DE10337198A1

DE10337198A1 - Träger auf Basis von Granulaten, die aus pyrogen hergestelltem Siliciumdioxiden hergestellt sind

Träger auf Basis von Granulaten, die aus pyrogen hergestelltem Siliciumdioxiden hergestellt sind Download PDF

Info

Publication number: DE10337198A1
Authority: DE; Germany
Prior art keywords: silica; granules; pyrogenic; pyrogenic silica; granulate
Prior art date: 2003-08-13
Legal status : Ceased

Application number

DE10337198A

Other languages

German (de)

English (en)

Inventor

Peter Dr. Neugebauer

Steffen Hasenzahl

Claus-Peter Dr. Drexel

Jürgen Dr. Meyer

Current Assignee

Evonik Operations GmbH

Original Assignee

Degussa GmbH

Priority date

2003-08-13

Filing date

2003-08-13

Publication date

2005-03-17

2003-08-13 Application filed by Degussa GmbH filed Critical Degussa GmbH

2003-08-13 Priority to DE10337198A priority Critical patent/DE10337198A1/de

2004-06-22 Priority to US10/568,012 priority patent/US20060229210A1/en

2004-06-22 Priority to PCT/EP2004/006719 priority patent/WO2005016823A1/en

2004-06-22 Priority to CNB2004800230417A priority patent/CN100384727C/zh

2004-06-22 Priority to JP2006522904A priority patent/JP2007501762A/ja

2004-06-22 Priority to KR1020067002992A priority patent/KR100863453B1/ko

2004-06-22 Priority to EP04740149A priority patent/EP1654197A1/en

2005-03-17 Publication of DE10337198A1 publication Critical patent/DE10337198A1/de

Status Ceased legal-status Critical Current

Links

239000008187 granular material Substances 0.000 title claims abstract description 82
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical class O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims description 97
235000012239 silicon dioxide Nutrition 0.000 title claims description 9
239000000969 carrier Substances 0.000 title 1
-1 alkalis Substances 0.000 claims abstract description 45
239000000126 substance Substances 0.000 claims abstract description 37
239000002253 acid Substances 0.000 claims abstract description 12
239000003381 stabilizer Substances 0.000 claims abstract description 12
239000003674 animal food additive Substances 0.000 claims abstract description 11
239000003963 antioxidant agent Substances 0.000 claims abstract description 11
239000003995 emulsifying agent Substances 0.000 claims abstract description 11
150000003839 salts Chemical class 0.000 claims abstract description 11
239000011230 binding agent Substances 0.000 claims abstract description 10
235000019264 food flavour enhancer Nutrition 0.000 claims abstract description 10
235000003599 food sweetener Nutrition 0.000 claims abstract description 10
239000003349 gelling agent Substances 0.000 claims abstract description 10
239000000543 intermediate Substances 0.000 claims abstract description 10
239000003755 preservative agent Substances 0.000 claims abstract description 10
239000003765 sweetening agent Substances 0.000 claims abstract description 10
239000002562 thickening agent Substances 0.000 claims abstract description 10
239000004097 EU approved flavor enhancer Substances 0.000 claims abstract description 9
150000007513 acids Chemical class 0.000 claims abstract description 9
239000001692 EU approved anti-caking agent Substances 0.000 claims abstract description 8
235000013373 food additive Nutrition 0.000 claims abstract description 8
239000002778 food additive Substances 0.000 claims abstract description 8
230000008719 thickening Effects 0.000 claims abstract description 8
239000000975 dye Substances 0.000 claims abstract description 6
229910021485 fumed silica Inorganic materials 0.000 claims description 45
239000000377 silicon dioxide Substances 0.000 claims description 45
239000002510 pyrogen Substances 0.000 claims description 23
239000002156 adsorbate Substances 0.000 claims description 18
239000003795 chemical substances by application Substances 0.000 claims description 11
239000000417 fungicide Substances 0.000 claims description 8
239000004009 herbicide Substances 0.000 claims description 8
239000002917 insecticide Substances 0.000 claims description 8
239000000796 flavoring agent Substances 0.000 claims description 5
235000019634 flavors Nutrition 0.000 claims description 5
239000004476 plant protection product Substances 0.000 claims description 5
230000001698 pyrogenic effect Effects 0.000 claims description 5
239000002585 base Substances 0.000 claims description 4
239000003086 colorant Substances 0.000 claims description 4
239000000575 pesticide Substances 0.000 claims description 4
239000003513 alkali Substances 0.000 claims description 3
230000003078 antioxidant effect Effects 0.000 claims description 2
230000002335 preservative effect Effects 0.000 claims description 2
239000011814 protection agent Substances 0.000 abstract description 2
125000000217 alkyl group Chemical group 0.000 description 20
229920001223 polyethylene glycol Polymers 0.000 description 16
239000011148 porous material Substances 0.000 description 13
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Substances OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 12
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Natural products CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 10
125000003118 aryl group Chemical group 0.000 description 10
239000011734 sodium Substances 0.000 description 10
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 8
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 8
229910052757 nitrogen Inorganic materials 0.000 description 8
239000002904 solvent Substances 0.000 description 8
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 7
235000006708 antioxidants Nutrition 0.000 description 7
BDAGIHXWWSANSR-UHFFFAOYSA-N formic acid Substances OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 7
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 6
VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Substances [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 6
235000015165 citric acid Nutrition 0.000 description 6
FLKPEMZONWLCSK-UHFFFAOYSA-N diethyl phthalate Chemical compound CCOC(=O)C1=CC=CC=C1C(=O)OCC FLKPEMZONWLCSK-UHFFFAOYSA-N 0.000 description 6
239000007788 liquid Substances 0.000 description 6
238000002156 mixing Methods 0.000 description 6
239000005022 packaging material Substances 0.000 description 6
GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulphite Substances [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 6
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AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Natural products OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 description 5
239000000987 azo dye Substances 0.000 description 5
235000014113 dietary fatty acids Nutrition 0.000 description 5
235000013804 distarch phosphate Nutrition 0.000 description 5
239000001245 distarch phosphate Substances 0.000 description 5
238000009826 distribution Methods 0.000 description 5
150000002148 esters Chemical class 0.000 description 5
229930195729 fatty acid Natural products 0.000 description 5
239000000194 fatty acid Substances 0.000 description 5
150000004665 fatty acids Chemical class 0.000 description 5
229940041616 menthol Drugs 0.000 description 5
238000000034 method Methods 0.000 description 5
239000002245 particle Substances 0.000 description 5
NBIIXXVUZAFLBC-UHFFFAOYSA-N phosphoric acid Substances OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 5
229920000728 polyester Polymers 0.000 description 5
239000000047 product Substances 0.000 description 5
238000002444 silanisation Methods 0.000 description 5
239000007858 starting material Substances 0.000 description 5
240000007436 Cananga odorata Species 0.000 description 4
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
239000002202 Polyethylene glycol Substances 0.000 description 4
RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 4
235000011054 acetic acid Nutrition 0.000 description 4
ZOJBYZNEUISWFT-UHFFFAOYSA-N allyl isothiocyanate Chemical compound C=CCN=C=S ZOJBYZNEUISWFT-UHFFFAOYSA-N 0.000 description 4
235000012665 annatto Nutrition 0.000 description 4
SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 description 4
235000010216 calcium carbonate Nutrition 0.000 description 4
239000001354 calcium citrate Substances 0.000 description 4
SHZIWNPUGXLXDT-UHFFFAOYSA-N ethyl hexanoate Chemical compound CCCCCC(=O)OCC SHZIWNPUGXLXDT-UHFFFAOYSA-N 0.000 description 4
NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 description 4
239000010642 eucalyptus oil Substances 0.000 description 4
229940044949 eucalyptus oil Drugs 0.000 description 4
RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 description 4
235000019253 formic acid Nutrition 0.000 description 4
235000011187 glycerol Nutrition 0.000 description 4
BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 4
235000011167 hydrochloric acid Nutrition 0.000 description 4
MLFHJEHSLIIPHL-UHFFFAOYSA-N isoamyl acetate Chemical compound CC(C)CCOC(C)=O MLFHJEHSLIIPHL-UHFFFAOYSA-N 0.000 description 4
239000001095 magnesium carbonate Substances 0.000 description 4
239000000203 mixture Substances 0.000 description 4
150000001282 organosilanes Chemical class 0.000 description 4
239000005011 phenolic resin Substances 0.000 description 4
239000001508 potassium citrate Substances 0.000 description 4
235000011082 potassium citrates Nutrition 0.000 description 4
KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Substances [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 4
229920005989 resin Polymers 0.000 description 4
239000011347 resin Substances 0.000 description 4
239000001509 sodium citrate Substances 0.000 description 4
235000011083 sodium citrates Nutrition 0.000 description 4
235000010267 sodium hydrogen sulphite Nutrition 0.000 description 4
HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Substances [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 4
235000010262 sodium metabisulphite Nutrition 0.000 description 4
235000010265 sodium sulphite Nutrition 0.000 description 4
239000007921 spray Substances 0.000 description 4
235000010269 sulphur dioxide Nutrition 0.000 description 4
RUVINXPYWBROJD-ONEGZZNKSA-N trans-anethole Chemical compound COC1=CC=C(\C=C\C)C=C1 RUVINXPYWBROJD-ONEGZZNKSA-N 0.000 description 4
WEFHSZAZNMEWKJ-KEDVMYETSA-N (6Z,8E)-undeca-6,8,10-trien-2-one (6E,8E)-undeca-6,8,10-trien-2-one (6Z,8E)-undeca-6,8,10-trien-3-one (6E,8E)-undeca-6,8,10-trien-3-one (6Z,8E)-undeca-6,8,10-trien-4-one (6E,8E)-undeca-6,8,10-trien-4-one Chemical compound CCCC(=O)C\C=C\C=C\C=C.CCCC(=O)C\C=C/C=C/C=C.CCC(=O)CC\C=C\C=C\C=C.CCC(=O)CC\C=C/C=C/C=C.CC(=O)CCC\C=C\C=C\C=C.CC(=O)CCC\C=C/C=C/C=C WEFHSZAZNMEWKJ-KEDVMYETSA-N 0.000 description 3
IANQTJSKSUMEQM-UHFFFAOYSA-N 1-benzofuran Chemical compound C1=CC=C2OC=CC2=C1 IANQTJSKSUMEQM-UHFFFAOYSA-N 0.000 description 3
CMCBDXRRFKYBDG-UHFFFAOYSA-N 1-dodecoxydodecane Chemical compound CCCCCCCCCCCCOCCCCCCCCCCCC CMCBDXRRFKYBDG-UHFFFAOYSA-N 0.000 description 3
244000283070 Abies balsamea Species 0.000 description 3
235000007173 Abies balsamea Nutrition 0.000 description 3
QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 3
NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 3
ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 description 3
241000116713 Ferula gummosa Species 0.000 description 3
241000218657 Picea Species 0.000 description 3
244000028419 Styrax benzoin Species 0.000 description 3
235000000126 Styrax benzoin Nutrition 0.000 description 3
239000005844 Thymol Substances 0.000 description 3
240000002657 Thymus vulgaris Species 0.000 description 3
235000007303 Thymus vulgaris Nutrition 0.000 description 3
239000001670 anatto Substances 0.000 description 3
235000001053 badasse Nutrition 0.000 description 3
230000015572 biosynthetic process Effects 0.000 description 3
235000010290 biphenyl Nutrition 0.000 description 3
239000004305 biphenyl Substances 0.000 description 3
125000006267 biphenyl group Chemical group 0.000 description 3
235000012730 carminic acid Nutrition 0.000 description 3
239000004106 carminic acid Substances 0.000 description 3
230000000052 comparative effect Effects 0.000 description 3
ZAKOWWREFLAJOT-UHFFFAOYSA-N d-alpha-Tocopheryl acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-UHFFFAOYSA-N 0.000 description 3
235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 description 3
239000000284 extract Substances 0.000 description 3
239000012530 fluid Substances 0.000 description 3
239000004864 galbanum Substances 0.000 description 3
239000003112 inhibitor Substances 0.000 description 3
244000056931 lavandin Species 0.000 description 3
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235000010445 lecithin Nutrition 0.000 description 3
239000000787 lecithin Substances 0.000 description 3
238000004519 manufacturing process Methods 0.000 description 3
235000012658 paprika extract Nutrition 0.000 description 3
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ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 3
235000011007 phosphoric acid Nutrition 0.000 description 3
229920001451 polypropylene glycol Polymers 0.000 description 3
SCVFZCLFOSHCOH-UHFFFAOYSA-M potassium acetate Substances [K+].CC([O-])=O SCVFZCLFOSHCOH-UHFFFAOYSA-M 0.000 description 3
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