 redox polymerization reaction Methods 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 229910001961 silver nitrate Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2/00—Addition polymers of aldehydes or cyclic oligomers thereof or of ketones; Addition copolymers thereof with less than 50 molar percent of other substances
- C08G2/30—Chemical modification by after-treatment
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/06—Oxidation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2/00—Addition polymers of aldehydes or cyclic oligomers thereof or of ketones; Addition copolymers thereof with less than 50 molar percent of other substances
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL234952D NL234952A (enrdf_load_stackoverflow) | 1958-01-31 | ||
| NL108917D NL108917C (enrdf_load_stackoverflow) | 1958-01-31 | ||
| US3127374D US3127374A (en) | 1958-01-31 | Process for the production of poly- | |
| DED27321A DE1063806B (de) | 1958-01-31 | 1958-01-31 | Verfahren zur Herstellung polyvalenter makromolekularer Saeuren |
| CH6759958A CH376667A (de) | 1958-01-31 | 1958-12-23 | Verfahren zur Herstellung polyvalenter makromolekularer Säuren |
| FR783658A FR1231054A (fr) | 1958-01-31 | 1959-01-09 | Procédé pour préparer des acides macromoléculaires polyvalents |
| GB3283/59A GB913766A (en) | 1958-01-31 | 1959-01-29 | Process for the production of polyvalent macromolecular acids |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DED27321A DE1063806B (de) | 1958-01-31 | 1958-01-31 | Verfahren zur Herstellung polyvalenter makromolekularer Saeuren |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1063806B true DE1063806B (de) | 1959-08-20 |
Family
ID=7039209
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DED27321A Pending DE1063806B (de) | 1958-01-31 | 1958-01-31 | Verfahren zur Herstellung polyvalenter makromolekularer Saeuren |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3127374A (enrdf_load_stackoverflow) |
| CH (1) | CH376667A (enrdf_load_stackoverflow) |
| DE (1) | DE1063806B (enrdf_load_stackoverflow) |
| FR (1) | FR1231054A (enrdf_load_stackoverflow) |
| GB (1) | GB913766A (enrdf_load_stackoverflow) |
| NL (2) | NL234952A (enrdf_load_stackoverflow) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR88792E (enrdf_load_stackoverflow) * | 1964-07-22 | 1967-06-07 | ||
| US3379688A (en) * | 1965-04-07 | 1968-04-23 | Dynamit Nobel Ag | Process for the manufacture of waterinsoluble polysulfonic acids on the basis of acrolein polymers and copolymers |
| CH985766D (enrdf_load_stackoverflow) * | 1965-07-16 | |||
| DE1570494A1 (de) * | 1965-12-24 | 1970-03-12 | Dynamit Nobel Ag | Verfahren zur Polymerisation von Akroleinen |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR554555A (fr) * | 1921-08-27 | 1923-06-13 | Consortium Elektrochem Ind | Procédé de préparation d'une résine artificielle égalant la gomme-laque naturelle |
| US2789099A (en) * | 1953-09-04 | 1957-04-16 | Union Carbide & Carbon Corp | Polymerization of acrylic acid in aqueous solution |
| NL99604C (enrdf_load_stackoverflow) * | 1955-03-23 |
-
0
- NL NL108917D patent/NL108917C/xx active
- NL NL234952D patent/NL234952A/xx unknown
- US US3127374D patent/US3127374A/en not_active Expired - Lifetime
-
1958
- 1958-01-31 DE DED27321A patent/DE1063806B/de active Pending
- 1958-12-23 CH CH6759958A patent/CH376667A/de unknown
-
1959
- 1959-01-09 FR FR783658A patent/FR1231054A/fr not_active Expired
- 1959-01-29 GB GB3283/59A patent/GB913766A/en not_active Expired
Non-Patent Citations (1)
| Title |
|---|
| None * |
Also Published As
| Publication number | Publication date |
|---|---|
| NL108917C (enrdf_load_stackoverflow) | |
| US3127374A (en) | 1964-03-31 |
| FR1231054A (fr) | 1960-09-26 |
| GB913766A (en) | 1962-12-28 |
| CH376667A (de) | 1964-04-15 |
| NL234952A (enrdf_load_stackoverflow) |
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