CS221530B2 - Method of preparation of the suspensions or solutions of the kyanurchloride in organic solvent containing water - Google Patents
Method of preparation of the suspensions or solutions of the kyanurchloride in organic solvent containing water Download PDFInfo
- Publication number
- CS221530B2 CS221530B2 CS797560A CS756079A CS221530B2 CS 221530 B2 CS221530 B2 CS 221530B2 CS 797560 A CS797560 A CS 797560A CS 756079 A CS756079 A CS 756079A CS 221530 B2 CS221530 B2 CS 221530B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- cyanuric chloride
- water
- organic solvent
- liquid
- suspensions
- Prior art date
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 37
- 239000003960 organic solvent Substances 0.000 title claims abstract description 22
- 239000000725 suspension Substances 0.000 title claims abstract description 21
- 238000000034 method Methods 0.000 title claims abstract description 15
- 238000002360 preparation method Methods 0.000 title claims description 8
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 claims abstract description 67
- 239000007788 liquid Substances 0.000 claims abstract description 36
- 239000002904 solvent Substances 0.000 claims abstract description 20
- 239000000203 mixture Substances 0.000 claims description 16
- 239000000460 chlorine Substances 0.000 claims description 6
- 229910052801 chlorine Inorganic materials 0.000 claims description 6
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 5
- QPJDMGCKMHUXFD-UHFFFAOYSA-N cyanogen chloride Chemical compound ClC#N QPJDMGCKMHUXFD-UHFFFAOYSA-N 0.000 claims description 5
- 239000007789 gas Substances 0.000 claims description 4
- 150000002576 ketones Chemical class 0.000 claims description 3
- 125000001931 aliphatic group Chemical group 0.000 claims description 2
- 239000011261 inert gas Substances 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 230000007062 hydrolysis Effects 0.000 abstract description 9
- 238000006460 hydrolysis reaction Methods 0.000 abstract description 9
- 238000001816 cooling Methods 0.000 abstract description 2
- 210000000481 breast Anatomy 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 23
- 239000007921 spray Substances 0.000 description 17
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- 230000015572 biosynthetic process Effects 0.000 description 8
- 238000005755 formation reaction Methods 0.000 description 8
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
- 239000002245 particle Substances 0.000 description 6
- 239000002002 slurry Substances 0.000 description 5
- XLJMAIOERFSOGZ-UHFFFAOYSA-N cyanic acid Chemical compound OC#N XLJMAIOERFSOGZ-UHFFFAOYSA-N 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- -1 dlethylketone Chemical compound 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- RGSFGYAAUTVSQA-UHFFFAOYSA-N Cyclopentane Chemical compound C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 2
- YNQLUTRBYVCPMQ-UHFFFAOYSA-N Ethylbenzene Chemical compound CCC1=CC=CC=C1 YNQLUTRBYVCPMQ-UHFFFAOYSA-N 0.000 description 2
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 description 2
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 description 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 2
- 229960001701 chloroform Drugs 0.000 description 2
- NNBZCPXTIHJBJL-UHFFFAOYSA-N decalin Chemical compound C1CCCC2CCCCC21 NNBZCPXTIHJBJL-UHFFFAOYSA-N 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000004880 explosion Methods 0.000 description 2
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- BOSAWIQFTJIYIS-UHFFFAOYSA-N 1,1,1-trichloro-2,2,2-trifluoroethane Chemical compound FC(F)(F)C(Cl)(Cl)Cl BOSAWIQFTJIYIS-UHFFFAOYSA-N 0.000 description 1
- ZCJAYDKWZAWMPR-UHFFFAOYSA-N 1-chloro-2-fluorobenzene Chemical compound FC1=CC=CC=C1Cl ZCJAYDKWZAWMPR-UHFFFAOYSA-N 0.000 description 1
- YTCGOUNVIAWCMG-UHFFFAOYSA-N 1-chloro-3-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=CC=CC(Cl)=C1 YTCGOUNVIAWCMG-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical compound ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000004035 construction material Substances 0.000 description 1
- VMKJWLXVLHBJNK-UHFFFAOYSA-N cyanuric fluoride Chemical compound FC1=NC(F)=NC(F)=N1 VMKJWLXVLHBJNK-UHFFFAOYSA-N 0.000 description 1
- 150000001924 cycloalkanes Chemical class 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- DMEGYFMYUHOHGS-UHFFFAOYSA-N heptamethylene Natural products C1CCCCCC1 DMEGYFMYUHOHGS-UHFFFAOYSA-N 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 239000004434 industrial solvent Substances 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- MYWUZJCMWCOHBA-VIFPVBQESA-N methamphetamine Chemical compound CN[C@@H](C)CC1=CC=CC=C1 MYWUZJCMWCOHBA-VIFPVBQESA-N 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- XYKIUTSFQGXHOW-UHFFFAOYSA-N propan-2-one;toluene Chemical compound CC(C)=O.CC1=CC=CC=C1 XYKIUTSFQGXHOW-UHFFFAOYSA-N 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 235000020095 red wine Nutrition 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 229950011008 tetrachloroethylene Drugs 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 238000005829 trimerization reaction Methods 0.000 description 1
- PXXNTAGJWPJAGM-UHFFFAOYSA-N vertaline Natural products C1C2C=3C=C(OC)C(OC)=CC=3OC(C=C3)=CC=C3CCC(=O)OC1CC1N2CCCC1 PXXNTAGJWPJAGM-UHFFFAOYSA-N 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/50—Mixing liquids with solids
- B01F23/51—Methods thereof
- B01F23/511—Methods thereof characterised by the composition of the liquids or solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/16—Evaporating by spraying
- B01D1/18—Evaporating by spraying to obtain dry solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/405—Methods of mixing liquids with liquids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/70—Spray-mixers, e.g. for mixing intersecting sheets of material
- B01F25/72—Spray-mixers, e.g. for mixing intersecting sheets of material with nozzles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/28—Only halogen atoms, e.g. cyanuric chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Fertilizers (AREA)
- Paper (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2850308A DE2850308C2 (de) | 1978-11-20 | 1978-11-20 | Verfahren zur Herstellung von Suspensionen oder Lösungen von Cyanurchlorid in wasserhaltigen organischen Lösungsmitteln |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CS221530B2 true CS221530B2 (en) | 1983-04-29 |
Family
ID=6055154
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS797560A CS221530B2 (en) | 1978-11-20 | 1979-11-06 | Method of preparation of the suspensions or solutions of the kyanurchloride in organic solvent containing water |
Country Status (22)
| Country | Link |
|---|---|
| US (1) | US4271297A (de) |
| JP (1) | JPS5573666A (de) |
| AT (1) | AT368140B (de) |
| BE (1) | BE880136A (de) |
| BR (1) | BR7907280A (de) |
| CA (1) | CA1102328A (de) |
| CH (1) | CH642641A5 (de) |
| CS (1) | CS221530B2 (de) |
| DD (1) | DD147104A5 (de) |
| DE (1) | DE2850308C2 (de) |
| ES (1) | ES483869A1 (de) |
| FR (1) | FR2441622A1 (de) |
| GB (1) | GB2036730B (de) |
| HU (1) | HU184074B (de) |
| IL (1) | IL58601A (de) |
| IN (1) | IN152665B (de) |
| IT (1) | IT1119122B (de) |
| MX (1) | MX153773A (de) |
| NL (1) | NL7908434A (de) |
| SE (1) | SE446728B (de) |
| YU (1) | YU40226B (de) |
| ZA (1) | ZA796276B (de) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4552959A (en) * | 1982-05-18 | 1985-11-12 | Ciba Geigy Ag | Process for producing a suspension of cyanuric chloride in water |
| WO2004087306A1 (ja) * | 2003-03-28 | 2004-10-14 | Suntory Limited | 固形物の排出機構及び排出方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1695117U (de) | 1954-07-16 | 1955-03-17 | Verschleisstechnik Dr Ing Hans | Kern fuer hohlziegelformen. |
| US3256070A (en) * | 1960-10-12 | 1966-06-14 | Geigy Chem Corp | Desublimation using a rotating cooling drum containing particulate tumbling and grinding media |
| DE1545840A1 (de) * | 1965-07-24 | 1969-10-23 | Bayer Ag | Verfahren zur kontinuierlichen Herstellung von reaktionsbereitem Cyanursaeurechlorid in waessriger Suspension |
| GB1095454A (de) * | 1965-08-21 | |||
| DE1670731B2 (de) * | 1966-08-11 | 1974-01-03 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung einer von Lösungsmitteln freien, wäßrigen, neutralen Cyanurchlorid-Suspension |
| FR1534235A (fr) * | 1966-08-11 | 1968-07-26 | Bayer Ag | Procédé de préparation d'une suspension aqueuse neutre de chlorure de cyanuryle exempte de solvants |
| CH546247A (de) | 1968-12-27 | 1974-02-28 | Agripat Sa | Adiabatisches verfahren zur herstellung von n-monosubstituierten 2,4-dichlor-6-amino-s-triazinen. |
| DE2162064A1 (de) * | 1971-12-14 | 1973-06-20 | Sueddeutsche Kalkstickstoff | Verfahren zur gewinnung von festem cyanurchlorid |
| DD111378A5 (de) * | 1973-06-27 | 1975-02-12 | ||
| RO70804A (ro) * | 1974-11-20 | 1980-08-15 | Deutsche Gold-Und Silber-Scheideanstalt Vormals Roessler,De | Procedeu si dispozitiv pentru prepararea unor solutii sau suspensii de clorura de cianuril |
| DE2551164A1 (de) * | 1975-11-14 | 1977-05-26 | Degussa | Verfahren und vorrichtung zum herstellen von loesungen oder suspensionen von cyanurchlorid in wasserhaltigen organischen loesungsmitteln |
-
1978
- 1978-11-20 DE DE2850308A patent/DE2850308C2/de not_active Expired
-
1979
- 1979-07-03 YU YU1610/79A patent/YU40226B/xx unknown
- 1979-08-06 IT IT68621/79A patent/IT1119122B/it active
- 1979-08-09 MX MX178857A patent/MX153773A/es unknown
- 1979-08-29 IN IN895/CAL/79A patent/IN152665B/en unknown
- 1979-09-04 ES ES483869A patent/ES483869A1/es not_active Expired
- 1979-10-25 DD DD79216458A patent/DD147104A5/de unknown
- 1979-11-01 IL IL58601A patent/IL58601A/xx unknown
- 1979-11-06 CS CS797560A patent/CS221530B2/cs unknown
- 1979-11-09 BR BR7907280A patent/BR7907280A/pt unknown
- 1979-11-13 GB GB7939165A patent/GB2036730B/en not_active Expired
- 1979-11-16 US US06/094,872 patent/US4271297A/en not_active Expired - Lifetime
- 1979-11-19 BE BE6/47010A patent/BE880136A/fr not_active IP Right Cessation
- 1979-11-19 SE SE7909564A patent/SE446728B/sv not_active IP Right Cessation
- 1979-11-19 HU HU79DE1029A patent/HU184074B/hu unknown
- 1979-11-19 CH CH1029979A patent/CH642641A5/de not_active IP Right Cessation
- 1979-11-19 NL NL7908434A patent/NL7908434A/nl not_active Application Discontinuation
- 1979-11-19 CA CA340,146A patent/CA1102328A/en not_active Expired
- 1979-11-19 AT AT0734779A patent/AT368140B/de not_active IP Right Cessation
- 1979-11-20 JP JP14962679A patent/JPS5573666A/ja active Pending
- 1979-11-20 FR FR7928606A patent/FR2441622A1/fr active Granted
- 1979-11-20 ZA ZA00796276A patent/ZA796276B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE2850308B1 (de) | 1980-06-12 |
| ATA734779A (de) | 1982-01-15 |
| BE880136A (fr) | 1980-05-19 |
| IN152665B (de) | 1984-03-10 |
| IL58601A (en) | 1983-11-30 |
| MX153773A (es) | 1987-01-09 |
| SE7909564L (sv) | 1980-05-21 |
| YU40226B (en) | 1985-08-31 |
| YU161079A (en) | 1982-08-31 |
| IT7968621A0 (it) | 1979-08-06 |
| IL58601A0 (en) | 1980-02-29 |
| NL7908434A (nl) | 1980-05-22 |
| HU184074B (en) | 1984-06-28 |
| US4271297A (en) | 1981-06-02 |
| IT1119122B (it) | 1986-03-03 |
| FR2441622A1 (fr) | 1980-06-13 |
| GB2036730B (en) | 1983-03-09 |
| AT368140B (de) | 1982-09-10 |
| SE446728B (sv) | 1986-10-06 |
| DD147104A5 (de) | 1981-03-18 |
| CH642641A5 (de) | 1984-04-30 |
| ES483869A1 (es) | 1980-04-16 |
| ZA796276B (en) | 1980-11-26 |
| FR2441622B1 (de) | 1983-04-15 |
| JPS5573666A (en) | 1980-06-03 |
| DE2850308C2 (de) | 1984-09-20 |
| GB2036730A (en) | 1980-07-02 |
| CA1102328A (en) | 1981-06-02 |
| BR7907280A (pt) | 1980-09-23 |
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