CN1951867A - 具有钙钛矿结构的陶瓷粉末 - Google Patents
具有钙钛矿结构的陶瓷粉末 Download PDFInfo
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- CN1951867A CN1951867A CNA2006101538962A CN200610153896A CN1951867A CN 1951867 A CN1951867 A CN 1951867A CN A2006101538962 A CNA2006101538962 A CN A2006101538962A CN 200610153896 A CN200610153896 A CN 200610153896A CN 1951867 A CN1951867 A CN 1951867A
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- powder
- ceramic powder
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- barium titanate
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- 239000000843 powder Substances 0.000 title claims abstract description 146
- 239000000919 ceramic Substances 0.000 title claims abstract description 84
- 239000002245 particle Substances 0.000 claims description 36
- 238000009826 distribution Methods 0.000 claims description 31
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical group [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 claims description 7
- JRPBQTZRNDNNOP-UHFFFAOYSA-N barium titanate Chemical compound [Ba+2].[Ba+2].[O-][Ti]([O-])([O-])[O-] JRPBQTZRNDNNOP-UHFFFAOYSA-N 0.000 abstract description 32
- 229910002113 barium titanate Inorganic materials 0.000 abstract description 32
- 238000004519 manufacturing process Methods 0.000 abstract description 18
- 239000010936 titanium Substances 0.000 abstract description 16
- 239000007864 aqueous solution Substances 0.000 abstract description 14
- 239000002994 raw material Substances 0.000 abstract description 8
- 238000010532 solid phase synthesis reaction Methods 0.000 abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 8
- AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 abstract description 5
- 238000010438 heat treatment Methods 0.000 abstract description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract description 3
- 230000015572 biosynthetic process Effects 0.000 abstract description 3
- 239000000203 mixture Substances 0.000 abstract description 3
- 238000003786 synthesis reaction Methods 0.000 abstract description 3
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 abstract 2
- RQPZNWPYLFFXCP-UHFFFAOYSA-L barium dihydroxide Chemical compound [OH-].[OH-].[Ba+2] RQPZNWPYLFFXCP-UHFFFAOYSA-L 0.000 abstract 1
- 229910001863 barium hydroxide Inorganic materials 0.000 abstract 1
- 238000000034 method Methods 0.000 description 57
- 239000000243 solution Substances 0.000 description 26
- 238000007669 thermal treatment Methods 0.000 description 23
- 239000007788 liquid Substances 0.000 description 17
- 238000005245 sintering Methods 0.000 description 17
- VEALVRVVWBQVSL-UHFFFAOYSA-N strontium titanate Chemical compound [Sr+2].[O-][Ti]([O-])=O VEALVRVVWBQVSL-UHFFFAOYSA-N 0.000 description 17
- 239000003985 ceramic capacitor Substances 0.000 description 16
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 12
- 229910052712 strontium Inorganic materials 0.000 description 10
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 9
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 8
- UUCCCPNEFXQJEL-UHFFFAOYSA-L strontium dihydroxide Chemical compound [OH-].[OH-].[Sr+2] UUCCCPNEFXQJEL-UHFFFAOYSA-L 0.000 description 8
- 229910001866 strontium hydroxide Inorganic materials 0.000 description 8
- 239000000470 constituent Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- 229910052788 barium Inorganic materials 0.000 description 6
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 6
- 230000002194 synthesizing effect Effects 0.000 description 6
- 229910052719 titanium Inorganic materials 0.000 description 6
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 5
- 229910001864 baryta Inorganic materials 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000011049 filling Methods 0.000 description 5
- 150000003839 salts Chemical class 0.000 description 5
- 238000004364 calculation method Methods 0.000 description 4
- 239000012530 fluid Substances 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 239000002003 electrode paste Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000008187 granular material Substances 0.000 description 3
- 230000007062 hydrolysis Effects 0.000 description 3
- 238000006460 hydrolysis reaction Methods 0.000 description 3
- 238000001027 hydrothermal synthesis Methods 0.000 description 3
- 125000000896 monocarboxylic acid group Chemical group 0.000 description 3
- 238000001308 synthesis method Methods 0.000 description 3
- 239000012808 vapor phase Substances 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 101100496858 Mus musculus Colec12 gene Proteins 0.000 description 2
- 229910010413 TiO 2 Inorganic materials 0.000 description 2
- 229910052787 antimony Inorganic materials 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000002788 crimping Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 239000003989 dielectric material Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- -1 hydrogen metal oxide Chemical class 0.000 description 2
- 229910052745 lead Inorganic materials 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910021645 metal ion Inorganic materials 0.000 description 2
- 229910052758 niobium Inorganic materials 0.000 description 2
- 235000006408 oxalic acid Nutrition 0.000 description 2
- 238000000634 powder X-ray diffraction Methods 0.000 description 2
- 229910052761 rare earth metal Inorganic materials 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 229910001631 strontium chloride Inorganic materials 0.000 description 2
- AHBGXTDRMVNFER-UHFFFAOYSA-L strontium dichloride Chemical compound [Cl-].[Cl-].[Sr+2] AHBGXTDRMVNFER-UHFFFAOYSA-L 0.000 description 2
- 229910052718 tin Inorganic materials 0.000 description 2
- 229910052721 tungsten Inorganic materials 0.000 description 2
- 229910052727 yttrium Inorganic materials 0.000 description 2
- 229910052726 zirconium Inorganic materials 0.000 description 2
- PDDYSBQASNZICP-UHFFFAOYSA-N 2-hydroxypropane-1,2,3-tricarboxylic acid;titanium Chemical compound [Ti].OC(=O)CC(O)(C(O)=O)CC(O)=O PDDYSBQASNZICP-UHFFFAOYSA-N 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- 229910002367 SrTiO Inorganic materials 0.000 description 1
- 239000003570 air Substances 0.000 description 1
- 150000004703 alkoxides Chemical class 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- WDIHJSXYQDMJHN-UHFFFAOYSA-L barium chloride Chemical compound [Cl-].[Cl-].[Ba+2] WDIHJSXYQDMJHN-UHFFFAOYSA-L 0.000 description 1
- 229910001626 barium chloride Inorganic materials 0.000 description 1
- 229940045511 barium chloride Drugs 0.000 description 1
- 229940006612 barium citrate Drugs 0.000 description 1
- PAVWOHWZXOQYDB-UHFFFAOYSA-H barium(2+);2-hydroxypropane-1,2,3-tricarboxylate Chemical compound [Ba+2].[Ba+2].[Ba+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O PAVWOHWZXOQYDB-UHFFFAOYSA-H 0.000 description 1
- 239000010953 base metal Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000007607 die coating method Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 description 1
- 229920000139 polyethylene terephthalate Polymers 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000007650 screen-printing Methods 0.000 description 1
- RXSHXLOMRZJCLB-UHFFFAOYSA-L strontium;diacetate Chemical compound [Sr+2].CC([O-])=O.CC([O-])=O RXSHXLOMRZJCLB-UHFFFAOYSA-L 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
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- H01R13/62—Means for facilitating engagement or disengagement of coupling parts or for holding them in engagement
- H01R13/639—Additional means for holding or locking coupling parts together, after engagement, e.g. separate keylock, retainer strap
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/46—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates
- C04B35/462—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates
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- C04B35/468—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates based on barium titanates
- C04B35/4682—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates based on titanates based on alkaline earth metal titanates based on barium titanates based on BaTiO3 perovskite phase
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G1/00—Methods of preparing compounds of metals not covered by subclasses C01B, C01C, C01D, or C01F, in general
- C01G1/02—Oxides
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- H01G4/00—Fixed capacitors; Processes of their manufacture
- H01G4/002—Details
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- H01G4/1209—Ceramic dielectrics characterised by the ceramic dielectric material
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- H01R12/70—Coupling devices
- H01R12/71—Coupling devices for rigid printing circuits or like structures
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- H01R13/46—Bases; Cases
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
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- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
- C04B2235/5454—Particle size related information expressed by the size of the particles or aggregates thereof nanometer sized, i.e. below 100 nm
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- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
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| JP2003080407A JP4141298B2 (ja) | 2003-03-24 | 2003-03-24 | ペロブスカイト構造を有する誘電体セラミック粉末の製造方法と、セラミック電子部品の製造方法と、積層セラミックコンデンサの製造方法 |
| JP080407/2003 | 2003-03-24 |
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| KR (1) | KR100707646B1 (https=) |
| CN (2) | CN1951867A (https=) |
| TW (1) | TW200420524A (https=) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN118164751A (zh) * | 2022-12-08 | 2024-06-11 | 福建贝思科电子材料股份有限公司 | 一种钛酸钡钙粉体、其制备方法及应用 |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005272295A (ja) * | 2004-02-26 | 2005-10-06 | Dowa Mining Co Ltd | 正方晶チタン酸バリウム粒子およびその製造方法並びにセラミックコンデンサ |
| EP1798200B1 (en) * | 2004-08-13 | 2017-03-22 | Sakai Chemical Industry Co., Ltd. | Process for producing perovskite compound powder |
| JP4766910B2 (ja) * | 2005-04-26 | 2011-09-07 | 京セラ株式会社 | チタン酸バリウム粉末の製法、チタン酸バリウム粉末、およびチタン酸バリウム焼結体 |
| JP4827011B2 (ja) * | 2006-03-10 | 2011-11-30 | Tdk株式会社 | セラミック粉末及びこれを用いた誘電体ペースト、積層セラミック電子部品、その製造方法 |
| WO2008078652A1 (ja) * | 2006-12-25 | 2008-07-03 | National Institute For Materials Science | 誘電体素子とその製造方法 |
| JP5184333B2 (ja) * | 2008-12-25 | 2013-04-17 | サムソン エレクトロ−メカニックス カンパニーリミテッド. | 誘電体セラミックス材料の製造方法 |
| JP5233763B2 (ja) * | 2009-03-13 | 2013-07-10 | 株式会社村田製作所 | チタン酸バリウム系誘電体原料粉末、その製造方法、セラミックグリーンシートの製造方法、および積層セラミックコンデンサの製造方法 |
| US8496893B2 (en) * | 2009-06-25 | 2013-07-30 | Eestor, Inc. | Method of forming a dielectric powder using a precipitated precursor powder |
| JP5445412B2 (ja) * | 2010-09-17 | 2014-03-19 | 株式会社村田製作所 | 複合酸化物粉末の製造方法 |
| JP2012072037A (ja) * | 2010-09-29 | 2012-04-12 | Tdk Corp | 誘電体磁器組成物およびその製造方法ならびにセラミック電子部品 |
| CN102074351A (zh) * | 2010-11-12 | 2011-05-25 | 无锡索垠飞科技有限公司 | 电容式储能电池及其制造方法 |
| CN102035265B (zh) * | 2010-12-06 | 2013-11-20 | 南京科孚纳米技术有限公司 | 电容器储能电池无线充电系统 |
| KR101218979B1 (ko) | 2010-12-10 | 2013-01-04 | 삼성전기주식회사 | 페롭스카이트 분말의 제조방법, 그 방법으로 제조한 페롭스카이트 분말 및 적층 세라믹 전자부품 |
| KR20130038695A (ko) * | 2011-10-10 | 2013-04-18 | 삼성전기주식회사 | 페롭스카이트 분말, 이의 제조방법 및 이를 이용한 적층 세라믹 전자부품 |
| JP5629719B2 (ja) * | 2012-03-30 | 2014-11-26 | 太陽誘電株式会社 | セラミック粉末及び積層セラミックコンデンサ |
| JP5484506B2 (ja) * | 2012-03-30 | 2014-05-07 | 太陽誘電株式会社 | セラミック粉末及び積層セラミックコンデンサ |
| JP5566434B2 (ja) * | 2012-09-25 | 2014-08-06 | 太陽誘電株式会社 | 積層セラミックコンデンサ |
| CN102886934A (zh) * | 2012-10-29 | 2013-01-23 | 哈尔滨工业大学 | 一种结晶完全且无杂相产生的多铁性薄膜及其制备方法 |
| JP2015109410A (ja) * | 2013-10-25 | 2015-06-11 | 株式会社村田製作所 | セラミック電子部品及びセラミック電子部品の製造方法 |
| CN105706199B (zh) * | 2013-11-18 | 2018-07-27 | 株式会社村田制作所 | 带有变阻器功能的层叠型半导体陶瓷电容器及其制造方法 |
| CN104045341A (zh) * | 2014-06-24 | 2014-09-17 | 天津大学 | 无铅高介电常数多层陶瓷电容器介质材料及其制备方法 |
| JP5874798B2 (ja) * | 2014-09-30 | 2016-03-02 | 株式会社村田製作所 | チタン酸バリウム系セラミック粉末 |
| CN104387088A (zh) * | 2014-10-29 | 2015-03-04 | 安徽省皖捷液压科技有限公司 | 一种废橡胶轮胎颗粒/氮化硅复合的陶瓷喷嘴及其制作方法 |
| JP7523922B2 (ja) * | 2020-03-03 | 2024-07-29 | 太陽誘電株式会社 | セラミック電子部品の製造方法、および金属導電ペースト |
| CN112919529A (zh) * | 2021-03-31 | 2021-06-08 | 成渝钒钛科技有限公司 | 一种利用含钛高炉渣制备钛酸钡的方法 |
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| US2166221A (en) * | 1937-06-29 | 1939-07-18 | Du Pont | Process for producing pigment titanates |
| BE478147A (https=) * | 1944-04-04 | |||
| US2976116A (en) * | 1958-03-03 | 1961-03-21 | Walter W Malinofsky | Method of preparation of barium titanate powder |
| US4874598A (en) * | 1987-01-20 | 1989-10-17 | Mitsubishi Petrochemical Co., Ltd. | Process for producing perovskite-type oxides of the ABO3 type |
| JP3302627B2 (ja) * | 1997-07-31 | 2002-07-15 | 太陽誘電株式会社 | セラミック粉末の製造方法 |
| WO2000001618A1 (en) * | 1998-07-01 | 2000-01-13 | Cabot Corporation | Hydrothermal process for making barium titanate powders |
| JP3780851B2 (ja) | 2000-03-02 | 2006-05-31 | 株式会社村田製作所 | チタン酸バリウムおよびその製造方法ならびに誘電体セラミックおよびセラミック電子部品 |
| CN1219725C (zh) * | 2000-05-12 | 2005-09-21 | 中国科学院大连化学物理研究所 | 一种制备高性能复合氧化物粉体的方法 |
| US6409983B1 (en) * | 2000-07-11 | 2002-06-25 | Korea Institute Of Science And Technology | Process for preparing crystalline barium titanate powder |
| JP4660935B2 (ja) | 2001-02-05 | 2011-03-30 | 株式会社村田製作所 | 正方晶ペロブスカイト構造を有するチタン酸バリウム系セラミック粉末の製造方法 |
| CN1172874C (zh) * | 2002-07-10 | 2004-10-27 | 清华大学 | 制备四方相钛酸钡纳米粉体的方法 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN118164751A (zh) * | 2022-12-08 | 2024-06-11 | 福建贝思科电子材料股份有限公司 | 一种钛酸钡钙粉体、其制备方法及应用 |
| CN118164751B (zh) * | 2022-12-08 | 2025-10-21 | 福建贝思科电子材料股份有限公司 | 一种钛酸钡钙粉体、其制备方法及应用 |
Also Published As
| Publication number | Publication date |
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| US20070104970A1 (en) | 2007-05-10 |
| CN100344579C (zh) | 2007-10-24 |
| CN1532167A (zh) | 2004-09-29 |
| KR100707646B1 (ko) | 2007-04-13 |
| JP4141298B2 (ja) | 2008-08-27 |
| JP2004284897A (ja) | 2004-10-14 |
| TW200420524A (en) | 2004-10-16 |
| KR20040084725A (ko) | 2004-10-06 |
| HK1066975A1 (zh) | 2005-03-18 |
| TWI304056B (https=) | 2008-12-11 |
| US7572406B2 (en) | 2009-08-11 |
| US7271114B2 (en) | 2007-09-18 |
| US7566439B2 (en) | 2009-07-28 |
| US20040188002A1 (en) | 2004-09-30 |
| US20070104640A1 (en) | 2007-05-10 |
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