CN1747987A - 环氧官能的杂化共聚物 - Google Patents
环氧官能的杂化共聚物 Download PDFInfo
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- CN1747987A CN1747987A CNA2003801097786A CN200380109778A CN1747987A CN 1747987 A CN1747987 A CN 1747987A CN A2003801097786 A CNA2003801097786 A CN A2003801097786A CN 200380109778 A CN200380109778 A CN 200380109778A CN 1747987 A CN1747987 A CN 1747987A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/48—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms
- C08G77/50—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule in which at least two but not all the silicon atoms are connected by linkages other than oxygen atoms by carbon linkages
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/42—Block-or graft-polymers containing polysiloxane sequences
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/22—Di-epoxy compounds
- C08G59/30—Di-epoxy compounds containing atoms other than carbon, hydrogen, oxygen and nitrogen
- C08G59/306—Di-epoxy compounds containing atoms other than carbon, hydrogen, oxygen and nitrogen containing silicon
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/32—Epoxy compounds containing three or more epoxy groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/32—Epoxy compounds containing three or more epoxy groups
- C08G59/3254—Epoxy compounds containing three or more epoxy groups containing atoms other than carbon, hydrogen, oxygen or nitrogen
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Silicon Polymers (AREA)
- Epoxy Resins (AREA)
- Sealing Material Composition (AREA)
- Paints Or Removers (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
Description
环氧树脂 | 饱和质量增益(%) | 备注 |
Epon 828a | 1.85 | 脆、硬、褐色 |
ERL 4221b | 5.19 | 非常脆、褐色 |
TBPASiCHO-G1-Siloxane,2 | 0.42 | 易弯曲、褐色 |
TBPASiCH0-G1-Silane,4 | 0.35 | 易弯曲、褐色 |
BPASiCHO,7 | 0.65 | 可弯曲、褐色 |
BPASiGE,8 | 0.87 | 可弯曲、褐色 |
样品 | 未固化1%重量损失的温度(℃) | 未固化10%重量损失的温度(℃) | 未固化300℃/30min后剩余重量(%) | 已固化1%重量损失的温度(℃) | 已固化10%重量损失的温度(℃) | 已固化300℃/30min后剩余重量(%) |
EPON828 | 206 | 249 | 11 | 149 | 279 | 46 |
ERL-4221 | 119 | 167 | 1.4 | 143 | 279 | 50 |
BPASiGE,8 | 135 | 265 | 44 | 203 | 295 | 83 |
BPASiCHO,7 | 182 | 大于300 | 77 | 219 | 300 | 79 |
TBPASiCHO-G1-Siloxane,2 | 244 | 大于300 | 96 | 248 | 300 | 78 |
TBPASiCHO-G1-Silane,4 | 270 | 大于300 | 97 | 208 | 295 | 80 |
树脂共混组合物 | 初始澄明度 | 混合物稳定性 | 备注 |
50%杂化环氧树脂2,50%SycarSiloxane | 澄明 | 72h/r.t.后澄明 | 两种树脂基本上完全混溶 |
2%杂化环氧树脂2,98%ERL4221 | 澄明 | 72h/r.t.后澄明 | 两种树脂宏观上混溶 |
5%杂化环氧树脂2,95%ERL4221 | 澄明 | 72h/r.t.后澄明 | 两种树脂宏观上混溶 |
10%杂化环氧树脂2,90%ERL4221 | 澄明 | 72h/r.t.后澄明 | 两种树脂宏观上混溶 |
2%杂化环氧树脂2,98%Epon 828 | 模糊 | 72h/r.t.后模糊;与初始外观无差别 | 混合物模糊,但无明显整体分离 |
5%杂化环氧树脂2,95%Epon 828 | 模糊 | 72h/r.t.后模糊;与初始外观无差别 | 混合物模糊,但无明显整体分离 |
10%杂化环氧树脂2,90%Epon 828 | 混浊 | 168h/r.t.后混浊;与初始外观无差别 | 混合物混浊,但未观察到整体分离 |
80%杂化环氧树脂2,20%液体马来酰亚胺/乙烯基醚共混物 | 轻微模糊 | 72h/r.t.后轻微模糊;与初始外观无差别 | 树脂体系在宏观上相容 |
90%杂化环氧树脂2,10%CHVE乙烯醚(IsP) | 澄明 | 澄明 | 两种树脂在大多数比例相容 |
80%杂化环氧树脂2,20%CHVE乙烯醚(ISP) | 澄明 | 澄明 | 两种树脂在大多数比例相容 |
90%Epon828,10%EMS-232(Gelest) | 混浊 | 60h/r.t.内整体相分离 | 清楚地观察到整体相分离 |
环氧树脂供混物 | ~E’@-50℃(×10-9Pa) | ~E’@25℃(×10-9Pa) | ~Tg(℃) |
100%Epon 828 | 2.1 | 2.0 | 190 |
95∶5Epon 828∶2 | 2.0 | 1.8 | 180 |
90∶10Epon 828∶2 | 1.5 | 1.0 | 165 |
100%TBPASiCHO-G1-siloxane 2 | 1.1 | 1.0 | 80 |
配混物 | 剪切强度(Kg)(固化:UV+70℃/10min) | 剪切强度(Kg)(固化:UV+175℃/1h) |
30-1(辐射状杂化2) | 12.3 | 44.6 |
30-2(Epon 828) | 22.9 | 33.7 |
Claims (57)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/327,353 US7034089B2 (en) | 2002-12-20 | 2002-12-20 | Epoxy-functional hybrid copolymers |
US10/327,353 | 2002-12-20 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1747987A true CN1747987A (zh) | 2006-03-15 |
CN100396716C CN100396716C (zh) | 2008-06-25 |
Family
ID=32594230
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB2003801097786A Expired - Fee Related CN100396716C (zh) | 2002-12-20 | 2003-12-08 | 环氧官能的杂化共聚物 |
Country Status (7)
Country | Link |
---|---|
US (1) | US7034089B2 (zh) |
EP (1) | EP1572781A1 (zh) |
JP (1) | JP4607600B2 (zh) |
KR (1) | KR20050085802A (zh) |
CN (1) | CN100396716C (zh) |
AU (1) | AU2003296306A1 (zh) |
WO (1) | WO2004060976A1 (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101460537B (zh) * | 2006-06-07 | 2012-07-04 | 昭和电工株式会社 | 新型环氧化合物及其制备方法 |
CN107814935A (zh) * | 2017-10-31 | 2018-03-20 | 江南大学 | 一种poss基有机‑无机杂化八臂环氧树脂及其制备方法 |
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JP4758230B2 (ja) * | 2003-09-18 | 2011-08-24 | 株式会社カネカ | 末端にエポキシ基および/またはオキセタン基含有ケイ素基を有する有機重合体を含む光硬化性組成物、それから得られる硬化物、及び製造方法 |
US7365135B2 (en) * | 2004-06-14 | 2008-04-29 | Chung-Shan Institute Of Science & Technology | Method for preparing a novolac phenolic resin/silica hybrid organic-inorganic nanocomposite |
US20050282976A1 (en) * | 2004-06-22 | 2005-12-22 | Gelcore Llc. | Silicone epoxy formulations |
DE102005009066A1 (de) * | 2005-02-28 | 2006-09-07 | Osram Opto Semiconductors Gmbh | Verfahren zur Herstellung eines optischen und eines strahlungsemittierenden Bauelementes und optisches sowie strahlungsemittierendes Bauelement |
DE102005027404A1 (de) * | 2005-06-13 | 2006-12-14 | Schröders, Theo | Brandschutzglas und Verfahren zu dessen Herstellung |
KR100779560B1 (ko) | 2006-07-20 | 2007-11-29 | 연세대학교 산학협력단 | 유기 박막 트랜지스터용 자가 패턴성 유전체 박막, 그 제조 방법, 및 이를 구비한 유기 박막 트랜지스터 |
US8084765B2 (en) * | 2007-05-07 | 2011-12-27 | Xerox Corporation | Electronic device having a dielectric layer |
CN102961794B (zh) * | 2007-08-20 | 2015-08-05 | 利贝尔-弗拉施姆有限公司 | 流体驱动医用注射器 |
US8604150B2 (en) * | 2007-11-07 | 2013-12-10 | Showa Denko K.K. | Epoxy group-containing organosiloxane compound, curable composition for transfer materials and method for forming micropattern using the composition |
EP2270020B1 (en) * | 2008-03-24 | 2014-03-19 | Showa Denko K.K. | Epoxy compound and process for producing the epoxy compound |
US20100119796A1 (en) * | 2008-11-12 | 2010-05-13 | Brighten Engineering Co., Ltd. | Anticorrosive Nanocomposite Coating Material, and a Preparation Process Thereof |
EP2445028A1 (en) * | 2010-10-25 | 2012-04-25 | Nederlandse Organisatie voor toegepast -natuurwetenschappelijk onderzoek TNO | Opto-electric device and method of manufacturing an opto-electric device |
KR101252063B1 (ko) | 2011-08-25 | 2013-04-12 | 한국생산기술연구원 | 알콕시실릴기를 갖는 에폭시 화합물, 이의 제조 방법, 이를 포함하는 조성물과 경화물 및 이의 용도 |
WO2015041325A1 (ja) * | 2013-09-20 | 2015-03-26 | 信越化学工業株式会社 | シリコーン変性エポキシ樹脂およびその組成物と硬化物 |
KR102315127B1 (ko) * | 2014-11-26 | 2021-10-20 | 에스케이이노베이션 주식회사 | 하드코팅층 형성용 조성물 |
CN107849223B (zh) | 2015-07-10 | 2020-07-28 | 住友精化株式会社 | 环氧树脂组合物、其制造方法、以及该组合物的用途 |
JP6553312B2 (ja) | 2017-01-10 | 2019-07-31 | 住友精化株式会社 | エポキシ樹脂組成物 |
EP3569627A4 (en) | 2017-01-10 | 2020-07-22 | Sumitomo Seika Chemicals Co. Ltd. | EPOXY RESIN COMPOSITION |
KR102459581B1 (ko) | 2017-01-10 | 2022-10-27 | 스미토모 세이카 가부시키가이샤 | 에폭시 수지 조성물 |
WO2018131563A1 (ja) | 2017-01-10 | 2018-07-19 | 住友精化株式会社 | エポキシ樹脂組成物 |
KR102126045B1 (ko) * | 2017-07-21 | 2020-06-23 | 삼성에스디아이 주식회사 | 유기발광소자 봉지용 조성물 및 이로부터 제조된 유기발광소자 표시장치 |
EP3578591A1 (en) | 2018-06-04 | 2019-12-11 | EMPA Eidgenössische Materialprüfungs- und Forschungsanstalt | Polymeric liquid molecular building block (mbb) material and method for producing the same |
KR102232340B1 (ko) | 2019-11-15 | 2021-03-26 | 한국생산기술연구원 | 알콕시실릴기를 갖는 에폭시 수지의 조성물 및 이의 복합체 |
CN111454689B (zh) * | 2019-12-31 | 2021-10-15 | 武汉长盈鑫科技有限公司 | 一种高玻璃化温度的导热胶及其制备方法 |
CN117003991A (zh) * | 2022-04-29 | 2023-11-07 | 华为技术有限公司 | 环氧树脂及其制备方法和树脂组合物 |
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-
2002
- 2002-12-20 US US10/327,353 patent/US7034089B2/en not_active Expired - Fee Related
-
2003
- 2003-12-08 WO PCT/US2003/038875 patent/WO2004060976A1/en active Application Filing
- 2003-12-08 CN CNB2003801097786A patent/CN100396716C/zh not_active Expired - Fee Related
- 2003-12-08 JP JP2004565245A patent/JP4607600B2/ja not_active Expired - Fee Related
- 2003-12-08 KR KR1020057011443A patent/KR20050085802A/ko active IP Right Grant
- 2003-12-08 EP EP03814660A patent/EP1572781A1/en not_active Withdrawn
- 2003-12-08 AU AU2003296306A patent/AU2003296306A1/en not_active Abandoned
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101460537B (zh) * | 2006-06-07 | 2012-07-04 | 昭和电工株式会社 | 新型环氧化合物及其制备方法 |
CN107814935A (zh) * | 2017-10-31 | 2018-03-20 | 江南大学 | 一种poss基有机‑无机杂化八臂环氧树脂及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
JP4607600B2 (ja) | 2011-01-05 |
US20040122186A1 (en) | 2004-06-24 |
US7034089B2 (en) | 2006-04-25 |
WO2004060976A1 (en) | 2004-07-22 |
CN100396716C (zh) | 2008-06-25 |
KR20050085802A (ko) | 2005-08-29 |
JP2006511664A (ja) | 2006-04-06 |
AU2003296306A1 (en) | 2004-07-29 |
EP1572781A1 (en) | 2005-09-14 |
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