CN1775038A - Green pesticide formula and production process - Google Patents
Green pesticide formula and production process Download PDFInfo
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Abstract
The present invention relates to a formula of green mycocide disinfectant and its production process. Said formula composition includes (by wt%) 4%-8% of Chinese medicinal material, 18%-25% of sulfur, 10%-20% of alum, 45%-63% of quicklime powder and 2%-5% of talcum powder, in which the Chinese medicinal material is formed from 18 Chinese herbal medicines of mahonia leaf, bletilla tuber, isatis root, wild chrysanthemum flower, aspidium and others. Its preparation process includes the following steps: heating sulfur and alum, adding quicklime powder, stir-frying until yellow, adding water to make decoction, adding Chinese medicinal material to make continuous decoction, filtering, standing still and clarifying so as to obtain the invented product.
Description
Technical field
The present invention relates to a kind of sterilization, the prescription and the production technology of go out malicious agricultural chemicals, particularly a kind of environment friendly agricultural.
Background technology
Domestic existing sterilization and disinfection class agricultural chemicals mostly is a chemical pesticide, use this type of agricultural chemicals easily to cause a large amount of the toxin remains in crops, vegetables and melon and fruit, make natural environment be subjected to severe contamination, the broken natural environment and the ecological balance encircled, constitute a public nuisance, directly threaten existent environment of people, be unfavorable for developing green agriculture and pollution-free food.
In recent years, someone develops several environment friendly agriculturals, the insecticidal effect of this type of agricultural chemicals is better, but the effect of sterilization, the poison that goes out a little less than, more crops are encouraged, help strong function, and the production technology more complicated, apparatus expensive, the cost height, production scale is very limited, and is difficult to promote and implement.
Summary of the invention
The objective of the invention is to provide a kind of efficient, nuisanceless, noresidue, property of medicine gentleness has sterilization, the prescription and a production technology of the environment friendly agricultural of the poison that goes out, growth encourage.
The content that solves the technology of the present invention problem comprises a kind of prescription of environment friendly agricultural:
Chinese herbal medicine: sulphur 4%~8%: alum 18%~25%: quicklime powder 10%~20%: talcum powder 45%~63%: 2%~5%;
The prescription of Chinese herbal medicine wherein:
Chinese mahonia: 7%-10%; The bletilla striata: 2%-5%; Radix Isatidis: 3%-5%; Mother chrysanthemum: 4%-7%; Cyrtomium fortunei: 4%-6%; Radix ampelopsis: 3%-6%; Kuh-seng: 15%-20%; Chinese violet: 3%-6%; Giant knotweed: 4%-6%; The capsule of weeping forsythia: 4%-7%; Folium isatidis: 3%-5%; Safflower: 3%-5%; Branch: 2%-4%; Subprostrate sophora: 7%-10%; Felwort: 4%-6%; Radix Wikstroemae: 3%-5%; Radix Glycyrrhizae: 4%-7%; Oldenlandia diffusa: 3%-5%.
Comprise and a kind ofly solve the process technology scheme that the technology of the present invention problem adopted and be:
1. sulphur and alum are put into pot and are heated to 100-120 degree centigrade, treat that sulphur and alum melt after, stir;
2. with quicklime powder 60 orders-100 order, be added in the pot of the sulphur of thawing and alum, with moderate heat the mixture of quicklime powder, sulphur and alum is fried to yellowish-brown, add clear water again with the quicklime powder equivalent weight, boil with moderate heat, and constantly stir, when medicine arsenic reaches thickness, it is taken the dish out of the pot, be placed on and leave standstill in the container; In leaving standstill container, add clear water immediately, medicine arsenic and clear water stirred greater than medicine arsenic two volumes, quiet put 12-36 hour after, the extraction supernatant liquor is semi-finished product liquid;
3. semi-finished product liquid is put into pot, add the Chinese herbal medicine prepare again, boil, use force earlier and burn after boil, use slow fire instead, boil after 40-60 minute and cease fire, pull the medium-height grass dregs of a decoction out;
4. the soup that boils is taken the dish out of the pot, puts into special container after the filtration, quietly put clarification in 24-48 hour, can obtain the finished product soup, qualified after testing after, can canned warehouse-in.
Beneficial effect: in the such scheme, the middle pure Chinese medicinal preparation that the soup that adopts natural Chinese medicinal herb to refine cooperates with Chinese medicine, Chinese herbal medicine mixes with Chinese medicine, a lot of useful compositions have been produced after boiling, its main component comprises: alkaloid, the plant organic acid, Radix Glycyrrhizae acetaldehyde, cement, sitosterol, glycoside, protease, starch, uranidin, tannin, carthamin, sulphur, materials such as calcium, has high-efficiency broad spectrum, no residual hazard, nuisanceless, pollution-free, the collection drug effect, fertilizer efficiency is characteristics such as one, non-stimulated to plant, can cure the disease, disease prevention in advance again, Chinese herbal medicine with always curing the disease for human and fowl poultry kind applies to on the plant disease treatment, uses the disease of treatment by Chinese herbs plant, it can be to the plurality of cereals class, fruit tree kind, the bacterium that vegetable category and other economic crops are taken place, fungi, disease such as mould and virus all has stronger killing effect, can effectively prevent and treat the various disease conditions of crops.The present invention is except containing pharmaceutical compositions; also contain the indispensable various trace elements of crop growthing development; the crops stalwartness is grown; play efficient; nuisanceless, noresidue, property of medicine gentleness; have sterilization, the poison that goes out, encourage to protect the unique effects of flower, fruit retention, guarantor's soil, volume increase, freeze proof evil, reached purpose of the present invention.This environment friendly agricultural is a kind of " environment-friendly type " pure Chinese medicinal preparation, can be to plant and poultry, bird sterilization, poison goes out, wide adaptability, the sediment of making agricultural chemicals is again good base fertilizer to agricultural crops, and environmentally safe helps promoting pollution-free food, promote agricultural development, change the present situation that current a large amount of use chemical pesticide destroys the natural environment and the ecological balance, improve the people's fitness, promote the well-being of mankind.
In addition, confirm through test, finished product soup of the present invention through spice or convert water by poultry edible or drink after, can improve the immunity of poultry, the generation of communicate illnesss such as prevention pestilence.
Through Henan and the large tracts of land agricultural experiment data acknowledgement of Shandong two province two places agricultural functional departments, disease cure rate to due to illness poison, germ initiation is more than 82%, and using method is simple, by 1: the 300-500 times of effect that soup is converted water spray, irritated root, dresses seed and all can reach sterilization, go out poison.
Embodiment
Embodiment 1: Chinese herbal medicine: sulphur 6%: alum 21%: quicklime powder 14%: talcum powder 55%: 4%.
The prescription of Chinese herbal medicine wherein:
Chinese mahonia: 7%; The bletilla striata: 2%; Radix Isatidis: 3%; Mother chrysanthemum: 4%; Cyrtomium fortunei: 4%; Radix ampelopsis: 3%; Kuh-seng: 15%; Chinese violet: 4%; Giant knotweed: 4%; The capsule of weeping forsythia: 7%; Folium isatidis: 5%; Safflower: 5%; Branch: 4%; Subprostrate sophora: 10%; Felwort: 6%; Radix Wikstroemae: 5%; Radix Glycyrrhizae: 7%; Oldenlandia diffusa: 5%.
The process technology scheme that solves its technical problem employing is:
1. sulphur and alum are put into pot and are heated to 110 degrees centigrade, treat that sulphur and alum melt after, stir;
2. with 80 order quicklime powders, be added in the pot of the sulphur of thawing and alum, with moderate heat the mixture of quicklime powder, sulphur and alum is fried to yellowish-brown, add clear water again with the quicklime powder equivalent weight, boil with moderate heat, and constantly stir, when medicine arsenic reaches thickness, it is taken the dish out of the pot, be placed on and leave standstill in the container; In leaving standstill container, add clear water immediately, medicine arsenic and clear water stirred greater than medicine arsenic two volumes, quiet put 24 hours after, the extraction supernatant liquor obtains semi-finished product liquid;
3. semi-finished product liquid is put into pot, add the Chinese herbal medicine prepare, boil, use force earlier and burn after boil, use slow fire instead, boil after 50 minutes and cease fire, pull the medium-height grass dregs of a decoction out;
4. the soup that boils is taken the dish out of the pot, put into special container after the filtration, quietly put clarification in 36 hours, can obtain the finished product soup; After qualified after testing, can canned warehouse-in.
Example: the villager Shao Mingzang of Shao Caiyuan administrative village, Bole town, Chengwu County, Shandong Province, in booth, plant vegetables and try out the situation of above-mentioned agricultural chemicals: the booth on half mu of ground, plantation cucumber and custard squash, all used this pesticide application in continuous 2 years, 1 year, plantation cucumber, custard squash, brought into use October 5 from the lunar calendar, with the dilution proportion of agricultural chemicals with 1: 300, spray on the seedling with soil in, spray in per 20 days is once, 1.5 kilograms in shared agricultural chemicals, 9830 yuan of final cucumber incomes, 3420 yuan of 192 incomes of custard squash are taken in 13070 yuan altogether.
1 year, still plant cucumber, custard squash begins to use this medicine from seedling, is to use 1: 500 times in the past 30 centimeters of heights of seedling, spray in per 15 days once, the blade face is thick, bottle green, and seedling is sturdy, use dilution 300-400 doubly in the time of cucumber and custard squash result, sprayed once in per 10 days, melon looks big and straight behind the setting, all is being with poppyhead after cucumber and custard squash grow up to, fruiting period is long simultaneously, can prolong a wheat harvesting period vegetative period than booth without this medicine, simultaneously without any disease, continuous 2 years, annual income all is surplus in the of 13000 yuan, than without the vicinity of this medicine preferably booth overcharge into more than 6000 yuan, this agricultural chemicals continuous administration effect is best, sprays a medicine and just equals to spray foliage fertilizer one time, seedling system is healthy and strong, look fast, significantly different, various diseases be cannot get up.
Use this agricultural chemicals to reflect the seedling characteristics:
1, crops fruiting rate height must fruit thinning to cucumber, custard squash, every leaf one fruit of cucumber or two fruits, and custard squash one leaf one fruit, fruit long sturdy, poppyhead is not curved, and the taste of fruit well all is the one-level dish.
2, the long strong any illness of failing of seedling, high yield, stable yields.
Example: the villager Shao Changshen of Shao Caiyuan administrative village, Bole town, Chengwu County, Shandong Province, use the situation of this pesticide application cotton: plant two mu of cottons, early stage, arid was serious, prometaphase is overcast and rainy more serious, rainfall is bigger simultaneously, and cotton grows under this disastrous weather, and ripe cotton boll seldom, it is inevitable that the cotton underproduction has become, looks preferably every mu of income of cotton about 500 yuan.But I have sprayed above-mentioned agricultural chemicals in the intermediary and later stages, 300 times of dilutions, agricultural chemicals of spray in every 7-10 days, the leaf that cotton growth comes out is big, thick, bottle green, and the seat peach is many, and cotton boll looks also big, and majority is all so big as duck's egg, and the cotton boll on the fruit branch is all tied fullly, to the top all is cotton boll, really is gratifying, cotton hanging down loosely of all pressing, who has seen that everybody agrees, every mu of income of my cotton is about 1100 yuan then, and the village promotes the use of now, and has all obtained good harvest.
Embodiment 2: Chinese herbal medicine: sulphur 4%: alum 18%: quicklime powder 10%: talcum powder 63%: 5%.
The prescription of Chinese herbal medicine wherein:
Chinese mahonia: 8%; The bletilla striata: 5%; Radix Isatidis: 5%; Mother chrysanthemum: 7%; Cyrtomium fortunei: 6%; Radix ampelopsis: 6%; Kuh-seng: 20%; Chinese violet: 3%; Giant knotweed: 5%; The capsule of weeping forsythia: 4%; Folium isatidis: 3%; Safflower: 5%; Branch: 2%; Subprostrate sophora: 7%; Felwort: 4%; Radix Wikstroemae: 3%; Radix Glycyrrhizae: 4%; Oldenlandia diffusa: 3%.
The process technology scheme that solves its technical problem employing is:
1. sulphur and alum are put into pot and are heated to 100 degrees centigrade, treat that sulphur and alum melt after, stir;
2. 60 order quicklime powders are added in the pot of the sulphur of thawing and alum, with moderate heat the mixture of quicklime powder, sulphur and alum is fried to yellowish-brown, add clear water again with the quicklime powder equivalent weight, boil with moderate heat, and constantly stir, when medicine arsenic reaches thickness, it is taken the dish out of the pot, be placed on and leave standstill in the container; In leaving standstill container, add clear water immediately, medicine arsenic and clear water stirred greater than medicine arsenic two volumes, quiet put 12 hours after, extract supernatant liquor, obtain the semi-finished product liquid first time; Again the quiet sediment of putting gained is put back in the pot, used identical method to boil again, obtain semi-finished product liquid for the second time;
3. put into pot after twice semi-finished product liquid being mixed by same ratio, add the Chinese herbal medicine for preparing, boil, use force earlier and burn after boil, use slow fire instead, boil after 60 minutes and cease fire, pull the medium-height grass dregs of a decoction out;
4. the soup that boils is taken the dish out of the pot, put into special container after the filtration, quietly put clarification in 24 hours, can obtain first finished product soup;
5. with the medium-height grass dregs of a decoction twice-cooked stir-frying of pulling out, add the semi-finished product liquid that mixes by same ratio again, use boils the identical method of Chinese medicine to be carried out boiling the second time, obtains second batch of finished product soup;
6. the finished product soup that boils for twice is mixed by same ratio and stirs, quietly put clarification in 48 hours, obtain final finished, qualified after testing after, get final product canned warehouse-in.
Example: Li Yihuan, Bao Feng township, Chengwu County, Shandong Province woods crossing villager.The situation of above-mentioned agricultural chemicals on probation in wheatland: last year, I was in 3.5 mu of wheatlands, two mu have been used 1.5 kilograms in above-mentioned agricultural chemicals, and two mu of wheats that use above-mentioned agricultural chemicals are received 2136 jin of wheats altogether, remaining 1.5 mu of wheats that do not use above-mentioned agricultural chemicals are received 832 kilograms of wheats altogether.
Administration time and method:
1, sow first three hour and use this agricultural chemicals to soak wheat seeds 10 minutes, agricultural chemicals was by dilution in 1: 300.
2, the unearthed back of wheat seeding two weeks sprays wheat seeding and soil system once with 1: 300 soup, with watering after 1: 300 the soup spray, sprays once continuous three times in later 20 days at the end of 1 year two months.
The growth characteristic of wheat after the medication: wheat was not afraid of and was frozen winter, did point, sent out prosperous spring soon, was not afraid of the spring frost, the wheat blackout, and long strong of seedling, without any defect, it is neat to go out fringe, the satisfying of confession, the wheat rate height, delicious of appearing.
Example: agriculture chemical examination institution, Henan Province and Henan Province face clever county plant protection unit and unite this agricultural chemicals is carried out the test of pesticide effectiveness, 2 years second trials have altogether successively been carried out, its test report result is: 1, experimental field select: test and Selection is faced clever county Ju Ling township oil mill Chen Cun one class capsicum field in Henan Province, pure work, plastic mulching, water and fertilizer condition is good, and kind is that grind No. 2 in Hunan, and the capsicum that infects mosaic virus is tested.2, it is 800 times, 500 times and 300 times with above-mentioned agricultural chemicals dilution.3, planting density, 1 meter of line-spacing; 0.5 meter of spacing in the rows; 1334 strain/mus, 0.7 yuan/kilogram of average price.4, application method: adopt the manual sprayer conventional spray, soup is 60 kilograms after every mu of spray dilution, in capsicum mosaic disease initial stage of origination, executes medicine for the first time on July 1, executes medicine for the second time on July 7, sprays medicine twice altogether, no bad weather effect during the dispenser.5, investigation method: before the dispenser, investigate the disease radix, after the secondary dispenser 7 days, 15 days, 30 days, investigate altogether four times, write down diseased plant numbers at different levels, severity, and, calculate the disease index control efficiency, mu per unit area yield and economic benefit to the double situation of controlling of other disease.6, result of the test: 800 times, 500 times and 300 times, 7 days control efficiency after the pepper virus disease dispenser for the second time is respectively: 59.5%, 63.3%, 67.9%, 15 days control efficiency are respectively after the dispenser for the second time: 65.0%, 68.8%, 75.6%, and 30 days control efficiency are respectively 69.5%, 73.2%, 82.1% after the dispenser for the second time.7, per mu yield and economic benefit: use 800 times, 500 times and 300 times of agricultural chemicals dilutions, and do not use the contrast situation of agricultural chemicals to be respectively: a mu single rate is respectively 3017.9 kilograms/mu, 3134 kilograms/mu, 3381.6 kilograms/mu and 2887.7 kilograms/mu; Mu per unit area yield value is respectively: 2112.5 yuan/mu, 2196.2 yuan/mu, 2367.1 yuan/mu, 2021.4 yuan/mu.8, conclusion: this agricultural chemicals has the better prevention effect to pepper virus disease, and to capsicum safety, the best multiple that uses is 300-500 times.
Embodiment 3: Chinese herbal medicine: sulphur 8%: alum 25%: quicklime powder 20%: talcum powder 45%: 2%.
The prescription of Chinese herbal medicine wherein:
Chinese mahonia: 10%; The bletilla striata: 3%; Radix Isatidis: 4%; Mother chrysanthemum: 5%; Cyrtomium fortunei: 5%; Radix ampelopsis: 3.5%; Kuh-seng: 16%; Chinese violet: 6%; Giant knotweed: 6%; The capsule of weeping forsythia: 4.5%; Folium isatidis: 4%; Safflower: 4%; Branch: 3%; Subprostrate sophora: 8%; Felwort: 5%; Radix Wikstroemae: 4%; Radix Glycyrrhizae: 5%; Oldenlandia diffusa: 4%.
The process technology scheme that solves its technical problem employing is:
1. sulphur and alum are put into pot and are heated to 120 degrees centigrade, treat that sulphur and alum melt after, stir;
2. 120 order quicklime powders are added in the pot of the sulphur of thawing and alum, with moderate heat the mixture of quicklime powder, sulphur and alum is fried to yellowish-brown, add clear water again with the quicklime powder equivalent weight, boil with moderate heat, and constantly stir, when medicine arsenic reaches thickness, it is taken the dish out of the pot, be placed on and leave standstill in the container; In leaving standstill container, add clear water immediately, medicine arsenic and clear water stirred greater than medicine arsenic two volumes, quiet put 36 hours after, extract supernatant liquor, obtain the semi-finished product liquid first time; The quiet sediment of putting gained is put back in the pot again, used identical method to boil again, obtain semi-finished product liquid for the second time;
3. put into pot after twice semi-finished product liquid being mixed by same ratio, add the Chinese herbal medicine for preparing, boil, use force earlier and burn after boil, use slow fire instead, boil after 40 minutes and cease fire, pull the medium-height grass dregs of a decoction out;
4. the soup that boils is taken the dish out of the pot, put into special container after the filtration, quietly put clarification in 24 hours, can obtain first finished product soup;
5. with the medium-height grass dregs of a decoction twice-cooked stir-frying of pulling out, add the semi-finished product liquid that mixes by same ratio again, carry out boiling the second time, method is the same, obtains second batch of finished product soup;
6. the finished product soup that boils for twice is mixed by same ratio and stirs, quietly put clarification in 12 hours, obtain final finished, qualified after testing after, get final product canned warehouse-in.
The experimenter: it is living that rural area, building people Ni Dong opens the Chengwu County in the Shandong Province, the situation of using above-mentioned agricultural chemicals that bird is used, and this agricultural chemicals all has unique control efficiency to poultry.The sick pest of bird have taken place in the surrounding area, and as: bird pestilence, red, dysentery characterized by white mucous stool etc., chicken, duck, goose in morbidity a few days ago for pre-diseases prevention pest involve, with the dilution in 1: 300 in proportion of above-mentioned agricultural chemicals, mix food or use for bird as drinking water to bird.All do not have infected, morbidity for the chicken of having used this agricultural chemicals, duck, goose, chicken, duck, geese are ridden out the sick pest phase of bird.Its using method: 1, mix that food is fed or as drinking water all by 1: 300 times of dilution.2, spraying disinfection is carried out in the life place of bird.
The experimenter: deputy director director Cai of Chengwu County, the Shandong Province National People's Congress, the situation of using above-mentioned agricultural chemicals that domestic animals are used, this agricultural chemicals also has special good result of treatment to the trauma infection contamination of animal class.For cat, dog, pig, ox, sheep, during because of symptoms such as wound inflammation, infection, use pure stoste to spread upon infection place of animal wound, get final product, cure after the week for one day 1-3 time.
Claims (2)
1, a kind of prescription of environment friendly agricultural is characterized in that:
Chinese herbal medicine: sulphur 4%~8%: alum 18%~25%: quicklime powder 10%~20%: talcum powder 45%~63%: 2%~5%;
The prescription of Chinese herbal medicine wherein:
Chinese mahonia: 7%-10%; The bletilla striata: 2%-5%; Radix Isatidis: 3%-5%; Mother chrysanthemum: 4%-7%; Cyrtomium fortunei: 4%-6%; Radix ampelopsis: 3%-6%; Kuh-seng: 15%-20%; Chinese violet: 3%-6%; Giant knotweed: 4%-6%; The capsule of weeping forsythia: 4%-7%; Folium isatidis: 3%-5%; Safflower: 3%-5%; Branch: 2%-4%; Subprostrate sophora: 7%-10%; Felwort: 4%-6%; Radix Wikstroemae: 3%-5%; Radix Glycyrrhizae: 4%-7%; Oldenlandia diffusa: 3%-5%.
2, a kind of production technology of environment friendly agricultural is characterized in that:
1. sulphur and alum are put into pot and are heated to 100-120 degree centigrade, treat that sulphur and alum melt after, stir;
2. with quicklime powder 60 orders-100 order, be added in the pot of the sulphur of thawing and alum, with moderate heat the mixture of quicklime powder, sulphur and alum is fried to yellowish-brown, add clear water again with the quicklime powder equivalent weight, boil with moderate heat, and constantly stir, when medicine arsenic reaches thickness, it is taken the dish out of the pot, be placed on and leave standstill in the container; In leaving standstill container, add clear water immediately, medicine arsenic and clear water stirred greater than medicine arsenic two volumes, quiet put 12-36 hour after, the extraction supernatant liquor is semi-finished product liquid;
3. semi-finished product liquid is put into pot, add the Chinese herbal medicine prepare again, boil, use force earlier and burn after boil, use slow fire instead, boil after 40-60 minute and cease fire, pull the medium-height grass dregs of a decoction out;
4. the soup that boils is taken the dish out of the pot, puts into special container after the filtration, quietly put clarification in 24-48 hour, can obtain the finished product soup, qualified after testing after, can canned warehouse-in.
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CN100379344C (en) | 2008-04-09 |
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