CN100441558C - Tcd-二醛的制备方法 - Google Patents

Tcd-二醛的制备方法 Download PDF

Info

Publication number
CN100441558C
CN100441558C CNB2004100871935A CN200410087193A CN100441558C CN 100441558 C CN100441558 C CN 100441558C CN B2004100871935 A CNB2004100871935 A CN B2004100871935A CN 200410087193 A CN200410087193 A CN 200410087193A CN 100441558 C CN100441558 C CN 100441558C
Authority
CN
China
Prior art keywords
rhodium
compound
hydroformylation step
iii
hydroformylation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB2004100871935A
Other languages
English (en)
Chinese (zh)
Other versions
CN1636955A (zh
Inventor
P·拉普
H·斯普林格
R·卢卡斯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Oxea GmbH
Original Assignee
Oxea Deutschland GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Oxea Deutschland GmbH filed Critical Oxea Deutschland GmbH
Publication of CN1636955A publication Critical patent/CN1636955A/zh
Application granted granted Critical
Publication of CN100441558C publication Critical patent/CN100441558C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78Separation; Purification; Stabilisation; Use of additives
    • C07C45/81Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00Compounds having —CHO groups
    • C07C47/28Saturated compounds having —CHO groups bound to carbon atoms of rings other than six—membered aromatic rings
    • C07C47/34Saturated compounds having —CHO groups bound to carbon atoms of rings other than six—membered aromatic rings polycyclic
    • C07C47/347Saturated compounds having —CHO groups bound to carbon atoms of rings other than six—membered aromatic rings polycyclic having a —CHO group on a condensed ring system
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/49Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide
    • C07C45/50Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide by oxo-reactions
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00Systems containing at least three condensed rings
    • C07C2603/56Ring systems containing bridged rings
    • C07C2603/58Ring systems containing bridged rings containing three rings
    • C07C2603/60Ring systems containing bridged rings containing three rings containing at least one ring with less than six members
    • C07C2603/66Ring systems containing bridged rings containing three rings containing at least one ring with less than six members containing five-membered rings
    • C07C2603/68Dicyclopentadienes; Hydrogenated dicyclopentadienes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Phenolic Resins Or Amino Resins (AREA)
CNB2004100871935A 2003-11-08 2004-11-04 Tcd-二醛的制备方法 Expired - Fee Related CN100441558C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10352261A DE10352261B4 (de) 2003-11-08 2003-11-08 Verfahren zur Herstellung von TCD-Dialdehyd
DE10352261.1 2003-11-08

Publications (2)

Publication Number Publication Date
CN1636955A CN1636955A (zh) 2005-07-13
CN100441558C true CN100441558C (zh) 2008-12-10

Family

ID=34428625

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB2004100871935A Expired - Fee Related CN100441558C (zh) 2003-11-08 2004-11-04 Tcd-二醛的制备方法

Country Status (7)

Country Link
US (1) US7015362B2 (enExample)
EP (1) EP1529769B8 (enExample)
JP (1) JP4681273B2 (enExample)
KR (1) KR101110085B1 (enExample)
CN (1) CN100441558C (enExample)
AT (1) ATE359255T1 (enExample)
DE (2) DE10352261B4 (enExample)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102006030557A1 (de) * 2006-07-03 2008-01-10 Celanese Emulsions Gmbh Verfahren zur Herstellung wässriger Vinylester-Dispersionen
DE102007012247A1 (de) * 2007-03-14 2008-09-25 Celanese Emulsions Gmbh Vernetzbare Polymerdispersionen, Verfahren zu deren Herstellung und Verwendung
CN100496736C (zh) * 2007-05-31 2009-06-10 南京大学 一种用于双环戊二烯氢甲酰化制醛的水溶性配体铑配合物催化剂
DE102007028917A1 (de) 2007-06-22 2008-12-24 Celanese Emulsions Gmbh Vernetzbare Polymerdispersionen, Beschichtungsmittel enthaltend diese und deren Verwendung
DE102007033595A1 (de) * 2007-07-19 2009-01-22 Celanese Emulsions Gmbh Polyvinylesterdispersionen, Verfahren zu deren Herstellung und deren Verwendung
DE102007033596A1 (de) * 2007-07-19 2009-01-22 Celanese Emulsions Gmbh Beschichtungsmittel mit hoher Bewitterungsbeständigkeit, Verfahren zu deren Herstellung und deren Verwendung
TWI361181B (en) * 2007-12-31 2012-04-01 Ind Tech Res Inst A hydroformylation process
CN101497561B (zh) * 2008-01-29 2015-03-18 财团法人工业技术研究院 氢甲酰化制程
US20100069679A1 (en) * 2008-09-12 2010-03-18 Eastman Chemical Company Acetylene tolerant hydroformylation catalysts
KR20130079413A (ko) * 2010-04-29 2013-07-10 다우 글로벌 테크놀로지스 엘엘씨 폴리시클로펜타디엔 폴리페놀의 비닐벤질 에테르
CN102139229B (zh) * 2011-01-19 2012-10-10 华东师范大学 一种负载型金催化剂的制备方法及其应用
CN102617311B (zh) * 2012-02-27 2014-01-08 中国科学院新疆理化技术研究所 一种合成三环癸烷不饱和单醛的方法
KR102712499B1 (ko) * 2018-06-15 2024-10-02 에스케이케미칼 주식회사 3(4),8(9)-비스포밀트리사이클로[5.2.1.0^2,6]데칸의 제조방법
EP3808728B1 (en) * 2018-06-15 2025-10-22 SK Chemicals Co., Ltd. Method for preparing 3(4),8(9)-bisformyltricyclo[5.2.1.0 ²,6]decane
US10538472B1 (en) 2019-02-14 2020-01-21 Dairen Chemical Corporation Extraction process for high-boiling aldehyde product separation and catalyst recovery
EP4008710B1 (de) * 2020-12-04 2024-05-01 OQ Chemicals GmbH Verfahren zur hydroformylierung von olefinen in homogener phase
EP4008709B1 (de) * 2020-12-04 2024-05-01 OQ Chemicals GmbH Verfahren zur herstellung polyzyklischer aliphatischer dialdehyde
US11801504B2 (en) 2021-12-30 2023-10-31 Industrial Technology Research Institute Hydrophilic phosphorus ligand and method for separation and recovery of catalyst
EP4303208A1 (de) * 2022-07-06 2024-01-10 Evonik Oxeno GmbH & Co. KG Verfahren zur herstellung von dicidal

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1065194A1 (en) * 1999-07-02 2001-01-03 Mitsubishi Gas Chemical Company, Inc. Production of tricyclodecane dicarbaldehyde, pentacyclopentadecane dicarbaldehyde and corresponding dimethanols

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3527809A (en) * 1967-08-03 1970-09-08 Union Carbide Corp Hydroformylation process
US4148830A (en) * 1975-03-07 1979-04-10 Union Carbide Corporation Hydroformylation of olefins
DE2928313A1 (de) 1979-07-13 1981-02-05 Ruhrchemie Ag Verfahren zur herstellung von 3-(4)- formyltricyclo- eckige klammer auf 5,2,1, 0 hoch 2,6 eckige klammer zu -decen-8
JPS5630938A (en) * 1979-08-23 1981-03-28 Mitsubishi Petrochem Co Ltd Preparation of tricyclodecanedialdehyde
US4283562A (en) * 1979-10-26 1981-08-11 Union Carbide Corporation Hydroformylation process using stable rhodium catalyst
JPS5821638A (ja) * 1981-07-31 1983-02-08 Mitsubishi Petrochem Co Ltd ジアルデヒド類の製造方法
DE3447030A1 (de) * 1984-12-22 1986-07-03 Ruhrchemie Ag, 4200 Oberhausen Verfahren zur herstellung von 8- und 9-formyl-tricyclo (5,2,1,0(pfeil hoch)2(pfeil hoch)(pfeil hoch),(pfeil hoch)(pfeil hoch)6(pfeil hoch))-decen-8
DE3822038A1 (de) 1988-06-30 1990-03-01 Hoechst Ag Verfahren zur herstellung von 3(4),8(9)-bis-(aminomethyl)-tricyclo (5.2.1.0(pfeil hoch)2(pfeil hoch)(pfeil hoch),(pfeil hoch)(pfeil hoch)6(pfeil hoch))-decan
DE4135049A1 (de) * 1991-10-24 1993-05-06 Hoechst Ag, 6230 Frankfurt, De Verfahren zur rueckgewinnung von rhodium aus den reaktionsprodukten der oxosynthese
TW225485B (enExample) * 1992-05-29 1994-06-21 Hoechst Ag
DE4427428A1 (de) * 1994-08-03 1996-02-29 Basf Ag Verfahren zur Herstellung von Aldehyden
DE19619527A1 (de) 1996-05-15 1997-11-20 Hoechst Ag Katalysatorsysteme auf der Basis von Rhodium-Komplexverbindungen mit Diphosphin-Liganden und ihre Verwendung bei der Herstellung von Aldehyden
JP2003146931A (ja) * 2001-11-14 2003-05-21 Mitsubishi Gas Chem Co Inc トリシクロデカンジカルバルデヒドおよびペンタシクロペンタデカンジカルバルデヒドの製造方法
JP4153221B2 (ja) * 2002-03-01 2008-09-24 丸善石油化学株式会社 環状ジカルバルデヒドの精製方法
JP4101534B2 (ja) * 2002-03-04 2008-06-18 丸善石油化学株式会社 第8族金属錯体触媒およびこれを利用するアルデヒドの製造方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1065194A1 (en) * 1999-07-02 2001-01-03 Mitsubishi Gas Chemical Company, Inc. Production of tricyclodecane dicarbaldehyde, pentacyclopentadecane dicarbaldehyde and corresponding dimethanols
US6365782B1 (en) * 1999-07-02 2002-04-02 Mitsbushi Gas Chemical Company, Inc. Production of tricyclodecane dicarbaldehyde, pentacyclopentadecane dicarbaldehyde and corresponding dimethanols

Also Published As

Publication number Publication date
JP2005139181A (ja) 2005-06-02
CN1636955A (zh) 2005-07-13
US7015362B2 (en) 2006-03-21
ATE359255T1 (de) 2007-05-15
KR101110085B1 (ko) 2012-02-17
DE10352261B4 (de) 2006-08-24
JP4681273B2 (ja) 2011-05-11
EP1529769B1 (de) 2007-04-11
DE10352261A1 (de) 2005-06-16
US20050101805A1 (en) 2005-05-12
EP1529769A1 (de) 2005-05-11
DE502004003450D1 (de) 2007-05-24
KR20050044845A (ko) 2005-05-13
EP1529769B8 (de) 2007-08-29

Similar Documents

Publication Publication Date Title
CN100441558C (zh) Tcd-二醛的制备方法
CN100352794C (zh) Tcd-醇dm的制备方法
Herrmann et al. Homogeneously catalyzed 1, 3‐diene functionalization–A success story from laboratory to miniplant scale
JP5070208B2 (ja) ヒドロホルミル化方法
de Bellefon et al. Efficient catalytic isomerization of allylic alcohols to carbonyl compounds with water soluble rhodium complexes
US7301057B2 (en) Process for preparing TCD-alcohol DM
JP2672473B2 (ja) α−位においてアルキル残基により置換されたアルデヒドの製法
US4723047A (en) Process for the preparation of nonadecanediols
US7122706B2 (en) Process for preparing TCD-monenal
US11993566B2 (en) Hydroformylation method
KR102340629B1 (ko) 하이드로포밀화 반응용 헤테로 리간드 배위결합 촉매 조성물 및 이의 용도
US7317128B2 (en) Process for preparing TCD-diamine
TW202222759A (zh) 烯烴於均相中之氫甲醯化方法
JP2007204470A (ja) 3(4),7(8)−ジヒドロキシメチル−ビシクロ[4.3.0]ノナンおよびそれの製造方法
JP7791631B2 (ja) 多環式脂肪族ジアルデヒドの製造方法
Huan et al. Novel Ir-Complexes for Hydroformylation of Olefins with H2O as the Hydrogen Source
JP2007204472A (ja) 3(4),7(8)−ビス(アミノメチル)−ビシクロ[4.3.0]ノナンおよびそれの製造方法
van Leeuwen et al. Carbon monoxide as a chemical feedstock: carbonylation catalysis
KR20230115563A (ko) 알코올의 제조방법
JP2023552392A (ja) 多環式脂肪族ジアルデヒドの製造方法
KR20220015128A (ko) 알데히드의 제조방법 및 알코올의 제조방법
Du Toit Use of water-soluble phosphine ligands in heterogeneous hydroformylation catalysis: application to long-chain 1-alkenes
HK1081528B (en) Process for preparing tcd-alcohol dm

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
ASS Succession or assignment of patent right

Owner name: OXEA GERMANY CORP

Free format text: FORMER OWNER: CELANESE CHEM EUROPE GMBH

Effective date: 20070810

C41 Transfer of patent application or patent right or utility model
TA01 Transfer of patent application right

Effective date of registration: 20070810

Address after: Germany Oberhausen

Applicant after: OXEA DEUTSCHLAND GmbH

Address before: Cron Begg, Federal Republic of Germany

Applicant before: Celanese Chemicals Europe GmbH

C14 Grant of patent or utility model
GR01 Patent grant
ASS Succession or assignment of patent right

Owner name: OKS CO., LTD.

Free format text: FORMER OWNER: OKS GERMANY CO., LTD.

Effective date: 20100919

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20100919

Address after: Germany Oberhausen

Patentee after: OXEA GmbH

Address before: Germany Oberhausen

Patentee before: Oxea Deutschland GmbH

CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20081210

Termination date: 20211104

CF01 Termination of patent right due to non-payment of annual fee