DE10352261B4 - Verfahren zur Herstellung von TCD-Dialdehyd - Google Patents

Verfahren zur Herstellung von TCD-Dialdehyd Download PDF

Info

Publication number
DE10352261B4
DE10352261B4 DE10352261A DE10352261A DE10352261B4 DE 10352261 B4 DE10352261 B4 DE 10352261B4 DE 10352261 A DE10352261 A DE 10352261A DE 10352261 A DE10352261 A DE 10352261A DE 10352261 B4 DE10352261 B4 DE 10352261B4
Authority
DE
Germany
Prior art keywords
rhodium
hydroformylation
tcd
reaction
ppm
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE10352261A
Other languages
German (de)
English (en)
Other versions
DE10352261A1 (de
Inventor
Peter Dr. Lappe
Helmut Springer
Rainer Dr. Lukas
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Oxea GmbH
Original Assignee
Celanese Chemicals Europe GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Celanese Chemicals Europe GmbH filed Critical Celanese Chemicals Europe GmbH
Priority to DE10352261A priority Critical patent/DE10352261B4/de
Priority to US10/967,731 priority patent/US7015362B2/en
Priority to DE502004003450T priority patent/DE502004003450D1/de
Priority to EP04025483A priority patent/EP1529769B8/de
Priority to AT04025483T priority patent/ATE359255T1/de
Priority to CNB2004100871935A priority patent/CN100441558C/zh
Priority to JP2004321212A priority patent/JP4681273B2/ja
Priority to KR1020040089633A priority patent/KR101110085B1/ko
Publication of DE10352261A1 publication Critical patent/DE10352261A1/de
Application granted granted Critical
Publication of DE10352261B4 publication Critical patent/DE10352261B4/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00—Compounds having —CHO groups
    • C07C47/28—Saturated compounds having —CHO groups bound to carbon atoms of rings other than six—membered aromatic rings
    • C07C47/34—Saturated compounds having —CHO groups bound to carbon atoms of rings other than six—membered aromatic rings polycyclic
    • C07C47/347—Saturated compounds having —CHO groups bound to carbon atoms of rings other than six—membered aromatic rings polycyclic having a —CHO group on a condensed ring system
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/49—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide
    • C07C45/50—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide by oxo-reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/56—Ring systems containing bridged rings
    • C07C2603/58—Ring systems containing bridged rings containing three rings
    • C07C2603/60—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members
    • C07C2603/66—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members containing five-membered rings
    • C07C2603/68—Dicyclopentadienes; Hydrogenated dicyclopentadienes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Phenolic Resins Or Amino Resins (AREA)
DE10352261A 2003-11-08 2003-11-08 Verfahren zur Herstellung von TCD-Dialdehyd Expired - Fee Related DE10352261B4 (de)

Priority Applications (8)

Application Number Priority Date Filing Date Title
DE10352261A DE10352261B4 (de) 2003-11-08 2003-11-08 Verfahren zur Herstellung von TCD-Dialdehyd
US10/967,731 US7015362B2 (en) 2003-11-08 2004-10-18 Process for preparing TCD-dialdehyde
EP04025483A EP1529769B8 (de) 2003-11-08 2004-10-27 Verfahren zur Herstellung von TCD-Dialdehyd
AT04025483T ATE359255T1 (de) 2003-11-08 2004-10-27 Verfahren zur herstellung von tcd-dialdehyd
DE502004003450T DE502004003450D1 (de) 2003-11-08 2004-10-27 Verfahren zur Herstellung von TCD-Dialdehyd
CNB2004100871935A CN100441558C (zh) 2003-11-08 2004-11-04 Tcd-二醛的制备方法
JP2004321212A JP4681273B2 (ja) 2003-11-08 2004-11-04 Ｔｃｄ−ジアルデヒドの製造方法
KR1020040089633A KR101110085B1 (ko) 2003-11-08 2004-11-05 Ｔｃｄ-디알데히드의 제조방법

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10352261A DE10352261B4 (de) 2003-11-08 2003-11-08 Verfahren zur Herstellung von TCD-Dialdehyd

Publications (2)

Publication Number Publication Date
DE10352261A1 DE10352261A1 (de) 2005-06-16
DE10352261B4 true DE10352261B4 (de) 2006-08-24

Family

ID=34428625

Family Applications (2)

Application Number Title Priority Date Filing Date
DE10352261A Expired - Fee Related DE10352261B4 (de) 2003-11-08 2003-11-08 Verfahren zur Herstellung von TCD-Dialdehyd
DE502004003450T Expired - Fee Related DE502004003450D1 (de) 2003-11-08 2004-10-27 Verfahren zur Herstellung von TCD-Dialdehyd

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE502004003450T Expired - Fee Related DE502004003450D1 (de) 2003-11-08 2004-10-27 Verfahren zur Herstellung von TCD-Dialdehyd

Country Status (7)

Country Link
US (1) US7015362B2 (enExample)
EP (1) EP1529769B8 (enExample)
JP (1) JP4681273B2 (enExample)
KR (1) KR101110085B1 (enExample)
CN (1) CN100441558C (enExample)
AT (1) ATE359255T1 (enExample)
DE (2) DE10352261B4 (enExample)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006030557A1 (de) * 2006-07-03 2008-01-10 Celanese Emulsions Gmbh Verfahren zur Herstellung wässriger Vinylester-Dispersionen
DE102007012247A1 (de) * 2007-03-14 2008-09-25 Celanese Emulsions Gmbh Vernetzbare Polymerdispersionen, Verfahren zu deren Herstellung und Verwendung
CN100496736C (zh) * 2007-05-31 2009-06-10 南京大学 一种用于双环戊二烯氢甲酰化制醛的水溶性配体铑配合物催化剂
DE102007028917A1 (de) 2007-06-22 2008-12-24 Celanese Emulsions Gmbh Vernetzbare Polymerdispersionen, Beschichtungsmittel enthaltend diese und deren Verwendung
DE102007033596A1 (de) * 2007-07-19 2009-01-22 Celanese Emulsions Gmbh Beschichtungsmittel mit hoher Bewitterungsbeständigkeit, Verfahren zu deren Herstellung und deren Verwendung
DE102007033595A1 (de) * 2007-07-19 2009-01-22 Celanese Emulsions Gmbh Polyvinylesterdispersionen, Verfahren zu deren Herstellung und deren Verwendung
TWI361181B (en) * 2007-12-31 2012-04-01 Ind Tech Res Inst A hydroformylation process
CN101497561B (zh) * 2008-01-29 2015-03-18 财团法人工业技术研究院 氢甲酰化制程
US20100069679A1 (en) * 2008-09-12 2010-03-18 Eastman Chemical Company Acetylene tolerant hydroformylation catalysts
US8664341B2 (en) * 2010-04-29 2014-03-04 Dow Global Technologies, Llc Vinylbenzyl ethers of polycyclopentadiene polyphenol
CN102139229B (zh) * 2011-01-19 2012-10-10 华东师范大学 一种负载型金催化剂的制备方法及其应用
CN102617311B (zh) * 2012-02-27 2014-01-08 中国科学院新疆理化技术研究所 一种合成三环癸烷不饱和单醛的方法
KR102712499B1 (ko) 2018-06-15 2024-10-02 에스케이케미칼 주식회사 3(4),8(9)-비스포밀트리사이클로[5.2.1.0^2,6]데칸의 제조방법
EP3808728B1 (en) * 2018-06-15 2025-10-22 SK Chemicals Co., Ltd. Method for preparing 3(4),8(9)-bisformyltricyclo[5.2.1.0 ²,6]decane
US10538472B1 (en) 2019-02-14 2020-01-21 Dairen Chemical Corporation Extraction process for high-boiling aldehyde product separation and catalyst recovery
EP4008710B1 (de) * 2020-12-04 2024-05-01 OQ Chemicals GmbH Verfahren zur hydroformylierung von olefinen in homogener phase
EP4008709B1 (de) * 2020-12-04 2024-05-01 OQ Chemicals GmbH Verfahren zur herstellung polyzyklischer aliphatischer dialdehyde
US11801504B2 (en) 2021-12-30 2023-10-31 Industrial Technology Research Institute Hydrophilic phosphorus ligand and method for separation and recovery of catalyst
EP4303208A1 (de) * 2022-07-06 2024-01-10 Evonik Oxeno GmbH & Co. KG Verfahren zur herstellung von dicidal

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0186075B1 (de) * 1984-12-22 1990-02-28 Hoechst Aktiengesellschaft Verfahren zur Herstellung von 8- und 9-Formyl-tricyclo-(5,2,1,0, 2,6)-decen-3
DE3822038A1 (de) * 1988-06-30 1990-03-01 Hoechst Ag Verfahren zur herstellung von 3(4),8(9)-bis-(aminomethyl)-tricyclo (5.2.1.0(pfeil hoch)2(pfeil hoch)(pfeil hoch),(pfeil hoch)(pfeil hoch)6(pfeil hoch))-decan
EP0571819A1 (de) * 1992-05-29 1993-12-01 Hoechst Aktiengesellschaft Sulfonierte 2,2'-Bis(diphenylphosphinomethyl)-1,1'binaphthaline, Verfahren zu ihrer Herstellung und ihre Verwendung in einem Verfahren zur Hydroformylierung vonolefinisch ungesättigten Verbindungen
DE4427428A1 (de) * 1994-08-03 1996-02-29 Basf Ag Verfahren zur Herstellung von Aldehyden

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3527809A (en) * 1967-08-03 1970-09-08 Union Carbide Corp Hydroformylation process
US4148830A (en) * 1975-03-07 1979-04-10 Union Carbide Corporation Hydroformylation of olefins
DE2928313A1 (de) 1979-07-13 1981-02-05 Ruhrchemie Ag Verfahren zur herstellung von 3-(4)- formyltricyclo- eckige klammer auf 5,2,1, 0 hoch 2,6 eckige klammer zu -decen-8
JPS5630938A (en) * 1979-08-23 1981-03-28 Mitsubishi Petrochem Co Ltd Preparation of tricyclodecanedialdehyde
US4283562A (en) * 1979-10-26 1981-08-11 Union Carbide Corporation Hydroformylation process using stable rhodium catalyst
JPS5821638A (ja) * 1981-07-31 1983-02-08 Mitsubishi Petrochem Co Ltd ジアルデヒド類の製造方法
DE4135049A1 (de) * 1991-10-24 1993-05-06 Hoechst Ag, 6230 Frankfurt, De Verfahren zur rueckgewinnung von rhodium aus den reaktionsprodukten der oxosynthese
DE19619527A1 (de) 1996-05-15 1997-11-20 Hoechst Ag Katalysatorsysteme auf der Basis von Rhodium-Komplexverbindungen mit Diphosphin-Liganden und ihre Verwendung bei der Herstellung von Aldehyden
EP1065194B2 (en) * 1999-07-02 2007-03-28 Mitsubishi Gas Chemical Company, Inc. Production of tricyclodecane dicarbaldehyde, pentacyclopentadecane dicarbaldehyde and corresponding dimethanols
JP2003146931A (ja) * 2001-11-14 2003-05-21 Mitsubishi Gas Chem Co Inc トリシクロデカンジカルバルデヒドおよびペンタシクロペンタデカンジカルバルデヒドの製造方法
JP4153221B2 (ja) * 2002-03-01 2008-09-24 丸善石油化学株式会社 環状ジカルバルデヒドの精製方法
JP4101534B2 (ja) * 2002-03-04 2008-06-18 丸善石油化学株式会社 第８族金属錯体触媒およびこれを利用するアルデヒドの製造方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0186075B1 (de) * 1984-12-22 1990-02-28 Hoechst Aktiengesellschaft Verfahren zur Herstellung von 8- und 9-Formyl-tricyclo-(5,2,1,0, 2,6)-decen-3
DE3822038A1 (de) * 1988-06-30 1990-03-01 Hoechst Ag Verfahren zur herstellung von 3(4),8(9)-bis-(aminomethyl)-tricyclo (5.2.1.0(pfeil hoch)2(pfeil hoch)(pfeil hoch),(pfeil hoch)(pfeil hoch)6(pfeil hoch))-decan
EP0571819A1 (de) * 1992-05-29 1993-12-01 Hoechst Aktiengesellschaft Sulfonierte 2,2'-Bis(diphenylphosphinomethyl)-1,1'binaphthaline, Verfahren zu ihrer Herstellung und ihre Verwendung in einem Verfahren zur Hydroformylierung vonolefinisch ungesättigten Verbindungen
DE4427428A1 (de) * 1994-08-03 1996-02-29 Basf Ag Verfahren zur Herstellung von Aldehyden

Also Published As

Publication number Publication date
DE502004003450D1 (de) 2007-05-24
US7015362B2 (en) 2006-03-21
CN1636955A (zh) 2005-07-13
JP2005139181A (ja) 2005-06-02
EP1529769A1 (de) 2005-05-11
EP1529769B8 (de) 2007-08-29
CN100441558C (zh) 2008-12-10
DE10352261A1 (de) 2005-06-16
EP1529769B1 (de) 2007-04-11
KR101110085B1 (ko) 2012-02-17
ATE359255T1 (de) 2007-05-15
KR20050044845A (ko) 2005-05-13
JP4681273B2 (ja) 2011-05-11
US20050101805A1 (en) 2005-05-12

Similar Documents

Publication Publication Date Title
DE10352260B3 (de) Verfahren zur Herstellung von TCD-Alkohol DM
DE10352261B4 (de) Verfahren zur Herstellung von TCD-Dialdehyd
EP0163234B1 (de) Verfahren zur Herstellung von Aldehyden
DE10108475A1 (de) Verfahren zur Herstellung von Aldehyden
EP0805138A1 (de) Verfahren zur Hydroformylierung olefinisch ungesättigter Verbindungen
DE102004027955B3 (de) Verfahren zur Herstellung TCD-Alkohol DM
EP2318349B1 (de) Verfahren zur gewinnung von aliphatischen c3- bis c-10-aldehyden aus hochsiedenden stoffen mitels thermischer verfahren
WO2002068369A1 (de) Verfahren zur herstellung von aldehyden
EP0216314B1 (de) Verfahren zur Herstellung von Nonadecandiolen
DE10352258B4 (de) Verfahren zur Herstellung von TCD-Diamin
DE10352263A1 (de) Verfahren zur Herstellung von TCD-Monenal
EP1813587A1 (de) 3(4),7(8)-Dihydroxymethyl-bicyclo[4.3.0] nonan und ein Verfahren zu seiner Herstellung
EP0186075B1 (de) Verfahren zur Herstellung von 8- und 9-Formyl-tricyclo-(5,2,1,0, 2,6)-decen-3
DE102006004317B4 (de) 3(4),7(8)-Bisformyl-bicyclo[4.3.0]nonan und ein Verfahren zu seiner Herstellung
EP1813595A1 (de) "3(4),7(8)-Bis (aminomethyl)-bicyclo[4.3.0] nonan und ein Verfahren zu seiner Herstellung
DE10205835B4 (de) Verfahren zur Herstellung von Terpinolenaldehyd
EP0173226B1 (de) Verfahren zur Herstellung von beta-Formylpropionsäure-tert.-butylester
DE102005019237B4 (de) Verfahren zur Hydroformylierung von substituierten Allylbenzolen
DE19612814C2 (de) Verfahren zur Herstellung kalamithischer Acylcyclohexane
WO1997049490A1 (de) Katalysator und ein verfahren zur herstellung von aldehyden in gegenwart dieses katalysators
DE102006025813A1 (de) 3(4)-Aminomethyl-8(9)-hydroxy-tricyclo[5.2.1.02,6]decan und ein Verfahren zu seiner Herstellung
DE102006004316A1 (de) Gemisch enthaltend 7(8)-Formyl-bicyclo[4.3.0]non-3-en und 3(4)-Formyl-bicyclo[4.3.0]non-7-en sowie ein Verfahren zu seiner Herstellung

Legal Events

Date Code Title Description
OP8 Request for examination as to paragraph 44 patent law
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: OXEA DEUTSCHLAND GMBH, 46147 OBERHAUSEN, DE

8327 Change in the person/name/address of the patent owner

Owner name: OXEA GMBH, 46147 OBERHAUSEN, DE

R081 Change of applicant/patentee

Owner name: OXEA GMBH, DE

Free format text: FORMER OWNER: OXEA DEUTSCHLAND GMBH, 46147 OBERHAUSEN, DE

Effective date: 20110315

R081 Change of applicant/patentee

Owner name: OQ CHEMICALS GMBH, DE

Free format text: FORMER OWNER: OXEA GMBH, 46147 OBERHAUSEN, DE

R119 Application deemed withdrawn, or ip right lapsed, due to non-payment of renewal fee