DE69701731T2 - Verfahren zur herstellung einer waschmittelzusammensetzung - Google Patents
Verfahren zur herstellung einer waschmittelzusammensetzungInfo
- Publication number
- DE69701731T2 DE69701731T2 DE69701731T DE69701731T DE69701731T2 DE 69701731 T2 DE69701731 T2 DE 69701731T2 DE 69701731 T DE69701731 T DE 69701731T DE 69701731 T DE69701731 T DE 69701731T DE 69701731 T2 DE69701731 T2 DE 69701731T2
- Authority
- DE
- Germany
- Prior art keywords
- bulk density
- weight
- process according
- detergent
- low
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Revoked
Links
- 239000000203 mixture Substances 0.000 title claims description 44
- 239000003599 detergent Substances 0.000 title claims description 42
- 238000004519 manufacturing process Methods 0.000 title description 6
- 238000000034 method Methods 0.000 claims description 36
- 238000002156 mixing Methods 0.000 claims description 24
- 239000007858 starting material Substances 0.000 claims description 17
- 239000000463 material Substances 0.000 claims description 14
- 238000001694 spray drying Methods 0.000 claims description 14
- 239000008187 granular material Substances 0.000 claims description 12
- 239000011230 binding agent Substances 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 8
- 239000011236 particulate material Substances 0.000 claims description 8
- 229910021536 Zeolite Inorganic materials 0.000 claims description 6
- 239000002243 precursor Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 239000010457 zeolite Substances 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 3
- 229910000323 aluminium silicate Inorganic materials 0.000 claims description 3
- 238000011065 in-situ storage Methods 0.000 claims description 3
- 239000004615 ingredient Substances 0.000 claims description 3
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 claims description 2
- 229910019142 PO4 Inorganic materials 0.000 claims description 2
- 150000005323 carbonate salts Chemical class 0.000 claims description 2
- 229910017053 inorganic salt Inorganic materials 0.000 claims description 2
- 239000000344 soap Substances 0.000 claims description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims 1
- 239000010452 phosphate Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 claims 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims 1
- 239000000843 powder Substances 0.000 description 25
- 238000005469 granulation Methods 0.000 description 8
- 230000003179 granulation Effects 0.000 description 8
- 235000019832 sodium triphosphate Nutrition 0.000 description 7
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 238000005520 cutting process Methods 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 239000007921 spray Substances 0.000 description 4
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 3
- 239000011149 active material Substances 0.000 description 3
- 238000013019 agitation Methods 0.000 description 3
- 150000001298 alcohols Chemical class 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- -1 potassium alkyl sulphates Chemical class 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 235000010724 Wisteria floribunda Nutrition 0.000 description 2
- SRSXLGNVWSONIS-UHFFFAOYSA-N benzenesulfonic acid Chemical class OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 239000011591 potassium Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 125000001165 hydrophobic group Chemical group 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- VSXGXPNADZQTGQ-UHFFFAOYSA-N oxirane;phenol Chemical compound C1CO1.OC1=CC=CC=C1 VSXGXPNADZQTGQ-UHFFFAOYSA-N 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GBGB9601920.3A GB9601920D0 (en) | 1996-01-31 | 1996-01-31 | Process for the production of a detergent composition |
| PCT/EP1997/000118 WO1997028246A1 (en) | 1996-01-31 | 1997-01-06 | Process for the production of a detergent composition |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69701731D1 DE69701731D1 (de) | 2000-05-25 |
| DE69701731T2 true DE69701731T2 (de) | 2000-08-10 |
Family
ID=10787857
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69701731T Revoked DE69701731T2 (de) | 1996-01-31 | 1997-01-06 | Verfahren zur herstellung einer waschmittelzusammensetzung |
Country Status (16)
| Country | Link |
|---|---|
| EP (1) | EP0882126B1 (hu) |
| CN (1) | CN1191351C (hu) |
| AR (1) | AR005576A1 (hu) |
| AU (1) | AU1440997A (hu) |
| BR (1) | BR9707474A (hu) |
| CA (1) | CA2242420C (hu) |
| DE (1) | DE69701731T2 (hu) |
| EA (1) | EA001314B1 (hu) |
| ES (1) | ES2145567T3 (hu) |
| GB (1) | GB9601920D0 (hu) |
| HU (1) | HUP9901180A3 (hu) |
| IN (1) | IN188387B (hu) |
| PL (1) | PL184656B1 (hu) |
| TR (1) | TR199801444T2 (hu) |
| WO (1) | WO1997028246A1 (hu) |
| ZA (1) | ZA97255B (hu) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9513327D0 (en) * | 1995-06-30 | 1995-09-06 | Uniliver Plc | Process for the production of a detergent composition |
| GB9526097D0 (en) * | 1995-12-20 | 1996-02-21 | Unilever Plc | Process |
| US6150323A (en) * | 1996-10-04 | 2000-11-21 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6121229A (en) * | 1996-10-04 | 2000-09-19 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6136777A (en) * | 1996-10-04 | 2000-10-24 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6211137B1 (en) | 1996-10-04 | 2001-04-03 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6143711A (en) * | 1996-10-04 | 2000-11-07 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6211138B1 (en) | 1996-10-04 | 2001-04-03 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6172034B1 (en) | 1996-10-04 | 2001-01-09 | The Procter & Gamble | Process for making a detergent composition by non-tower process |
| US6391844B1 (en) | 1996-10-04 | 2002-05-21 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| GB9712583D0 (en) | 1997-06-16 | 1997-08-20 | Unilever Plc | Production of detergent granulates |
| GB9712580D0 (en) * | 1997-06-16 | 1997-08-20 | Unilever Plc | Production of detergent granulates |
| GB9713748D0 (en) * | 1997-06-27 | 1997-09-03 | Unilever Plc | Production of detergent granulates |
| CA2346926A1 (en) * | 1998-10-26 | 2000-05-04 | Christopher Andrew Morrison | Processes for making granular detergent composition having improved appearance and solubility |
| EP1141229A1 (en) * | 1998-12-22 | 2001-10-10 | The Procter & Gamble Company | Process for making a low bulk density detergent composition by agglomeration |
| US6596683B1 (en) | 1998-12-22 | 2003-07-22 | The Procter & Gamble Company | Process for preparing a granular detergent composition |
| US6858572B1 (en) | 1999-03-09 | 2005-02-22 | The Procter & Gamble Company | Process for producing coated detergent particles |
| GB9913546D0 (en) | 1999-06-10 | 1999-08-11 | Unilever Plc | Granular detergent component containing zeolite map and laundry detergent compositions containing it |
| GB9913544D0 (en) * | 1999-06-10 | 1999-08-11 | Unilever Plc | Process for preparing granular detergent compositions |
| US6894018B1 (en) | 1999-06-21 | 2005-05-17 | The Procter & Gamble Company | Process for making granular detergent in a fluidized bed granulator having recycling of improperly sized particles |
| MX2012000482A (es) * | 2009-07-09 | 2012-01-27 | Procter & Gamble | Proceso continuo para fabricar una composicion detergen te de lavanderia. |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS59157198A (ja) * | 1983-02-28 | 1984-09-06 | ライオン株式会社 | 嵩密度の小さい洗剤ビルダ−造粒物の製造法 |
| JPS6072998A (ja) * | 1983-09-30 | 1985-04-25 | 花王株式会社 | 粉末物性に優れた界面活性剤粉体組成物の製造法 |
| JPS6072999A (ja) * | 1983-09-30 | 1985-04-25 | 花王株式会社 | 超濃縮粉末洗剤の製法 |
| JPH06128594A (ja) * | 1992-10-16 | 1994-05-10 | Lion Corp | 界面活性剤粉粒体組成物の製造方法 |
| AU699818B2 (en) * | 1993-07-02 | 1998-12-17 | Unilever Plc | Process for the production of high bulk density detergent composition |
| JPH0813000A (ja) * | 1994-06-28 | 1996-01-16 | Lion Corp | 高嵩密度粒状洗剤組成物の製造方法 |
-
1996
- 1996-01-31 GB GBGB9601920.3A patent/GB9601920D0/en active Pending
-
1997
- 1997-01-06 BR BR9707474A patent/BR9707474A/pt not_active IP Right Cessation
- 1997-01-06 DE DE69701731T patent/DE69701731T2/de not_active Revoked
- 1997-01-06 CN CNB971919607A patent/CN1191351C/zh not_active Expired - Fee Related
- 1997-01-06 AU AU14409/97A patent/AU1440997A/en not_active Abandoned
- 1997-01-06 ES ES97901008T patent/ES2145567T3/es not_active Expired - Lifetime
- 1997-01-06 WO PCT/EP1997/000118 patent/WO1997028246A1/en not_active Application Discontinuation
- 1997-01-06 CA CA002242420A patent/CA2242420C/en not_active Expired - Fee Related
- 1997-01-06 EA EA199800668A patent/EA001314B1/ru not_active IP Right Cessation
- 1997-01-06 EP EP97901008A patent/EP0882126B1/en not_active Revoked
- 1997-01-06 PL PL97328022A patent/PL184656B1/pl not_active IP Right Cessation
- 1997-01-06 HU HU9901180A patent/HUP9901180A3/hu unknown
- 1997-01-06 TR TR1998/01444T patent/TR199801444T2/xx unknown
- 1997-01-13 ZA ZA97255A patent/ZA97255B/xx unknown
- 1997-01-28 AR ARP970100333A patent/AR005576A1/es unknown
- 1997-01-31 IN IN61BO1997 patent/IN188387B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| GB9601920D0 (en) | 1996-04-03 |
| PL328022A1 (en) | 1999-01-04 |
| IN188387B (hu) | 2002-09-14 |
| BR9707474A (pt) | 1999-07-27 |
| CN1209835A (zh) | 1999-03-03 |
| CA2242420C (en) | 2005-08-30 |
| CN1191351C (zh) | 2005-03-02 |
| EP0882126B1 (en) | 2000-04-19 |
| EA199800668A1 (ru) | 1999-02-25 |
| DE69701731D1 (de) | 2000-05-25 |
| PL184656B1 (pl) | 2002-11-29 |
| TR199801444T2 (xx) | 1998-10-21 |
| CA2242420A1 (en) | 1997-08-07 |
| ZA97255B (en) | 1998-07-14 |
| HUP9901180A2 (hu) | 1999-08-30 |
| HUP9901180A3 (en) | 2002-04-29 |
| ES2145567T3 (es) | 2000-07-01 |
| EP0882126A1 (en) | 1998-12-09 |
| EA001314B1 (ru) | 2001-02-26 |
| WO1997028246A1 (en) | 1997-08-07 |
| AR005576A1 (es) | 1999-06-23 |
| AU1440997A (en) | 1997-08-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8363 | Opposition against the patent | ||
| 8331 | Complete revocation |