CN1663714A - 制备纳米金溶液的方法 - Google Patents
制备纳米金溶液的方法 Download PDFInfo
- Publication number
- CN1663714A CN1663714A CN 200410089252 CN200410089252A CN1663714A CN 1663714 A CN1663714 A CN 1663714A CN 200410089252 CN200410089252 CN 200410089252 CN 200410089252 A CN200410089252 A CN 200410089252A CN 1663714 A CN1663714 A CN 1663714A
- Authority
- CN
- China
- Prior art keywords
- solution
- gold
- hydrazine hydrate
- aqueous solution
- nano
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 9
- 239000010931 gold Substances 0.000 title claims description 49
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 title abstract description 31
- 229910052737 gold Inorganic materials 0.000 title description 30
- 239000000243 solution Substances 0.000 claims abstract description 21
- NWZSZGALRFJKBT-KNIFDHDWSA-N (2s)-2,6-diaminohexanoic acid;(2s)-2-hydroxybutanedioic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O.NCCCC[C@H](N)C(O)=O NWZSZGALRFJKBT-KNIFDHDWSA-N 0.000 claims abstract description 18
- 239000007864 aqueous solution Substances 0.000 claims abstract description 18
- IKDUDTNKRLTJSI-UHFFFAOYSA-N hydrazine monohydrate Substances O.NN IKDUDTNKRLTJSI-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 17
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims abstract description 12
- 239000008367 deionised water Substances 0.000 claims abstract description 9
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- FDWREHZXQUYJFJ-UHFFFAOYSA-M gold monochloride Chemical compound [Cl-].[Au+] FDWREHZXQUYJFJ-UHFFFAOYSA-M 0.000 claims description 18
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 claims description 10
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 10
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims description 10
- 239000011259 mixed solution Substances 0.000 claims description 8
- SJUCACGNNJFHLB-UHFFFAOYSA-N O=C1N[ClH](=O)NC2=C1NC(=O)N2 Chemical compound O=C1N[ClH](=O)NC2=C1NC(=O)N2 SJUCACGNNJFHLB-UHFFFAOYSA-N 0.000 abstract 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 1
- 239000002245 particle Substances 0.000 description 13
- FUSNOPLQVRUIIM-UHFFFAOYSA-N 4-amino-2-(4,4-dimethyl-2-oxoimidazolidin-1-yl)-n-[3-(trifluoromethyl)phenyl]pyrimidine-5-carboxamide Chemical compound O=C1NC(C)(C)CN1C(N=C1N)=NC=C1C(=O)NC1=CC=CC(C(F)(F)F)=C1 FUSNOPLQVRUIIM-UHFFFAOYSA-N 0.000 description 3
- 229910000377 hydrazine sulfate Inorganic materials 0.000 description 3
- 239000012493 hydrazine sulfate Substances 0.000 description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000002003 electron diffraction Methods 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- -1 pottery Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Landscapes
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2004100892522A CN1302882C (zh) | 2004-12-02 | 2004-12-02 | 制备纳米金溶液的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2004100892522A CN1302882C (zh) | 2004-12-02 | 2004-12-02 | 制备纳米金溶液的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1663714A true CN1663714A (zh) | 2005-09-07 |
CN1302882C CN1302882C (zh) | 2007-03-07 |
Family
ID=35035130
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB2004100892522A Expired - Fee Related CN1302882C (zh) | 2004-12-02 | 2004-12-02 | 制备纳米金溶液的方法 |
Country Status (1)
Country | Link |
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CN (1) | CN1302882C (zh) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100425372C (zh) * | 2005-09-09 | 2008-10-15 | 吉林大学 | 一种免疫层析检测用单分散金纳米粒子的制备方法 |
WO2015125980A1 (en) * | 2014-02-21 | 2015-08-27 | Kim Il Sung University | Nanogold injection and its manufacturing method |
CN105033281A (zh) * | 2015-08-27 | 2015-11-11 | 华南理工大学 | 一种简易环保型纳米金颗粒溶液的制备方法 |
CN107965263A (zh) * | 2017-12-21 | 2018-04-27 | 大连轶德科技有限公司 | 多功能卫生环保纱窗及其制备方法 |
CN108941612A (zh) * | 2018-09-27 | 2018-12-07 | 天津工业大学 | 一种尺寸可控的小粒径金纳米粒子的制备方法 |
CN109811545A (zh) * | 2017-11-21 | 2019-05-28 | 广州泓一生物科技有限公司 | 一种纳米金柔顺剂及其制备方法 |
CN113351876A (zh) * | 2021-04-21 | 2021-09-07 | 南京大学 | 一种制备水溶性纳米金的方法 |
CN115501917A (zh) * | 2022-11-01 | 2022-12-23 | 航天科工(长沙)新材料研究院有限公司 | 一种纳米金催化剂及其制备方法 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100472496B1 (ko) * | 1997-07-23 | 2005-05-16 | 삼성에스디아이 주식회사 | 투명도전성조성물,이로부터형성된투명도전막및그제조방법 |
CN1101288C (zh) * | 1999-01-21 | 2003-02-12 | 中国科学技术大学 | 一种纳米金属粉的制备方法 |
CN1155448C (zh) * | 2000-04-28 | 2004-06-30 | 南京大学 | 一种纳米级金粉的制备方法 |
CN1247708C (zh) * | 2003-03-11 | 2006-03-29 | 中国科学院固体物理研究所 | 纳米金/介孔二氧化硅复合体及制备方法 |
KR100532695B1 (ko) * | 2003-03-14 | 2005-11-30 | 한국화학연구원 | 고농도 초미세 금속입자 용액의 제조방법 |
CN1260025C (zh) * | 2003-07-15 | 2006-06-21 | 武汉大学 | 一种金纳米粒子的制备方法 |
-
2004
- 2004-12-02 CN CNB2004100892522A patent/CN1302882C/zh not_active Expired - Fee Related
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100425372C (zh) * | 2005-09-09 | 2008-10-15 | 吉林大学 | 一种免疫层析检测用单分散金纳米粒子的制备方法 |
WO2015125980A1 (en) * | 2014-02-21 | 2015-08-27 | Kim Il Sung University | Nanogold injection and its manufacturing method |
CN105033281A (zh) * | 2015-08-27 | 2015-11-11 | 华南理工大学 | 一种简易环保型纳米金颗粒溶液的制备方法 |
CN105033281B (zh) * | 2015-08-27 | 2017-10-20 | 华南理工大学 | 一种简易环保型纳米金颗粒溶液的制备方法 |
CN109811545A (zh) * | 2017-11-21 | 2019-05-28 | 广州泓一生物科技有限公司 | 一种纳米金柔顺剂及其制备方法 |
CN107965263A (zh) * | 2017-12-21 | 2018-04-27 | 大连轶德科技有限公司 | 多功能卫生环保纱窗及其制备方法 |
CN108941612A (zh) * | 2018-09-27 | 2018-12-07 | 天津工业大学 | 一种尺寸可控的小粒径金纳米粒子的制备方法 |
CN113351876A (zh) * | 2021-04-21 | 2021-09-07 | 南京大学 | 一种制备水溶性纳米金的方法 |
CN115501917A (zh) * | 2022-11-01 | 2022-12-23 | 航天科工(长沙)新材料研究院有限公司 | 一种纳米金催化剂及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
CN1302882C (zh) | 2007-03-07 |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: SHANGHAI HUASHI NANO MATERIALS CO., LTD. Free format text: FORMER OWNER: HUANG DEHUAN Effective date: 20080404 |
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Effective date of registration: 20080404 Address after: A building, Xin Mei Industrial Zone, No. 260 Lian Cao Road, Shanghai, Minhang District Patentee after: Shanghai Huashi Nano Material Co., Ltd. Address before: Room 13, No. 288, Lane 301, Macao Road, Shanghai, Putuo District Patentee before: Huang Dehuan |
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Granted publication date: 20070307 Termination date: 20111202 |