CN1263678C - 从盐液获得氯化锂的方法和实施此方法的设备 - Google Patents
从盐液获得氯化锂的方法和实施此方法的设备 Download PDFInfo
- Publication number
- CN1263678C CN1263678C CNB01823738XA CN01823738A CN1263678C CN 1263678 C CN1263678 C CN 1263678C CN B01823738X A CNB01823738X A CN B01823738XA CN 01823738 A CN01823738 A CN 01823738A CN 1263678 C CN1263678 C CN 1263678C
- Authority
- CN
- China
- Prior art keywords
- solution
- lithium chloride
- container
- pipe fitting
- eluant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
- B01J39/04—Processes using organic exchangers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/42—Electrodialysis; Electro-osmosis ; Electro-ultrafiltration; Membrane capacitive deionization
- B01D61/44—Ion-selective electrodialysis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
- B01J20/046—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing halogens, e.g. halides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/34—Regenerating or reactivating
- B01J20/3433—Regenerating or reactivating of sorbents or filter aids other than those covered by B01J20/3408 - B01J20/3425
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/34—Regenerating or reactivating
- B01J20/345—Regenerating or reactivating using a particular desorbing compound or mixture
- B01J20/3475—Regenerating or reactivating using a particular desorbing compound or mixture in the liquid phase
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J47/00—Ion-exchange processes in general; Apparatus therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
- B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
- B01J49/53—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for cationic exchangers
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D15/00—Lithium compounds
- C01D15/04—Halides
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Analytical Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Water Supply & Treatment (AREA)
- Materials Engineering (AREA)
- Urology & Nephrology (AREA)
- Health & Medical Sciences (AREA)
- Water Treatment By Electricity Or Magnetism (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
Description
Claims (11)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/DE2001/004061 WO2003037794A1 (de) | 2001-10-25 | 2001-10-25 | Verfahren zur gewinnung von lithiumchlorid aus salzlaugen und anlage zur durchführung des verfahrens |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1558871A CN1558871A (zh) | 2004-12-29 |
CN1263678C true CN1263678C (zh) | 2006-07-12 |
Family
ID=5648304
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB01823738XA Expired - Lifetime CN1263678C (zh) | 2001-10-25 | 2001-10-25 | 从盐液获得氯化锂的方法和实施此方法的设备 |
Country Status (3)
Country | Link |
---|---|
CN (1) | CN1263678C (zh) |
DE (1) | DE10197021D2 (zh) |
WO (1) | WO2003037794A1 (zh) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2763955C1 (ru) * | 2021-08-15 | 2022-01-11 | Акционерное общество "Аксион - Редкие и Драгоценные Металлы" | Способ сорбционного извлечения лития из литийсодержащих рассолов |
WO2023067101A3 (en) * | 2021-10-20 | 2023-06-15 | IIDC International Investment Development Corporation | Method and electrochemical filter cell for extracting lithium |
Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1844805B (zh) * | 2006-03-12 | 2012-04-25 | 王俊 | 制冷机用溴化锂溶液中钙镁离子消除的方法与装置 |
US20090246603A1 (en) * | 2008-03-27 | 2009-10-01 | Honeywell, Inc. | Process for reclaiming a contaminated electrolyte from an electrolytic cell used in the production of gaseous fluorine |
US10190030B2 (en) | 2009-04-24 | 2019-01-29 | Alger Alternative Energy, Llc | Treated geothermal brine compositions with reduced concentrations of silica, iron and lithium |
US8741256B1 (en) | 2009-04-24 | 2014-06-03 | Simbol Inc. | Preparation of lithium carbonate from lithium chloride containing brines |
US9051827B1 (en) | 2009-09-02 | 2015-06-09 | Simbol Mining Corporation | Selective removal of silica from silica containing brines |
US8637428B1 (en) | 2009-12-18 | 2014-01-28 | Simbol Inc. | Lithium extraction composition and method of preparation thereof |
US9034294B1 (en) | 2009-04-24 | 2015-05-19 | Simbol, Inc. | Preparation of lithium carbonate from lithium chloride containing brines |
US8753594B1 (en) | 2009-11-13 | 2014-06-17 | Simbol, Inc. | Sorbent for lithium extraction |
US10935006B2 (en) | 2009-06-24 | 2021-03-02 | Terralithium Llc | Process for producing geothermal power, selective removal of silica and iron from brines, and improved injectivity of treated brines |
CA2789771C (en) | 2010-02-17 | 2022-06-14 | Simbol Mining Corp. | Highly pure lithium carbonate prepared using reverse osmosis |
DE102010019554B4 (de) | 2010-05-05 | 2012-11-29 | Technische Universität Bergakademie Freiberg | Verfahren zur Abreicherung von Magnesium und Anreicherung von Lithium in chloridisch geprägten Salzlösungen |
RU2516538C2 (ru) * | 2012-02-17 | 2014-05-20 | Закрытое акционерное общество (ЗАО) "Экостра-Наутех" | Способ получения литиевого концентрата из литиеносных природных рассолов и его переработки |
DE102015000872A1 (de) | 2015-01-23 | 2016-07-28 | K-Utec Ag Salt Technologies | Methode zur Gewinnung von Lithiumchlorid |
CN106048218A (zh) * | 2016-07-14 | 2016-10-26 | 四川思达能环保科技有限公司 | 一种氯化锂混合溶液的净化除杂方法 |
CN106745101B (zh) * | 2017-01-06 | 2018-09-25 | 深圳市聚能永拓科技开发有限公司 | 一种采用吸附和煅烧方法从卤水中制备碳酸锂的方法 |
CN106629788B (zh) * | 2017-02-13 | 2019-04-30 | 青海盐湖工业股份有限公司 | 一种氯化锂的生产工艺 |
RU2659968C1 (ru) * | 2017-04-14 | 2018-07-04 | Общество с ограниченной ответственностью (ООО) "Экостар-Наутех" | Способ получения литиевого концентрата из литиеносных природных рассолов и его переработки в хлорид лития или карбонат лития |
US11655150B2 (en) * | 2017-12-22 | 2023-05-23 | Posco Co., Ltd | Preparation method for lithium phosphate, preparation method for lithium hydroxide, and preparation method for lithium carbonate |
RU2688593C1 (ru) * | 2018-08-16 | 2019-05-21 | Публичное акционерное общество "Татнефть" имени В.Д. Шашина | Способ сорбционного извлечения лития из литийсодержащих хлоридных рассолов |
CN109019641B (zh) * | 2018-10-12 | 2020-12-11 | 中国科学院青海盐湖研究所 | 从硫酸钠亚型盐湖卤水中分离镁锂并富集锂的方法 |
CN110395749A (zh) * | 2019-08-09 | 2019-11-01 | 山东科技大学 | 一种利用四隔室置换反应电渗析制备氯化锂的方法 |
CN112174172A (zh) * | 2020-11-03 | 2021-01-05 | 严永生 | 一种电渗析方法提纯浓缩氟化铍的制备方法 |
RU2751948C1 (ru) * | 2021-02-09 | 2021-07-21 | Акционерное общество «Аксион - Редкие и Драгоценные Металлы» | Способ переработки гидроминерального литийсодержащего сырья |
CN113368537B (zh) * | 2021-06-28 | 2022-05-24 | 青海盐湖工业股份有限公司 | 吸附法利用老卤制备高锂母液的方法和装置 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SU1378890A1 (ru) * | 1986-03-03 | 1988-03-07 | Предприятие П/Я А-7638 | Электродиализатор фильтр-прессного типа |
DE3712142A1 (de) * | 1986-04-11 | 1987-10-15 | Lithium Corp | Verfahren zum reinigen von solen |
WO1994019280A1 (en) * | 1993-02-16 | 1994-09-01 | Nauchno-Proizvodstvennoe Aktsionernoe Obschestvo 'ekostar' | Process for obtaining lithium chloride from solutions and a device for carrying out the same |
JPH07155563A (ja) * | 1993-12-06 | 1995-06-20 | Hitachi Ltd | 電気透析によるNaCl回収装置 |
DE19541558A1 (de) * | 1995-11-08 | 1997-05-15 | Bayer Ag | Verfahren zur Reinigung von Lithiumchlorid-Lösungen |
-
2001
- 2001-10-25 DE DE10197021T patent/DE10197021D2/de not_active Expired - Fee Related
- 2001-10-25 CN CNB01823738XA patent/CN1263678C/zh not_active Expired - Lifetime
- 2001-10-25 WO PCT/DE2001/004061 patent/WO2003037794A1/de active Application Filing
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2763955C1 (ru) * | 2021-08-15 | 2022-01-11 | Акционерное общество "Аксион - Редкие и Драгоценные Металлы" | Способ сорбционного извлечения лития из литийсодержащих рассолов |
WO2023067101A3 (en) * | 2021-10-20 | 2023-06-15 | IIDC International Investment Development Corporation | Method and electrochemical filter cell for extracting lithium |
Also Published As
Publication number | Publication date |
---|---|
WO2003037794A1 (de) | 2003-05-08 |
CN1558871A (zh) | 2004-12-29 |
DE10197021D2 (de) | 2004-10-14 |
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Legal Events
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: XIE LIANGHAN Free format text: FORMER OWNER: HUAOU TECHNOLOGY CONSULATION AND LAYOUT DEVELOPMENT CO., LTD. Effective date: 20080418 |
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C41 | Transfer of patent application or patent right or utility model | ||
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Effective date of registration: 20080418 Address after: Berlin Patentee after: Xie Lianghan Address before: Berlin Patentee before: Eurosina Technology Consulting |
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ASS | Succession or assignment of patent right |
Owner name: QINGHAI TIANJI RARE ELEMENTS SCIENCE AND TECHNOLOG Free format text: FORMER OWNER: XIE LIANGHAN Effective date: 20091120 |
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Effective date of registration: 20091120 Address after: Hongkong Yuchang des Voeux Road No. 48-52 building 10 floor, room 1005 Patentee after: Qinghai horizon rare element science and Technology Development Co Ltd Address before: Berlin Patentee before: Xie Lianghan |
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ASS | Succession or assignment of patent right |
Owner name: QINGHAI FOZHAO LITHIUM ENERGY DEVELOPMENT CO., LTD Free format text: FORMER OWNER: QINGHAI TIANJI RARE ELEMENTS SCIENCE AND TECHNOLOGY DEVELOPMENT CO., LTD. Effective date: 20100122 |
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Effective date of registration: 20100122 Address after: Qinghai province Xining economic and Technological Development Zone Jinqiao Road 36, science and technology incubation building, building 4, 6407 Patentee after: Qinghai according to Li Li Energy Development Co., Ltd. Address before: Hongkong Yuchang des Voeux Road No. 48-52 building 10 floor, room 1005 Patentee before: Qinghai horizon rare element science and Technology Development Co Ltd |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Method for recovering lithium chloride from brine and installation for carrying out said method Effective date of registration: 20101217 Granted publication date: 20060712 Pledgee: Bank of Qinghai, Limited by Share Ltd, Golmud branch Pledgor: Qinghai Weili new energy material Co., Ltd.|Qinghai Buddha shine lithium energy development Co., Ltd. Registration number: 2010990001010 |
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ASS | Succession or assignment of patent right |
Owner name: QINGHAI SALT LAKE LANKE LITHIUM INDUSTRY CO., LTD. Free format text: FORMER OWNER: QINGHAI FOZHAO LITHIUM ENERGY DEVELOPMENT CO., LTD. Effective date: 20110426 |
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Free format text: CORRECT: ADDRESS; FROM: 810007 6407, 4/F, TECHNOLOGY INCUBATION BUILDING, NO. 36, JINQIAO ROAD, XINING ECONOMIC AND TECHNOLOGICAL DEVELOPMENT ZONE, QINGHAI PROVINCE TO: 816000 NO. 1, HUANGHE ROAD, GOLMUD CITY, QINGHAI PROVINCE |
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Effective date of registration: 20110426 Address after: 816000 No. 1, the Yellow River Road, Golmud, Qinghai Patentee after: Saline Lake, Qinghai, blue, lithium, Limited by Share Ltd Address before: 4 Building 810007, science and technology incubation building, Jinqiao Road 36, Xining economic and Technological Development Zone, Qinghai, 6407 Patentee before: Qinghai according to Li Li Energy Development Co., Ltd. |
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Granted publication date: 20060712 Termination date: 20111025 |
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Former decision: cessation of patent right due to non-payment of the annual fee Former decision publication date: 20121226 |
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Date of cancellation: 20131120 Granted publication date: 20060712 Pledgee: Bank of Qinghai, Limited by Share Ltd, Golmud branch Pledgor: Qinghai Weili new energy material Co., Ltd.|Qinghai Buddha shine lithium energy development Co., Ltd. Registration number: 2010990001010 |
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ASS | Succession or assignment of patent right |
Owner name: QINGHAI SALTLAKE FOZHAO LAKE LITHIUM CO., LTD. Free format text: FORMER OWNER: QINGHAI FOZHAO LITHIUM ENERGY DEVELOPMENT CO., LTD. Effective date: 20131210 |
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Free format text: CORRECT: ADDRESS; FROM: 810007 XINING, QINGHAI PROVINCE TO: 816000 HAIXI MONGOL AND TIBETAN AUTONOMOUS PREFECTURE, QINGHAI PROVINCE |
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TR01 | Transfer of patent right |
Effective date of registration: 20131210 Address after: 816000 Haixi Mongol and Tibetan Autonomous Prefecture, Golmud, Qinghai Patentee after: QINGHAI SALT LAKE FOZHAO LANKE LITHIUM INDUSTRY CO., LTD. Address before: 4 Building 810007, science and technology incubation building, Jinqiao Road 36, Xining economic and Technological Development Zone, Qinghai, 6407 Patentee before: Qinghai according to Li Li Energy Development Co., Ltd. |
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CX01 | Expiry of patent term |
Granted publication date: 20060712 |
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