CN1507433A - 烷基-n-(3-二甲氨基)烷基氨基甲酸酯的制备方法 - Google Patents
烷基-n-(3-二甲氨基)烷基氨基甲酸酯的制备方法 Download PDFInfo
- Publication number
- CN1507433A CN1507433A CNA028093399A CN02809339A CN1507433A CN 1507433 A CN1507433 A CN 1507433A CN A028093399 A CNA028093399 A CN A028093399A CN 02809339 A CN02809339 A CN 02809339A CN 1507433 A CN1507433 A CN 1507433A
- Authority
- CN
- China
- Prior art keywords
- propyl
- dimethylamino
- alkyl
- alcohol
- carbamate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title claims abstract description 5
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical group CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 14
- -1 alkyl carbamate Chemical compound 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 150000002191 fatty alcohols Chemical class 0.000 claims description 6
- 239000003960 organic solvent Substances 0.000 claims description 5
- 239000002904 solvent Substances 0.000 claims description 3
- 239000003153 chemical reaction reagent Substances 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 10
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 21
- IUNMPGNGSSIWFP-UHFFFAOYSA-N dimethylaminopropylamine Chemical compound CN(C)CCCN IUNMPGNGSSIWFP-UHFFFAOYSA-N 0.000 description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
- 239000012442 inert solvent Substances 0.000 description 4
- YNTOKMNHRPSGFU-UHFFFAOYSA-N n-Propyl carbamate Chemical compound CCCOC(N)=O YNTOKMNHRPSGFU-UHFFFAOYSA-N 0.000 description 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 239000012046 mixed solvent Substances 0.000 description 2
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- BZLVMXJERCGZMT-UHFFFAOYSA-N Methyl tert-butyl ether Chemical compound COC(C)(C)C BZLVMXJERCGZMT-UHFFFAOYSA-N 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 229940031815 mycocide Drugs 0.000 description 1
- SNMVRZFUUCLYTO-UHFFFAOYSA-N n-propyl chloride Chemical compound CCCCl SNMVRZFUUCLYTO-UHFFFAOYSA-N 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C269/00—Preparation of derivatives of carbamic acid, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
- C07C269/04—Preparation of derivatives of carbamic acid, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups from amines with formation of carbamate groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C07C255/45—Carboxylic acid nitriles having cyano groups bound to carbon atoms of rings other than six-membered aromatic rings
- C07C255/46—Carboxylic acid nitriles having cyano groups bound to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of non-condensed rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
Description
Claims (6)
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP01110711.7 | 2001-05-03 | ||
EP01110711A EP1254894A1 (en) | 2001-05-03 | 2001-05-03 | Process for the preparation of propamocarb |
EP01113778A EP1264824A1 (en) | 2001-06-06 | 2001-06-06 | Preparation of alkyl-N-(3-dimethylamino)alkylcarbamates |
EP01113778.3 | 2001-06-06 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1507433A true CN1507433A (zh) | 2004-06-23 |
CN1246305C CN1246305C (zh) | 2006-03-22 |
Family
ID=26076565
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB028093399A Expired - Lifetime CN1246305C (zh) | 2001-05-03 | 2002-04-18 | 烷基-n-(3-二甲氨基)烷基氨基甲酸酯的制备方法 |
Country Status (21)
Country | Link |
---|---|
US (1) | US6872847B2 (zh) |
EP (1) | EP1383737B1 (zh) |
JP (1) | JP4261915B2 (zh) |
KR (1) | KR100867910B1 (zh) |
CN (1) | CN1246305C (zh) |
AT (1) | ATE386015T1 (zh) |
AU (1) | AU2002314078B2 (zh) |
BR (1) | BR0209410A (zh) |
CA (1) | CA2443820C (zh) |
CZ (1) | CZ299629B6 (zh) |
DE (1) | DE60224998T2 (zh) |
DK (1) | DK1383737T3 (zh) |
ES (1) | ES2301649T3 (zh) |
HU (1) | HUP0303821A3 (zh) |
IL (2) | IL158015A0 (zh) |
MX (1) | MXPA03010032A (zh) |
PL (1) | PL203712B1 (zh) |
PT (1) | PT1383737E (zh) |
SK (1) | SK287055B6 (zh) |
TW (1) | TWI247732B (zh) |
WO (1) | WO2002090322A1 (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101548682B (zh) * | 2009-04-14 | 2012-07-25 | 陕西恒田化工有限公司 | 一种合成722克/升霜霉威盐酸盐的方法 |
CN108218745A (zh) * | 2018-03-12 | 2018-06-29 | 浙江禾本科技有限公司 | 一种霜霉威盐酸盐合成配方及其合成方法 |
CN113563230A (zh) * | 2020-08-24 | 2021-10-29 | 江苏禾本生化有限公司 | 一种霜霉威盐酸盐原药的制备方法 |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BR112019006239A2 (pt) * | 2016-10-31 | 2019-06-18 | Eastman Chem Co | processo para preparar 3-(dimetilamino)propilcarbamato de propila. |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL157191C (nl) * | 1966-12-17 | Schering Ag | Werkwijze voor het bereiden van een preparaat met fungicide en fungistatische werking. | |
DE4133516A1 (de) * | 1991-10-10 | 1993-04-15 | Bayer Ag | Verfahren zur herstellung von n-(hydroxyalkyl)-carbamidsaeure-alkylestern |
-
2002
- 2002-04-18 AU AU2002314078A patent/AU2002314078B2/en not_active Ceased
- 2002-04-18 MX MXPA03010032A patent/MXPA03010032A/es active IP Right Grant
- 2002-04-18 CA CA002443820A patent/CA2443820C/en not_active Expired - Fee Related
- 2002-04-18 DE DE60224998T patent/DE60224998T2/de not_active Expired - Lifetime
- 2002-04-18 PL PL366847A patent/PL203712B1/pl not_active IP Right Cessation
- 2002-04-18 BR BR0209410-0A patent/BR0209410A/pt not_active Application Discontinuation
- 2002-04-18 ES ES02740612T patent/ES2301649T3/es not_active Expired - Lifetime
- 2002-04-18 AT AT02740612T patent/ATE386015T1/de active
- 2002-04-18 DK DK02740612T patent/DK1383737T3/da active
- 2002-04-18 WO PCT/EP2002/005456 patent/WO2002090322A1/en active IP Right Grant
- 2002-04-18 HU HU0303821A patent/HUP0303821A3/hu unknown
- 2002-04-18 SK SK1477-2003A patent/SK287055B6/sk not_active IP Right Cessation
- 2002-04-18 EP EP02740612A patent/EP1383737B1/en not_active Expired - Lifetime
- 2002-04-18 CZ CZ20033261A patent/CZ299629B6/cs not_active IP Right Cessation
- 2002-04-18 IL IL15801502A patent/IL158015A0/xx unknown
- 2002-04-18 JP JP2002587402A patent/JP4261915B2/ja not_active Expired - Lifetime
- 2002-04-18 US US10/476,706 patent/US6872847B2/en not_active Expired - Lifetime
- 2002-04-18 PT PT02740612T patent/PT1383737E/pt unknown
- 2002-04-18 KR KR1020037014063A patent/KR100867910B1/ko active IP Right Grant
- 2002-04-18 CN CNB028093399A patent/CN1246305C/zh not_active Expired - Lifetime
- 2002-04-24 TW TW091108426A patent/TWI247732B/zh not_active IP Right Cessation
-
2003
- 2003-09-18 IL IL158015A patent/IL158015A/en unknown
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101548682B (zh) * | 2009-04-14 | 2012-07-25 | 陕西恒田化工有限公司 | 一种合成722克/升霜霉威盐酸盐的方法 |
CN108218745A (zh) * | 2018-03-12 | 2018-06-29 | 浙江禾本科技有限公司 | 一种霜霉威盐酸盐合成配方及其合成方法 |
CN113563230A (zh) * | 2020-08-24 | 2021-10-29 | 江苏禾本生化有限公司 | 一种霜霉威盐酸盐原药的制备方法 |
Also Published As
Publication number | Publication date |
---|---|
JP4261915B2 (ja) | 2009-05-13 |
ATE386015T1 (de) | 2008-03-15 |
PT1383737E (pt) | 2008-03-17 |
DK1383737T3 (da) | 2008-03-17 |
ES2301649T3 (es) | 2008-07-01 |
AU2002314078B2 (en) | 2007-01-11 |
KR20030094370A (ko) | 2003-12-11 |
IL158015A0 (en) | 2004-03-28 |
CA2443820A1 (en) | 2002-11-14 |
DE60224998D1 (de) | 2008-03-27 |
CZ20033261A3 (en) | 2004-03-17 |
JP2004526801A (ja) | 2004-09-02 |
CA2443820C (en) | 2009-08-18 |
US20040152914A1 (en) | 2004-08-05 |
HUP0303821A3 (en) | 2007-02-28 |
SK287055B6 (sk) | 2009-10-07 |
TWI247732B (en) | 2006-01-21 |
PL366847A1 (en) | 2005-02-07 |
WO2002090322A1 (en) | 2002-11-14 |
BR0209410A (pt) | 2004-07-06 |
KR100867910B1 (ko) | 2008-11-10 |
US6872847B2 (en) | 2005-03-29 |
EP1383737A1 (en) | 2004-01-28 |
SK14772003A3 (sk) | 2004-05-04 |
DE60224998T2 (de) | 2009-02-05 |
MXPA03010032A (es) | 2004-02-27 |
HUP0303821A2 (hu) | 2004-03-29 |
PL203712B1 (pl) | 2009-11-30 |
IL158015A (en) | 2009-05-04 |
EP1383737B1 (en) | 2008-02-13 |
CZ299629B6 (cs) | 2008-09-24 |
CN1246305C (zh) | 2006-03-22 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C56 | Change in the name or address of the patentee |
Owner name: BAYER CROPSCIENCE AG Free format text: FORMER NAME OR ADDRESS: BAYER AGROSCIENCE GMBH |
|
CP01 | Change in the name or title of a patent holder |
Address after: Frankfurt, Germany Patentee after: Bayer Cropscience SA Address before: Frankfurt, Germany Patentee before: Bayer Agroscience GmbH |
|
TR01 | Transfer of patent right |
Effective date of registration: 20180408 Address after: German Monheim Patentee after: Bayer Pharma Aktiengesellschaft Address before: Frankfurt, Germany Patentee before: Bayer Cropscience SA |
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TR01 | Transfer of patent right | ||
CX01 | Expiry of patent term |
Granted publication date: 20060322 |
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CX01 | Expiry of patent term |