DE102010045142B4 - Verfahren zur Herstellung primärer aliphatischer Amine aus Aldehyden - Google Patents

Verfahren zur Herstellung primärer aliphatischer Amine aus Aldehyden Download PDF

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Publication number
DE102010045142B4
DE102010045142B4 DE102010045142A DE102010045142A DE102010045142B4 DE 102010045142 B4 DE102010045142 B4 DE 102010045142B4 DE 102010045142 A DE102010045142 A DE 102010045142A DE 102010045142 A DE102010045142 A DE 102010045142A DE 102010045142 B4 DE102010045142 B4 DE 102010045142B4
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DE
Germany
Prior art keywords
ammonia
aldehydes
hydrogenation catalyst
aliphatic
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE102010045142A
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German (de)
English (en)
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DE102010045142A1 (de
Inventor
Kurt Schalapski
Dr. Nowotny Norman
Matthias Eisenacher
Dirk Bermann
Dr. Kreickmann Thorsten
Dr. Heymanns Peter
Dr. Strutz Heinz
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Oxea GmbH
Original Assignee
OQ Chemicals GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to DE102010045142A priority Critical patent/DE102010045142B4/de
Application filed by OQ Chemicals GmbH filed Critical OQ Chemicals GmbH
Priority to CN201180043554.4A priority patent/CN103097336B/zh
Priority to US13/817,155 priority patent/US8664444B2/en
Priority to JP2013527482A priority patent/JP5846697B2/ja
Priority to EP11751819.1A priority patent/EP2614044B1/de
Priority to PCT/EP2011/004156 priority patent/WO2012031672A1/de
Priority to MX2013002708A priority patent/MX2013002708A/es
Priority to TW100132513A priority patent/TWI429615B/zh
Publication of DE102010045142A1 publication Critical patent/DE102010045142A1/de
Application granted granted Critical
Publication of DE102010045142B4 publication Critical patent/DE102010045142B4/de
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
    • C07C209/26—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds by reduction with hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B43/00—Formation or introduction of functional groups containing nitrogen
    • C07B43/04—Formation or introduction of functional groups containing nitrogen of amino groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/86—Chromium
    • B01J23/866—Nickel and chromium

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE102010045142A 2010-09-11 2010-09-11 Verfahren zur Herstellung primärer aliphatischer Amine aus Aldehyden Expired - Fee Related DE102010045142B4 (de)

Priority Applications (8)

Application Number Priority Date Filing Date Title
DE102010045142A DE102010045142B4 (de) 2010-09-11 2010-09-11 Verfahren zur Herstellung primärer aliphatischer Amine aus Aldehyden
US13/817,155 US8664444B2 (en) 2010-09-11 2011-08-18 Method for producing primary aliphatic amines from aldehydes
JP2013527482A JP5846697B2 (ja) 2010-09-11 2011-08-18 アルデヒドからの第一脂肪族アミンの製造方法
EP11751819.1A EP2614044B1 (de) 2010-09-11 2011-08-18 Verfahren zur herstellung primärer aliphatischer amine aus aldehyden
CN201180043554.4A CN103097336B (zh) 2010-09-11 2011-08-18 由醛制备脂肪族伯胺的方法
PCT/EP2011/004156 WO2012031672A1 (de) 2010-09-11 2011-08-18 Verfahren zur herstellung primärer aliphatischer amine aus aldehyden
MX2013002708A MX2013002708A (es) 2010-09-11 2011-08-18 Metodo para producir aminas alifaticas primarias a partir de aldehidos.
TW100132513A TWI429615B (zh) 2010-09-11 2011-09-09 一級脂族胺之連續製造方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102010045142A DE102010045142B4 (de) 2010-09-11 2010-09-11 Verfahren zur Herstellung primärer aliphatischer Amine aus Aldehyden

Publications (2)

Publication Number Publication Date
DE102010045142A1 DE102010045142A1 (de) 2012-03-15
DE102010045142B4 true DE102010045142B4 (de) 2013-02-21

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Family Applications (1)

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DE102010045142A Expired - Fee Related DE102010045142B4 (de) 2010-09-11 2010-09-11 Verfahren zur Herstellung primärer aliphatischer Amine aus Aldehyden

Country Status (8)

Country Link
US (1) US8664444B2 (cg-RX-API-DMAC7.html)
EP (1) EP2614044B1 (cg-RX-API-DMAC7.html)
JP (1) JP5846697B2 (cg-RX-API-DMAC7.html)
CN (1) CN103097336B (cg-RX-API-DMAC7.html)
DE (1) DE102010045142B4 (cg-RX-API-DMAC7.html)
MX (1) MX2013002708A (cg-RX-API-DMAC7.html)
TW (1) TWI429615B (cg-RX-API-DMAC7.html)
WO (1) WO2012031672A1 (cg-RX-API-DMAC7.html)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102012016433A1 (de) * 2012-08-17 2014-05-15 Oxea Gmbh Kontinuierliches Verfahren zur Herstellung primärer aliphatischer Amine aus Aldehyden
DE102013106787A1 (de) * 2013-06-28 2014-12-31 Oxea Gmbh Verfahren zur Herstellung von n-Butanderivaten
CN106552661B (zh) * 2016-10-28 2019-06-14 中南民族大学 一种氮掺杂碳材料负载钴催化剂及利用其催化加氢还原胺化制备胺类化合物的方法
CN106622244B (zh) * 2016-12-31 2019-06-14 中南民族大学 一种氮掺杂碳材料包裹钴催化剂及利用其制备仲胺类化合物的方法
CN111097421A (zh) * 2018-10-29 2020-05-05 中国科学院大连化学物理研究所 负载型金属催化剂及其催化醛类化合物制备伯胺的方法
CN114425347B (zh) * 2020-10-29 2023-08-08 中国石油化工股份有限公司 环己亚胺的合成方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4322065A1 (de) * 1993-06-07 1995-01-12 Chemie Linz Deutschland Verfahren zur Herstellung primärer Amine aus Aldehyden
DE19627265A1 (de) * 1996-07-06 1998-01-08 Degussa Verfahren zur Herstellung primärer und/oder sekundärer Amine aus Oxoverbindungen
DE19935448A1 (de) * 1999-07-28 2001-02-01 Oxea Gmbh Verfahren zur Herstellung sekundärer aliphatischer Amine aus Aldehyden mittlerer Kettenlänge
EP1471998A1 (en) * 2001-12-14 2004-11-03 Huntsman Petrochemical Corporation Advances in amination catalysis

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE936211C (de) 1952-01-01 1955-12-07 Ruhrchemie Ag Verfahren zur Herstellung von aliphatischen Aminen
GB1575481A (en) * 1977-03-17 1980-09-24 Texaco Development Corp Selective oxoamination process
JPS58219148A (ja) * 1982-06-14 1983-12-20 Kuraray Co Ltd ７−オクテンアミンおよびその製造方法
SK281672B6 (sk) * 1993-06-07 2001-06-11 Carlo Kos Spôsob výroby primárnych amínov z aldehydov a zariadenie na vykonávanie tohto spôsobu
JP4059978B2 (ja) * 1998-05-29 2008-03-12 株式会社クラレ 一級アミンの製造法
DE19910960A1 (de) * 1999-03-12 2000-09-14 Basf Ag Verfahren zur Herstellung von Aminen

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4322065A1 (de) * 1993-06-07 1995-01-12 Chemie Linz Deutschland Verfahren zur Herstellung primärer Amine aus Aldehyden
DE19627265A1 (de) * 1996-07-06 1998-01-08 Degussa Verfahren zur Herstellung primärer und/oder sekundärer Amine aus Oxoverbindungen
DE19935448A1 (de) * 1999-07-28 2001-02-01 Oxea Gmbh Verfahren zur Herstellung sekundärer aliphatischer Amine aus Aldehyden mittlerer Kettenlänge
EP1471998A1 (en) * 2001-12-14 2004-11-03 Huntsman Petrochemical Corporation Advances in amination catalysis

Also Published As

Publication number Publication date
EP2614044B1 (de) 2014-10-08
CN103097336A (zh) 2013-05-08
DE102010045142A1 (de) 2012-03-15
JP5846697B2 (ja) 2016-01-20
US8664444B2 (en) 2014-03-04
EP2614044A1 (de) 2013-07-17
MX2013002708A (es) 2013-08-27
TW201210991A (en) 2012-03-16
CN103097336B (zh) 2015-11-25
TWI429615B (zh) 2014-03-11
JP2013540724A (ja) 2013-11-07
US20130150624A1 (en) 2013-06-13
WO2012031672A1 (de) 2012-03-15

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R018 Grant decision by examination section/examining division
R020 Patent grant now final

Effective date: 20130522

R119 Application deemed withdrawn, or ip right lapsed, due to non-payment of renewal fee