CN1191351C - 一种洗涤剂组合物的生产方法 - Google Patents
一种洗涤剂组合物的生产方法 Download PDFInfo
- Publication number
- CN1191351C CN1191351C CNB971919607A CN97191960A CN1191351C CN 1191351 C CN1191351 C CN 1191351C CN B971919607 A CNB971919607 A CN B971919607A CN 97191960 A CN97191960 A CN 97191960A CN 1191351 C CN1191351 C CN 1191351C
- Authority
- CN
- China
- Prior art keywords
- particulate material
- bulk density
- grams per
- detergent
- detergent composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 55
- 238000000034 method Methods 0.000 title claims abstract description 41
- 239000003599 detergent Substances 0.000 title claims abstract description 36
- 238000004519 manufacturing process Methods 0.000 title abstract description 13
- 238000002156 mixing Methods 0.000 claims abstract description 29
- 239000011236 particulate material Substances 0.000 claims abstract description 19
- 239000007788 liquid Substances 0.000 claims abstract description 13
- 238000001035 drying Methods 0.000 claims description 13
- 239000002245 particle Substances 0.000 claims description 12
- 238000005507 spraying Methods 0.000 claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 11
- 238000005406 washing Methods 0.000 claims description 11
- 239000000463 material Substances 0.000 claims description 10
- 229910021536 Zeolite Inorganic materials 0.000 claims description 6
- 239000000853 adhesive Substances 0.000 claims description 6
- 230000001070 adhesive effect Effects 0.000 claims description 6
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 6
- 239000002243 precursor Substances 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 239000010457 zeolite Substances 0.000 claims description 6
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 5
- 150000003016 phosphoric acids Chemical class 0.000 claims description 3
- 239000000344 soap Substances 0.000 claims description 2
- 239000011230 binding agent Substances 0.000 abstract 1
- 239000012530 fluid Substances 0.000 abstract 1
- 239000008187 granular material Substances 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- 239000000843 powder Substances 0.000 description 24
- 235000019832 sodium triphosphate Nutrition 0.000 description 16
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 9
- 229910052708 sodium Inorganic materials 0.000 description 8
- 239000011734 sodium Substances 0.000 description 8
- 101710194948 Protein phosphatase PhpP Proteins 0.000 description 7
- 238000005520 cutting process Methods 0.000 description 6
- 239000002648 laminated material Substances 0.000 description 5
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 4
- 238000010008 shearing Methods 0.000 description 4
- 238000001694 spray drying Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 239000000758 substrate Substances 0.000 description 4
- -1 Sodium alkyl sulfate Chemical class 0.000 description 3
- 239000011149 active material Substances 0.000 description 3
- 125000000217 alkyl group Chemical group 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000012747 synergistic agent Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 235000010724 Wisteria floribunda Nutrition 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000003472 neutralizing effect Effects 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 239000011591 potassium Substances 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- MZSDGDXXBZSFTG-UHFFFAOYSA-M sodium;benzenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C1=CC=CC=C1 MZSDGDXXBZSFTG-UHFFFAOYSA-M 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical group C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- 241000237502 Ostreidae Species 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Natural products OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 1
- GBFLZEXEOZUWRN-VKHMYHEASA-N S-carboxymethyl-L-cysteine Chemical compound OC(=O)[C@@H](N)CSCC(O)=O GBFLZEXEOZUWRN-VKHMYHEASA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000009795 derivation Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- RBNPOMFGQQGHHO-UHFFFAOYSA-N glyceric acid Chemical compound OCC(O)C(O)=O RBNPOMFGQQGHHO-UHFFFAOYSA-N 0.000 description 1
- 238000010237 hybrid technique Methods 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 125000001165 hydrophobic group Chemical group 0.000 description 1
- 229910017053 inorganic salt Inorganic materials 0.000 description 1
- 239000002563 ionic surfactant Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- VSXGXPNADZQTGQ-UHFFFAOYSA-N oxirane;phenol Chemical compound C1CO1.OC1=CC=CC=C1 VSXGXPNADZQTGQ-UHFFFAOYSA-N 0.000 description 1
- 235000020636 oyster Nutrition 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 229960003742 phenol Drugs 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 150000003333 secondary alcohols Chemical class 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 235000017550 sodium carbonate Nutrition 0.000 description 1
- 239000001488 sodium phosphate Substances 0.000 description 1
- 229910000162 sodium phosphate Inorganic materials 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GBGB9601920.3A GB9601920D0 (en) | 1996-01-31 | 1996-01-31 | Process for the production of a detergent composition |
| GB9601920.3 | 1996-01-31 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1209835A CN1209835A (zh) | 1999-03-03 |
| CN1191351C true CN1191351C (zh) | 2005-03-02 |
Family
ID=10787857
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB971919607A Expired - Fee Related CN1191351C (zh) | 1996-01-31 | 1997-01-06 | 一种洗涤剂组合物的生产方法 |
Country Status (16)
| Country | Link |
|---|---|
| EP (1) | EP0882126B1 (hu) |
| CN (1) | CN1191351C (hu) |
| AR (1) | AR005576A1 (hu) |
| AU (1) | AU1440997A (hu) |
| BR (1) | BR9707474A (hu) |
| CA (1) | CA2242420C (hu) |
| DE (1) | DE69701731T2 (hu) |
| EA (1) | EA001314B1 (hu) |
| ES (1) | ES2145567T3 (hu) |
| GB (1) | GB9601920D0 (hu) |
| HU (1) | HUP9901180A3 (hu) |
| IN (1) | IN188387B (hu) |
| PL (1) | PL184656B1 (hu) |
| TR (1) | TR199801444T2 (hu) |
| WO (1) | WO1997028246A1 (hu) |
| ZA (1) | ZA97255B (hu) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9513327D0 (en) * | 1995-06-30 | 1995-09-06 | Uniliver Plc | Process for the production of a detergent composition |
| GB9526097D0 (en) * | 1995-12-20 | 1996-02-21 | Unilever Plc | Process |
| US6211138B1 (en) | 1996-10-04 | 2001-04-03 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6211137B1 (en) | 1996-10-04 | 2001-04-03 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6136777A (en) * | 1996-10-04 | 2000-10-24 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6143711A (en) * | 1996-10-04 | 2000-11-07 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6391844B1 (en) | 1996-10-04 | 2002-05-21 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6172034B1 (en) | 1996-10-04 | 2001-01-09 | The Procter & Gamble | Process for making a detergent composition by non-tower process |
| US6121229A (en) * | 1996-10-04 | 2000-09-19 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6150323A (en) * | 1996-10-04 | 2000-11-21 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| GB9712583D0 (en) | 1997-06-16 | 1997-08-20 | Unilever Plc | Production of detergent granulates |
| GB9712580D0 (en) * | 1997-06-16 | 1997-08-20 | Unilever Plc | Production of detergent granulates |
| GB9713748D0 (en) * | 1997-06-27 | 1997-09-03 | Unilever Plc | Production of detergent granulates |
| DE69904499T2 (de) * | 1998-10-26 | 2003-10-30 | Procter & Gamble | Verfahren zur herstellung eines granularen waschmittels mit verbessertem aussehen und erhöhter löslichkeit |
| US6596683B1 (en) | 1998-12-22 | 2003-07-22 | The Procter & Gamble Company | Process for preparing a granular detergent composition |
| JP2002533532A (ja) * | 1998-12-22 | 2002-10-08 | ザ、プロクター、エンド、ギャンブル、カンパニー | 凝集による低かさ密度洗剤組成物の製造方法 |
| US6858572B1 (en) | 1999-03-09 | 2005-02-22 | The Procter & Gamble Company | Process for producing coated detergent particles |
| GB9913546D0 (en) | 1999-06-10 | 1999-08-11 | Unilever Plc | Granular detergent component containing zeolite map and laundry detergent compositions containing it |
| GB9913544D0 (en) * | 1999-06-10 | 1999-08-11 | Unilever Plc | Process for preparing granular detergent compositions |
| US6894018B1 (en) | 1999-06-21 | 2005-05-17 | The Procter & Gamble Company | Process for making granular detergent in a fluidized bed granulator having recycling of improperly sized particles |
| BR112012000460A2 (pt) * | 2009-07-09 | 2016-02-16 | Procter & Gamble | processo contínuo para produção de uma composição detergente para lavagem de roupas |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59157198A (ja) * | 1983-02-28 | 1984-09-06 | ライオン株式会社 | 嵩密度の小さい洗剤ビルダ−造粒物の製造法 |
| JPS6072998A (ja) * | 1983-09-30 | 1985-04-25 | 花王株式会社 | 粉末物性に優れた界面活性剤粉体組成物の製造法 |
| JPS6072999A (ja) * | 1983-09-30 | 1985-04-25 | 花王株式会社 | 超濃縮粉末洗剤の製法 |
| JPH06128594A (ja) * | 1992-10-16 | 1994-05-10 | Lion Corp | 界面活性剤粉粒体組成物の製造方法 |
| ES2106557T3 (es) * | 1993-07-02 | 1997-11-01 | Unilever Nv | Procedimiento para la produccion de una composicion detergente. |
| JPH0813000A (ja) * | 1994-06-28 | 1996-01-16 | Lion Corp | 高嵩密度粒状洗剤組成物の製造方法 |
-
1996
- 1996-01-31 GB GBGB9601920.3A patent/GB9601920D0/en active Pending
-
1997
- 1997-01-06 WO PCT/EP1997/000118 patent/WO1997028246A1/en not_active Application Discontinuation
- 1997-01-06 EP EP97901008A patent/EP0882126B1/en not_active Revoked
- 1997-01-06 ES ES97901008T patent/ES2145567T3/es not_active Expired - Lifetime
- 1997-01-06 EA EA199800668A patent/EA001314B1/ru not_active IP Right Cessation
- 1997-01-06 HU HU9901180A patent/HUP9901180A3/hu unknown
- 1997-01-06 PL PL97328022A patent/PL184656B1/pl not_active IP Right Cessation
- 1997-01-06 DE DE69701731T patent/DE69701731T2/de not_active Revoked
- 1997-01-06 TR TR1998/01444T patent/TR199801444T2/xx unknown
- 1997-01-06 CN CNB971919607A patent/CN1191351C/zh not_active Expired - Fee Related
- 1997-01-06 CA CA002242420A patent/CA2242420C/en not_active Expired - Fee Related
- 1997-01-06 BR BR9707474A patent/BR9707474A/pt not_active IP Right Cessation
- 1997-01-06 AU AU14409/97A patent/AU1440997A/en not_active Abandoned
- 1997-01-13 ZA ZA97255A patent/ZA97255B/xx unknown
- 1997-01-28 AR ARP970100333A patent/AR005576A1/es unknown
- 1997-01-31 IN IN61BO1997 patent/IN188387B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EA199800668A1 (ru) | 1999-02-25 |
| AU1440997A (en) | 1997-08-22 |
| ZA97255B (en) | 1998-07-14 |
| PL184656B1 (pl) | 2002-11-29 |
| CN1209835A (zh) | 1999-03-03 |
| BR9707474A (pt) | 1999-07-27 |
| CA2242420C (en) | 2005-08-30 |
| TR199801444T2 (xx) | 1998-10-21 |
| DE69701731T2 (de) | 2000-08-10 |
| IN188387B (hu) | 2002-09-14 |
| DE69701731D1 (de) | 2000-05-25 |
| HUP9901180A3 (en) | 2002-04-29 |
| WO1997028246A1 (en) | 1997-08-07 |
| PL328022A1 (en) | 1999-01-04 |
| GB9601920D0 (en) | 1996-04-03 |
| EP0882126B1 (en) | 2000-04-19 |
| CA2242420A1 (en) | 1997-08-07 |
| ES2145567T3 (es) | 2000-07-01 |
| EA001314B1 (ru) | 2001-02-26 |
| EP0882126A1 (en) | 1998-12-09 |
| HUP9901180A2 (hu) | 1999-08-30 |
| AR005576A1 (es) | 1999-06-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |