CN1429266A - 发酵麦芽饮料用麦汁的制造方法 - Google Patents
发酵麦芽饮料用麦汁的制造方法 Download PDFInfo
- Publication number
- CN1429266A CN1429266A CN01809401A CN01809401A CN1429266A CN 1429266 A CN1429266 A CN 1429266A CN 01809401 A CN01809401 A CN 01809401A CN 01809401 A CN01809401 A CN 01809401A CN 1429266 A CN1429266 A CN 1429266A
- Authority
- CN
- China
- Prior art keywords
- wheat juice
- time
- wort
- fermented malt
- flavor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 78
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 title claims abstract description 38
- 230000008569 process Effects 0.000 title abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 64
- 238000001914 filtration Methods 0.000 claims abstract description 62
- 230000015556 catabolic process Effects 0.000 claims abstract description 14
- 238000006731 degradation reaction Methods 0.000 claims abstract description 14
- 159000000007 calcium salts Chemical class 0.000 claims abstract description 11
- 150000007524 organic acids Chemical class 0.000 claims abstract description 9
- BSAIUMLZVGUGKX-BQYQJAHWSA-N (E)-non-2-enal Chemical compound CCCCCC\C=C\C=O BSAIUMLZVGUGKX-BQYQJAHWSA-N 0.000 claims abstract description 6
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 180
- 241000209140 Triticum Species 0.000 claims description 179
- 235000021307 Triticum Nutrition 0.000 claims description 179
- 239000000796 flavoring agent Substances 0.000 claims description 79
- 235000019634 flavors Nutrition 0.000 claims description 79
- 230000006866 deterioration Effects 0.000 claims description 67
- 239000000463 material Substances 0.000 claims description 61
- 238000004519 manufacturing process Methods 0.000 claims description 49
- 238000012545 processing Methods 0.000 claims description 35
- 235000021577 malt beverage Nutrition 0.000 claims description 33
- 230000009467 reduction Effects 0.000 claims description 27
- 238000000855 fermentation Methods 0.000 claims description 12
- 230000004151 fermentation Effects 0.000 claims description 12
- 235000014101 wine Nutrition 0.000 claims description 12
- 230000005764 inhibitory process Effects 0.000 claims description 9
- 239000000126 substance Substances 0.000 claims description 9
- BSAIUMLZVGUGKX-UHFFFAOYSA-N 2-Nonenal Natural products CCCCCCC=CC=O BSAIUMLZVGUGKX-UHFFFAOYSA-N 0.000 claims description 4
- 238000010828 elution Methods 0.000 abstract 1
- 235000005985 organic acids Nutrition 0.000 abstract 1
- 235000013405 beer Nutrition 0.000 description 29
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 11
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 10
- 235000015040 sparkling wine Nutrition 0.000 description 10
- 238000012360 testing method Methods 0.000 description 9
- 239000007788 liquid Substances 0.000 description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 6
- 239000003205 fragrance Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 230000003647 oxidation Effects 0.000 description 6
- 238000007254 oxidation reaction Methods 0.000 description 6
- 239000004310 lactic acid Substances 0.000 description 5
- 235000014655 lactic acid Nutrition 0.000 description 5
- 239000002243 precursor Substances 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- -1 unsaturated hydroxy fatty acid Chemical class 0.000 description 5
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 4
- 235000008694 Humulus lupulus Nutrition 0.000 description 4
- 229910019142 PO4 Inorganic materials 0.000 description 4
- 239000001110 calcium chloride Substances 0.000 description 4
- 229910001628 calcium chloride Inorganic materials 0.000 description 4
- 150000002632 lipids Chemical class 0.000 description 4
- 239000010452 phosphate Substances 0.000 description 4
- NOEGNKMFWQHSLB-UHFFFAOYSA-N 5-hydroxymethylfurfural Chemical compound OCC1=CC=C(C=O)O1 NOEGNKMFWQHSLB-UHFFFAOYSA-N 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 3
- 108090000790 Enzymes Proteins 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 244000287680 Garcinia dulcis Species 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 3
- 150000001413 amino acids Chemical class 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- KPQYDVAFRDWIBW-UHFFFAOYSA-N 5-(dimethylamino)naphthalene-1-sulfonohydrazide Chemical compound C1=CC=C2C(N(C)C)=CC=CC2=C1S(=O)(=O)NN KPQYDVAFRDWIBW-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 2
- 239000008351 acetate buffer Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000001506 calcium phosphate Substances 0.000 description 2
- 229910000389 calcium phosphate Inorganic materials 0.000 description 2
- 235000011010 calcium phosphates Nutrition 0.000 description 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000020477 pH reduction Effects 0.000 description 2
- 239000000123 paper Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000007669 thermal treatment Methods 0.000 description 2
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 2
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 description 1
- 241000821271 Aegilops tauschii x Triticum turgidum Species 0.000 description 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 229920002334 Spandex Polymers 0.000 description 1
- JNVCSEDACVAATK-UHFFFAOYSA-L [Ca+2].[S-]SSS[S-] Chemical compound [Ca+2].[S-]SSS[S-] JNVCSEDACVAATK-UHFFFAOYSA-L 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000006701 autoxidation reaction Methods 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 239000000872 buffer Substances 0.000 description 1
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 description 1
- 229910000020 calcium bicarbonate Inorganic materials 0.000 description 1
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Substances [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 1
- 235000010216 calcium carbonate Nutrition 0.000 description 1
- 235000011132 calcium sulphate Nutrition 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 229950001002 cianidanol Drugs 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- RJGBSYZFOCAGQY-UHFFFAOYSA-N hydroxymethylfurfural Natural products COC1=CC=C(C=O)O1 RJGBSYZFOCAGQY-UHFFFAOYSA-N 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000002414 normal-phase solid-phase extraction Methods 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 150000003141 primary amines Chemical class 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 229960004249 sodium acetate Drugs 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000004759 spandex Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229940051851 sulfurated lime Drugs 0.000 description 1
- 229940095064 tartrate Drugs 0.000 description 1
- 125000004149 thio group Chemical group *S* 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C7/00—Preparation of wort
- C12C7/04—Preparation or treatment of the mash
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C12/00—Processes specially adapted for making special kinds of beer
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C7/00—Preparation of wort
- C12C7/14—Lautering, i.e. clarifying wort
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C7/00—Preparation of wort
- C12C7/14—Lautering, i.e. clarifying wort
- C12C7/16—Lautering, i.e. clarifying wort by straining
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C7/00—Preparation of wort
- C12C7/28—After-treatment, e.g. sterilisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Food Science & Technology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Microbiology (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
- Non-Alcoholic Beverages (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Description
喷洒热水温度(过滤中的过滤层温度) | 糖度(°p) | pH | NP全过滤麦汁NPppb | NP全过滤麦汁NPppb按11°p换算 |
100℃(80℃) | 10.63 | 5.85 | 9.4 | 9.7 |
78℃(70℃) | 10.09 | 5.86 | 7.8 | 8.5 |
CaCl2(g/l) | 乳酸(g/l) | pH | |
对照 | 0 | 0 | |
试验1 | 0.40 | 0.24 | 3.16 |
试验2 | 1.00 | 0.60 | 2.93 |
糖度(°p) | pH | NP全过滤麦汁NPppb | NP全过滤麦汁NPppb按11°p换算 | |
对照 | 10.09 | 5.86 | 8.1 | 8.8 |
试验1 | 10.13 | 5.67 | 6.7 | 7.3 |
试验2 | 10.16 | 5.36 | 6.2 | 6.7 |
糖度(°p) | pH | NP全过滤麦汁NPppb | NP全过滤麦汁NPppb按11°p换算 | |
使用2成的取代添加用水进行酿造的场合 | 13.39 | 5.87 | 8.07 | 6.7 |
使用通常的用水进行酿造的场合 | 13.22 | 5.87 | 7.95 | 6.5 |
糖度(°p) | pH | 全部氮(mg/100ml) | NPppb | NPppb按11°p换算 | |
对照 | 7.85 | 6.04 | 76.4 | 6.17 | 8.65 |
1000ppm添加区 | 7.79 | 6.02 | 71.8 | 0.93 | 1.31 |
2000ppm添加区 | 7.74 | 6.03 | 66.9 | 0.47 | 0.67 |
Claims (13)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP140900/00 | 2000-05-12 | ||
JP140900/2000 | 2000-05-12 | ||
JP2000140900 | 2000-05-12 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1429266A true CN1429266A (zh) | 2003-07-09 |
CN100463959C CN100463959C (zh) | 2009-02-25 |
Family
ID=18648106
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB018094015A Expired - Fee Related CN100463959C (zh) | 2000-05-12 | 2001-05-09 | 发酵麦芽饮料用麦汁的制造方法 |
Country Status (9)
Country | Link |
---|---|
US (1) | US7247327B2 (zh) |
EP (1) | EP1281751B1 (zh) |
JP (1) | JP3831256B2 (zh) |
CN (1) | CN100463959C (zh) |
AT (1) | ATE357503T1 (zh) |
AU (1) | AU781273B2 (zh) |
DE (1) | DE60127397T2 (zh) |
DK (1) | DK1281751T3 (zh) |
WO (1) | WO2001085899A1 (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104034855A (zh) * | 2014-07-09 | 2014-09-10 | 中国食品发酵工业研究院 | 一种评价麦汁缓冲能力的方法 |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5265529B2 (ja) * | 2006-05-19 | 2013-08-14 | ハイネケン・サプライ・チェーン・ビー.ブイ. | マッシュ抽出物の製造方法およびそのような方法を行うための装置 |
US20120207909A1 (en) * | 2009-01-08 | 2012-08-16 | Kirin Beer Kabushiki Kaisha | Unfermented beer-flavored malt beverage having reduced unpleasant wort flavor and method for producing the same |
DE102011081648A1 (de) * | 2011-08-26 | 2013-02-28 | Krones Ag | Bierbrauverfahren |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3908021A (en) * | 1973-08-17 | 1975-09-23 | Schlitz Brewing Co J | Preparing a neutral tasting alcoholic base |
US5612072A (en) * | 1990-10-23 | 1997-03-18 | Cultor Ltd. | Process for the production of non-alcoholic or low alcohol malt beverage |
CA2052435C (en) * | 1991-10-01 | 2002-12-24 | Robert Leslie Barker | Improvements in beverage stability |
DE69625447D1 (de) * | 1995-10-27 | 2003-01-30 | Adriana Bravo | Verfahren zur Herstellung eines alkoholischen Malzgetränkes mit stabilisiertem Geschmack |
-
2001
- 2001-05-09 WO PCT/JP2001/003868 patent/WO2001085899A1/ja active IP Right Grant
- 2001-05-09 AT AT01930001T patent/ATE357503T1/de not_active IP Right Cessation
- 2001-05-09 DK DK01930001T patent/DK1281751T3/da active
- 2001-05-09 AU AU56671/01A patent/AU781273B2/en not_active Ceased
- 2001-05-09 DE DE60127397T patent/DE60127397T2/de not_active Expired - Lifetime
- 2001-05-09 US US10/275,695 patent/US7247327B2/en not_active Expired - Fee Related
- 2001-05-09 JP JP2001582489A patent/JP3831256B2/ja not_active Expired - Fee Related
- 2001-05-09 EP EP01930001A patent/EP1281751B1/en not_active Expired - Lifetime
- 2001-05-09 CN CNB018094015A patent/CN100463959C/zh not_active Expired - Fee Related
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104034855A (zh) * | 2014-07-09 | 2014-09-10 | 中国食品发酵工业研究院 | 一种评价麦汁缓冲能力的方法 |
Also Published As
Publication number | Publication date |
---|---|
EP1281751A1 (en) | 2003-02-05 |
WO2001085899A1 (fr) | 2001-11-15 |
DK1281751T3 (da) | 2007-07-09 |
DE60127397T2 (de) | 2007-11-29 |
US20030113404A1 (en) | 2003-06-19 |
EP1281751A4 (en) | 2004-04-21 |
US7247327B2 (en) | 2007-07-24 |
ATE357503T1 (de) | 2007-04-15 |
CN100463959C (zh) | 2009-02-25 |
EP1281751B1 (en) | 2007-03-21 |
AU781273B2 (en) | 2005-05-12 |
JP3831256B2 (ja) | 2006-10-11 |
DE60127397D1 (de) | 2007-05-03 |
AU5667101A (en) | 2001-11-20 |
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Legal Events
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---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
ASS | Succession or assignment of patent right |
Owner name: KIRIN BEER K.K. Free format text: FORMER OWNER: QILIN CO., LTD. Effective date: 20080725 Owner name: QILIN CO., LTD. Free format text: FORMER OWNER: KIRIN BEER K.K. Effective date: 20080725 |
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C41 | Transfer of patent application or patent right or utility model | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20080725 Address after: Tokyo, Japan Applicant after: KIRIN BEER Kabushiki Kaisha Address before: Tokyo, Japan Applicant before: KIRIN HOLDINGS Kabushiki Kaisha Effective date of registration: 20080725 Address after: Tokyo, Japan Applicant after: KIRIN HOLDINGS Kabushiki Kaisha Address before: Tokyo, Japan Applicant before: KIRIN BEER Kabushiki Kaisha |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C17 | Cessation of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20090225 Termination date: 20130509 |