JP3831256B2 - 発酵麦芽飲料用麦汁の製造方法 - Google Patents
発酵麦芽飲料用麦汁の製造方法 Download PDFInfo
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- JP3831256B2 JP3831256B2 JP2001582489A JP2001582489A JP3831256B2 JP 3831256 B2 JP3831256 B2 JP 3831256B2 JP 2001582489 A JP2001582489 A JP 2001582489A JP 2001582489 A JP2001582489 A JP 2001582489A JP 3831256 B2 JP3831256 B2 JP 3831256B2
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- fermented malt
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- 235000021577 malt beverage Nutrition 0.000 title claims abstract description 47
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 44
- BSAIUMLZVGUGKX-BQYQJAHWSA-N (E)-non-2-enal Chemical compound CCCCCC\C=C\C=O BSAIUMLZVGUGKX-BQYQJAHWSA-N 0.000 claims abstract description 56
- 239000000126 substance Substances 0.000 claims abstract description 53
- 238000000034 method Methods 0.000 claims abstract description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 39
- 230000008569 process Effects 0.000 claims abstract description 27
- 159000000007 calcium salts Chemical class 0.000 claims abstract description 12
- 150000007524 organic acids Chemical class 0.000 claims abstract description 10
- 235000005985 organic acids Nutrition 0.000 claims abstract description 6
- 238000005360 mashing Methods 0.000 claims abstract 2
- 238000001914 filtration Methods 0.000 claims description 36
- 230000006866 deterioration Effects 0.000 claims description 32
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 claims description 29
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 22
- 238000010828 elution Methods 0.000 claims description 11
- 230000009467 reduction Effects 0.000 claims description 11
- 238000000855 fermentation Methods 0.000 claims description 8
- 230000004151 fermentation Effects 0.000 claims description 8
- 230000001629 suppression Effects 0.000 claims description 6
- 231100000676 disease causative agent Toxicity 0.000 claims description 4
- 238000011946 reduction process Methods 0.000 claims description 4
- 235000013361 beverage Nutrition 0.000 claims description 3
- 230000005012 migration Effects 0.000 claims description 2
- 238000013508 migration Methods 0.000 claims description 2
- BSAIUMLZVGUGKX-UHFFFAOYSA-N non-2-enal Chemical compound CCCCCCC=CC=O BSAIUMLZVGUGKX-UHFFFAOYSA-N 0.000 claims 2
- 235000013405 beer Nutrition 0.000 abstract description 33
- 239000000796 flavoring agent Substances 0.000 abstract description 7
- 235000019634 flavors Nutrition 0.000 abstract description 7
- 238000000926 separation method Methods 0.000 abstract description 2
- 239000004458 spent grain Substances 0.000 abstract 1
- 235000019645 odor Nutrition 0.000 description 36
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 12
- 238000009835 boiling Methods 0.000 description 11
- 230000007423 decrease Effects 0.000 description 8
- 238000007254 oxidation reaction Methods 0.000 description 8
- 238000003672 processing method Methods 0.000 description 8
- 230000003647 oxidation Effects 0.000 description 7
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 6
- 239000000706 filtrate Substances 0.000 description 5
- 239000002243 precursor Substances 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 235000014347 soups Nutrition 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- NOEGNKMFWQHSLB-UHFFFAOYSA-N 5-hydroxymethylfurfural Chemical compound OCC1=CC=C(C=O)O1 NOEGNKMFWQHSLB-UHFFFAOYSA-N 0.000 description 3
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 3
- 235000008694 Humulus lupulus Nutrition 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 3
- 235000013334 alcoholic beverage Nutrition 0.000 description 3
- 150000001298 alcohols Chemical class 0.000 description 3
- 150000001413 amino acids Chemical class 0.000 description 3
- 239000000872 buffer Substances 0.000 description 3
- 239000001110 calcium chloride Substances 0.000 description 3
- 229910001628 calcium chloride Inorganic materials 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 235000014113 dietary fatty acids Nutrition 0.000 description 3
- 230000002255 enzymatic effect Effects 0.000 description 3
- 239000000194 fatty acid Substances 0.000 description 3
- 229930195729 fatty acid Natural products 0.000 description 3
- 239000004310 lactic acid Substances 0.000 description 3
- 235000014655 lactic acid Nutrition 0.000 description 3
- 150000002632 lipids Chemical class 0.000 description 3
- 238000012546 transfer Methods 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 240000005979 Hordeum vulgare Species 0.000 description 2
- 235000007340 Hordeum vulgare Nutrition 0.000 description 2
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 2
- 241000209140 Triticum Species 0.000 description 2
- 235000021307 Triticum Nutrition 0.000 description 2
- 239000001506 calcium phosphate Substances 0.000 description 2
- 229910000389 calcium phosphate Inorganic materials 0.000 description 2
- 235000011010 calcium phosphates Nutrition 0.000 description 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 235000019985 fermented beverage Nutrition 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000010525 oxidative degradation reaction Methods 0.000 description 2
- 230000037361 pathway Effects 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 235000019640 taste Nutrition 0.000 description 2
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 2
- -1 unsaturated hydroxy fatty acids Chemical class 0.000 description 2
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 description 1
- KPQYDVAFRDWIBW-UHFFFAOYSA-N 5-(dimethylamino)naphthalene-1-sulfonohydrazide Chemical compound C1=CC=C2C(N(C)C)=CC=CC2=C1S(=O)(=O)NN KPQYDVAFRDWIBW-UHFFFAOYSA-N 0.000 description 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 239000002262 Schiff base Substances 0.000 description 1
- 150000004753 Schiff bases Chemical class 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 235000011054 acetic acid Nutrition 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 description 1
- 229910000020 calcium bicarbonate Inorganic materials 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 description 1
- 235000005487 catechin Nutrition 0.000 description 1
- 229950001002 cianidanol Drugs 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000005429 filling process Methods 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 230000002431 foraging effect Effects 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- RJGBSYZFOCAGQY-UHFFFAOYSA-N hydroxymethylfurfural Natural products COC1=CC=C(C=O)O1 RJGBSYZFOCAGQY-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004890 malting Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 229910052751 metal Chemical class 0.000 description 1
- 239000002184 metal Chemical class 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 230000020477 pH reduction Effects 0.000 description 1
- 239000000123 paper Substances 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 150000003141 primary amines Chemical class 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 235000015040 sparkling wine Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 125000003396 thiol group Chemical group [H]S* 0.000 description 1
- 230000036962 time dependent Effects 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C7/00—Preparation of wort
- C12C7/04—Preparation or treatment of the mash
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C12/00—Processes specially adapted for making special kinds of beer
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C7/00—Preparation of wort
- C12C7/14—Lautering, i.e. clarifying wort
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C7/00—Preparation of wort
- C12C7/14—Lautering, i.e. clarifying wort
- C12C7/16—Lautering, i.e. clarifying wort by straining
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C7/00—Preparation of wort
- C12C7/28—After-treatment, e.g. sterilisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Food Science & Technology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Microbiology (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
- Non-Alcoholic Beverages (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Description
麦芽100gに湯300ml(麦芽:湯=1:3)を加えて、50℃で30分間、65℃で60分間、続いて78℃で10分間の温度プログラムで糖化した麦汁もろみを濾紙(東洋濾紙「#2」)を敷いたロートで濾過し、濾過後の濾過層に420mlの撒き湯を70mlずつ6回に分けて行った。各濾過液(二番搾り)の糖度、NPを測定した。糖度は比重を測定し、換算表から糖度(゜p)を算出した。結果を図1に示す。また、同様にして、KLレベルのパイロットプラント糖化麦汁もろみをロイター槽で濾過し、濾過液の糖度、NPを経時的に測定した。結果を図2に示す。図1及び図2から、二番搾りにおいては、NPの低下は糖度の低下と比較して小さく、特に図2から、麦汁中の糖分は濾過液量の増加に概ね比例して漸次低下するが、NPは糖分の低下に相関することなく、高い値で推移することや、一番搾り麦汁と二番搾り麦汁におけるNP含量に差がないことから、NPが濾過層(仕込粕)から溶出していることがわかった。
一番搾り麦汁と二番搾り麦汁を組み合わせ、糖度が共に11°pで、6.7ppbと7.4ppbのNP含量が異なる濾過麦汁を調製し、これら麦汁にそれぞれホップを添加した後煮沸を行い、冷却後に酵母を添加して発酵させビールを調製した。壜詰後、37℃で4日間保存し、生成するトランス−2−ノネナール量を測定すると共に、官能検査を実施した。ビール中のトランス−2−ノネナール量は、NP含量6.7ppbの麦汁を用いた場合0.16ppb、NP含量7.4ppbの麦汁を用いた場合0.19ppbであった。また官能検査においてもNP含量7.4ppbの麦汁を用いた場合の方が明らかに劣化臭(カードボード臭)が強かった。この結果から、全濾過麦汁中のNPを約1ppb低下させればビール中のトランス−2−ノネナール量を低下させ、劣化臭の生成を抑制できることがわかった。
麦芽100gに湯300ml(麦芽:湯=1:3)を加えて、50℃で30分間、65℃で60分間、続いて78℃で10分間の糖化後、保温ができるロートからなる濾過筒を用いて、78℃(試験区)、100℃(対照区)の撒き湯を、それぞれ100mlずつ5回に分けて行い、全濾過麦汁中の糖度、pH、NP含量を測定した。また、二番搾りの途中で濾過層の温度を測定したところ、それぞれ70℃(試験区)、80℃(対照区)であった。結果を表1に示す。表1から、濾過麦汁のNPは撒き湯の温度を低下させ、濾過層内の温度を低下させることにより低減できることがわかる。
麦芽100gに湯300ml(麦芽:湯=1:3)を加えて、50℃で30分間、65℃で60分間、続いて78℃で10分間の糖化後濾過し、その後濾過層に表2の条件で、塩化カルシウムと乳酸により用水処理した撒き湯を100mlずつ5回に分けて行い、濾過麦汁を得た。なお、塩化カルシウムと乳酸を添加しない湯を用いた場合を対照とした。結果を表3に示す。表3から、カルシウム塩と有機酸により用水処理した撒き湯を用いて濾過することにより、麦汁中のNPが低減できることがわかる。
麦芽100gに湯300ml(麦芽:湯=1:3)を加えて、50℃で30分間、65℃で60分間、続いて78℃で10分間の糖化後濾過し、一番搾りを行った。その後300mlの撒き湯を行って、二番搾り麦汁のみを採取した。二番搾り麦汁200mlに活性炭を、1000ppm、2000ppmとなるように添加して、2分間撹拌後、濾過し、濾過麦汁のNPを測定した。結果を表4に示す。表5から、活性炭処理することにより、糖度は殆ど減少しないが、NPは大きく低減することがわかる。
Claims (8)
- 発酵麦芽飲料の製造における仕込麦汁の濾過工程において、二番搾り麦汁における劣化臭原因物質の低減化処理を、トランス−2−ノネナール ポテンシャルを指標として行い、全濾過麦汁中のトランス−2−ノネナール ポテンシャルが、二番搾り麦汁における劣化臭原因物質の低減化処理を行なわないものに対して、糖度11゜p換算で、少なくとも1ppb低減されるように、二番搾り麦汁における劣化臭原因物質トランス−2−ノネナール ポテンシャルの含有量の低減化を行うことを特徴とする劣化臭原因物質トランス−2−ノネナール ポテンシャルの含有量が低減した発酵麦芽飲料用麦汁の製造方法。
- 劣化臭原因物質の低減化処理が、二番搾り麦汁への劣化臭原因物質の移行制限処理である二番搾り麦汁濾過工程におけるもろみ濾過層からの劣化臭原因物質の溶出の抑制処理であることを特徴とする請求項1記載の発酵麦芽飲料用麦汁の製造方法。
- 劣化臭原因物質の溶出の抑制処理が、カルシウム塩類及び有機酸を含む二番搾り用湯水を用いての処理であることを特徴とする請求項2記載の発酵麦芽飲料用麦汁の製造方法。
- 劣化臭原因物質の溶出の抑制処理が、濾過層内の温度を70℃以下に低下させることができる二番搾り用湯水を用いての処理であることを特徴とする請求項2記載の発酵麦芽飲料用麦汁の製造方法。
- 二番搾り麦汁への劣化臭原因物質の移行の制限処理が、二番搾り麦汁の糖度が3゜pを下回らない範囲で二番搾りが終了するように、二番搾り用湯水供給の制御処理であることを特徴とする請求項2記載の発酵麦芽飲料用麦汁の製造方法。
- 劣化臭原因物質の低減化処理が、二番搾り麦汁から劣化臭原因物質の除去・低減処理であることを特徴とする請求項1記載の発酵麦芽飲料用麦汁の製造方法。
- 二番搾り麦汁からの劣化臭原因物質の除去・低減処理が、二番搾り麦汁の一部又は全部を活性炭と接触させ、劣化臭原因物質の一部を除去・低減する処理であることを特徴とする請求項6記載の発酵麦芽飲料用麦汁の製造方法。
- 請求項1〜7のいずれか記載の発酵麦芽飲料用麦汁の製造方法により製造された麦汁から発酵工程を経て得られる劣化臭の生成が抑制された発酵麦芽飲料。
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2000140900 | 2000-05-12 | ||
PCT/JP2001/003868 WO2001085899A1 (fr) | 2000-05-12 | 2001-05-09 | Procede de fabrication de mout pour boissons fermentees a base de malt |
Publications (1)
Publication Number | Publication Date |
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JP3831256B2 true JP3831256B2 (ja) | 2006-10-11 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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JP2001582489A Expired - Fee Related JP3831256B2 (ja) | 2000-05-12 | 2001-05-09 | 発酵麦芽飲料用麦汁の製造方法 |
Country Status (9)
Country | Link |
---|---|
US (1) | US7247327B2 (ja) |
EP (1) | EP1281751B1 (ja) |
JP (1) | JP3831256B2 (ja) |
CN (1) | CN100463959C (ja) |
AT (1) | ATE357503T1 (ja) |
AU (1) | AU781273B2 (ja) |
DE (1) | DE60127397T2 (ja) |
DK (1) | DK1281751T3 (ja) |
WO (1) | WO2001085899A1 (ja) |
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PL2027245T3 (pl) * | 2006-05-19 | 2018-12-31 | Heineken Supply Chain B.V. | Sposób wytwarzania ekstraktu zacieru i urządzenie do przeprowadzania sposobu |
US20120207909A1 (en) * | 2009-01-08 | 2012-08-16 | Kirin Beer Kabushiki Kaisha | Unfermented beer-flavored malt beverage having reduced unpleasant wort flavor and method for producing the same |
DE102011081648A1 (de) * | 2011-08-26 | 2013-02-28 | Krones Ag | Bierbrauverfahren |
CN104034855A (zh) * | 2014-07-09 | 2014-09-10 | 中国食品发酵工业研究院 | 一种评价麦汁缓冲能力的方法 |
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US3908021A (en) * | 1973-08-17 | 1975-09-23 | Schlitz Brewing Co J | Preparing a neutral tasting alcoholic base |
US5612072A (en) * | 1990-10-23 | 1997-03-18 | Cultor Ltd. | Process for the production of non-alcoholic or low alcohol malt beverage |
CA2052435C (en) | 1991-10-01 | 2002-12-24 | Robert Leslie Barker | Improvements in beverage stability |
CA2188971A1 (en) * | 1995-10-27 | 1997-04-28 | Beatriz Sanchez | Malt beverage having stabilized flavor and methods of production thereof |
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2001
- 2001-05-09 AU AU56671/01A patent/AU781273B2/en not_active Ceased
- 2001-05-09 US US10/275,695 patent/US7247327B2/en not_active Expired - Fee Related
- 2001-05-09 JP JP2001582489A patent/JP3831256B2/ja not_active Expired - Fee Related
- 2001-05-09 DE DE60127397T patent/DE60127397T2/de not_active Expired - Lifetime
- 2001-05-09 AT AT01930001T patent/ATE357503T1/de not_active IP Right Cessation
- 2001-05-09 DK DK01930001T patent/DK1281751T3/da active
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US20030113404A1 (en) | 2003-06-19 |
EP1281751B1 (en) | 2007-03-21 |
AU781273B2 (en) | 2005-05-12 |
AU5667101A (en) | 2001-11-20 |
DE60127397D1 (de) | 2007-05-03 |
ATE357503T1 (de) | 2007-04-15 |
WO2001085899A1 (fr) | 2001-11-15 |
DK1281751T3 (da) | 2007-07-09 |
US7247327B2 (en) | 2007-07-24 |
DE60127397T2 (de) | 2007-11-29 |
EP1281751A1 (en) | 2003-02-05 |
CN100463959C (zh) | 2009-02-25 |
CN1429266A (zh) | 2003-07-09 |
EP1281751A4 (en) | 2004-04-21 |
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