CN114432164B - Aqueous facial mask - Google Patents
Aqueous facial mask Download PDFInfo
- Publication number
- CN114432164B CN114432164B CN202011220859.5A CN202011220859A CN114432164B CN 114432164 B CN114432164 B CN 114432164B CN 202011220859 A CN202011220859 A CN 202011220859A CN 114432164 B CN114432164 B CN 114432164B
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- China
- Prior art keywords
- tremella
- dendrobium
- facial mask
- extract
- mask
- Prior art date
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- 230000001815 facial effect Effects 0.000 title claims abstract description 67
- 241001506047 Tremella Species 0.000 claims abstract description 188
- 239000000284 extract Substances 0.000 claims abstract description 117
- 241001523681 Dendrobium Species 0.000 claims abstract description 115
- 239000007788 liquid Substances 0.000 claims abstract description 89
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 78
- 240000004638 Dendrobium nobile Species 0.000 claims abstract description 26
- 238000000605 extraction Methods 0.000 claims abstract description 17
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- 238000005406 washing Methods 0.000 claims abstract description 13
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- 235000011187 glycerol Nutrition 0.000 claims description 15
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- QGJDXUIYIUGQGO-UHFFFAOYSA-N 1-[2-[(2-methylpropan-2-yl)oxycarbonylamino]propanoyl]pyrrolidine-2-carboxylic acid Chemical compound CC(C)(C)OC(=O)NC(C)C(=O)N1CCCC1C(O)=O QGJDXUIYIUGQGO-UHFFFAOYSA-N 0.000 claims description 6
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- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 3
- QZKRHPLGUJDVAR-UHFFFAOYSA-K EDTA trisodium salt Chemical compound [Na+].[Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O QZKRHPLGUJDVAR-UHFFFAOYSA-K 0.000 claims description 3
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 3
- UEUXEKPTXMALOB-UHFFFAOYSA-J tetrasodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UEUXEKPTXMALOB-UHFFFAOYSA-J 0.000 claims description 3
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- OSCJHTSDLYVCQC-UHFFFAOYSA-N 2-ethylhexyl 4-[[4-[4-(tert-butylcarbamoyl)anilino]-6-[4-(2-ethylhexoxycarbonyl)anilino]-1,3,5-triazin-2-yl]amino]benzoate Chemical compound C1=CC(C(=O)OCC(CC)CCCC)=CC=C1NC1=NC(NC=2C=CC(=CC=2)C(=O)NC(C)(C)C)=NC(NC=2C=CC(=CC=2)C(=O)OCC(CC)CCCC)=N1 OSCJHTSDLYVCQC-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a water aqua facial mask, which comprises the following raw materials in parts by weight: 82.4 to 99.3 percent of tremella dendrobium extractive solution, 0.00 to 10.00 percent of humectant, 0.05 to 2.5 percent of preservative, 0.02 to 0.10 percent of chelating agent and 0.00 to 5.00 percent of skin feel regulator, wherein the preparation process of the tremella dendrobium extractive solution comprises the following steps: 1, 1:1 to 5: soaking tremella and dendrobium nobile in water according to the weight ratio of 1, washing, and extracting under the conditions of the extraction pressure of 40-130 KPa, the extraction temperature of 105-125 ℃ and the extraction time of 1-4 hours to obtain tremella dendrobium nobile extract. The facial mask liquid of the facial mask disclosed by the invention has the advantages that the skin feel is improved by adding the tremella dendrobium nobile extract, meanwhile, the skin affinity, the fitting property and the like of the facial mask cloth are improved, the whole facial mask achieves the effect of excellent skin feel, and the aqueous facial mask also has good moisturizing effect and can obviously improve the skin elasticity and the glossiness.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a water aqua facial mask.
Background
The facial mask is a product which is coated or applied on the surface of human skin, is removed, scrubbed or reserved after a period of time and has the function of concentrated nursing or cleaning. According to the types of products, the facial mask is mainly divided into a facial mask, a pasty facial mask, a gel facial mask and a powder facial mask, wherein the facial mask occupies more than 80% of the facial mask market. The facial mask can be used for rapidly supplementing water and moisturizing, and has good effects on repairing after sun exposure, supplementing water and calming. The Chinese herbal medicine is popular because of convenient use and obvious efficacy.
The face mask is a type of a patch product to be applied on the face for 10 to 15 minutes, and thus its use comfort and skin feel are properties of great concern to consumers. The facial mask is formed by combining facial mask cloth and facial mask liquid, and the using feeling of the facial mask is directly related to both the facial mask cloth and the facial mask liquid. The materials of the film-sticking base cloth (hereinafter referred to as 'mask cloth') on the market mainly comprise hydrogel, silk, tencel, biological fiber, bamboo charcoal fiber, pure cotton fiber, viscose fiber, cuprammonium fiber, long carbon fiber, chitosan fiber and the like. At present, most of facial mask products on the market can achieve a certain beautifying and skin care effect, but the comfort and skin-friendly feeling of the facial mask products can not meet the demands of consumers.
Chinese patent CN106236631B discloses a facial mask liquid for brightening skin color comprising: 1.65 to 7.2 percent of brightening composition, 0.05 to 0.2 percent of chelating agent, 0.02 to 0.1 percent of neutralizing agent, 0.1 to 0.5 percent of acrylic acid (esters)/C10-30 alkanol acrylate cross-linked polymer, 0.05 to 0.2 percent of xanthan gum, 5.1 to 17.8 percent of humectant and the balance of deionized water, wherein the brightening composition is selected from the combination of more than two substances in nicotinamide, acetylglucosamine, carnosine and dendrobium extract, and contains nicotinamide and acetylglucosamine. The facial mask liquid not only has excellent deep moisturizing effect, but also has obvious even color and brightening effect on dark and matt and yellow complexion, so that the skin is more similar to a natural brightening state; chinese patent CN106727148A discloses a dendrobium candidum moisturizing repair mask comprising: the A phase component comprises a humectant, a preservative, a thickener, sodium hyaluronate and water, and the B phase component comprises dendrobium candidum extract, american ginseng root extract, a cosolvent and water, and the mask has strong yin nourishing effect and strong water locking capability. Although the above document discloses that the dendrobium mask liquid has the effects of whitening and moisturizing, whether the mask liquid can improve the comfort and skin-friendly feeling of the mask or not is not studied.
The development of the plant component skin-friendly water aqua facial mask can well solve the requirements of consumers on comfort and skin-friendly feel of facial mask products on the market.
Disclosure of Invention
Based on the defects in the prior art, the invention aims to provide the water aqua facial mask with plant components for improving the skin-friendly property of facial mask cloth, and the facial mask liquid of the facial mask is added with the tremella dendrobium extract liquid for improving the skin feel, and simultaneously improving the skin-friendly property, the fitting property and the like of the facial mask cloth, so that the whole facial mask achieves the effect of excellent skin feel.
The technical problems to be solved by the invention are realized by the following technical scheme:
according to the invention, the raw materials for the aqueous facial mask comprise the following components in parts by weight: 82.4 to 99.3 percent of tremella dendrobium extractive solution, 0.00 to 10.00 percent of humectant, 0.05 to 2.5 percent of preservative, 0.02 to 0.10 percent of chelating agent and 0.00 to 5.00 percent of skin feel regulator.
According to the invention, the tremella and dendrobium nobile extract is prepared from tremella and dendrobium nobile according to a certain proportion.
According to the invention, the preparation method of the tremella dendrobium extractive solution comprises the following steps: the tremella dendrobium extract is prepared by adopting a high-temperature high-pressure method.
According to a further embodiment of the present invention, the preparation method of the tremella dendrobium extractive solution specifically includes the following steps:
soaking tremella and dendrobium nobile in water in a certain weight ratio, and then washing and extracting to obtain tremella dendrobium nobile extract;
in the extracting step, the extracting pressure is 40-130 KPa; the extraction temperature is 105-125 ℃; the extraction time is 1-4 h.
According to a further embodiment of the invention, the weight ratio of tremella to dendrobium in the tremella dendrobium extract is 1:1-5:1.
According to a further embodiment of the present invention, in the extracting step of the tremella dendrobium nobile extract, the extracting pressure is 40-75 KPa.
According to a further embodiment of the invention, in the extracting step of the tremella dendrobium nobile extracting solution, the extracting temperature is 105-115 ℃.
According to a further embodiment of the invention, in the extracting step of the tremella dendrobium nobile extracting solution, the extracting time is 2-3 hours.
According to still further preferred embodiments of the present invention, the extraction pressure in the extraction process is 70 KPa.
According to still further preferred embodiments of the present invention, the extraction temperature in the extraction process is 115 ℃.
According to still other preferred embodiments of the present invention, the extraction temperature time is 3 h.
According to a further embodiment of the invention, in the step of extracting the tremella dendrobium extractive solution, the ratio of the tremella dendrobium to water is 1:30-1:70.
According to some embodiments of the invention, the humectant is one or more of glycerin, 1, 3-propanediol, and polyalcohol.
According to some embodiments of the invention, the preservative is one or more of the conventional preservatives in the art.
According to some embodiments of the invention, the chelating agent is one or more of sodium glucoheptonate, disodium EDTA, trisodium EDTA, tetrasodium EDTA.
According to some embodiments of the invention, the skin feel modifier is one or more of glycerolyether-26, panthenol and other water agents.
According to the present invention, the aqueous mask may be prepared by a conventional method of the mask in the art.
According to some embodiments of the invention, the aqueous mask is prepared by:
taking 82.4-99.3% of tremella dendrobium extract, 0.00-10.00% of humectant (one or more of glycerin, 1, 3-propanediol and polyalcohol), 0.05-2.5% of preservative, 0.02-0.10% of chelating agent (one or more of sodium glucoheptonate, disodium EDTA, trisodium EDTA and tetrasodium EDTA) and 0.00-5.00% of skin feel regulator (one or more of glycerin polyether-26, panthenol and other skin feel regulator of water aqua) as A phase, sequentially adding all raw materials of the A phase, and uniformly stirring to obtain the water aqua surface patch.
The beneficial effects of the invention are as follows:
according to the aqueous facial mask disclosed by the invention, the tremella dendrobium extract is prepared by adding the aqueous facial mask disclosed by the invention, so that the skin feel is improved, and meanwhile, the skin affinity, the fitting property and the like of the facial mask cloth are improved, so that the effect of extremely good skin feel of the whole facial mask is achieved.
The aqueous facial mask also has good moisturizing effect, and can remarkably improve skin elasticity and glossiness.
Drawings
FIG. 1 is a diagram showing the comparison of skin feel of tremella and tremella dendrobium nobile extracts of two preparation processes;
FIG. 2 is a skin-feel radar chart of the dendrobium tremella extract with different addition ratios;
FIG. 3 is a graph of the results of the ABTS free radical scavenging experiments of the dendrobium nobile extracts with different addition amounts;
FIG. 4 is a graph of skin moisture content test results for a 90% tremella dendrobium extract and a mask solution containing 90% tremella dendrobium extract;
FIG. 5 is a skin elasticity test chart of 90% tremella dendrobium extract and mask solution containing 90% tremella dendrobium extract;
FIG. 6 is a chart of skin glossiness test of 90% tremella herba Dendrobii extract and facial mask liquid containing 90% tremella herba Dendrobii extract;
FIG. 7 is a graph of evaluation of primary feeling of a water-based face mask;
FIG. 8 is a graph showing evaluation of skin feel of an aqueous facial mask;
FIG. 9 is a graph showing the results of skin feel trials after the mask cloth (cotton cloth) is soaked with water, a commercially available mask solution, an aqueous extract tremella dendrobium mask solution, and the tremella dendrobium mask solution of the present invention, respectively;
FIG. 10 is a graph showing the results of skin feel trials after the mask cloth (flannelette) is soaked with water, a commercially available mask solution, an aqueous extract tremella dendrobe mask solution, and the tremella dendrobe mask solution of the present invention, respectively;
FIG. 11 is a graph showing the results of skin feel trials after the mask cloth (copper ammonia silk) is soaked with water, a commercially available mask solution, an aqueous extract tremella dendrobe mask solution, and the tremella dendrobe mask solution of the present invention, respectively;
FIG. 12 is a graph showing consistency comparison results of four mask liquids, namely, a tremella dendrobium mask liquid, a commercially available mask liquid, a water extraction tremella dendrobium mask liquid and water;
FIG. 13 is a chart showing the molecular weight distribution of dendrobe polysaccharide;
FIG. 14 is a graph showing the molecular weight distribution of tremella polysaccharides;
FIG. 15 is a graph showing the molecular weight distribution of the polysaccharide of Dendrobium tremella prepared in accordance with the present invention.
Detailed Description
The invention will be further illustrated with reference to specific examples, but the invention is not limited thereto.
It will be appreciated by persons skilled in the art that the present invention is not limited to the embodiments described above, and that any changes and modifications to the present invention fall within the scope of the present invention.
The experimental methods described in the following examples are all conventional methods unless otherwise specified; the experimental materials and reagents, unless otherwise specified, are commercially available.
TABLE 1 raw materials and sources
| Raw material name | INCI | Suppliers (suppliers) |
| DendrobiumDendrobium officinale Kimura et Migo | Dendrobium officinale Kimura et Migo | Pu' er Da Runfu Hu planting Co., ltd |
| Tremella fuciformis berk | Tremella fuciformis Berk | Kangwang food Co., ltd |
The plant components moisturizing mask comprises the following total components: the tremella dendrobium extract, water, glycerol, 1, 3-propanediol, 1, 2-pentanediol, glycereth-26, panthenol, 1, 2-hexanediol and sodium glucoheptonate.
Table 2 plant component moisturizing mask full ingredients
| Raw materials | Additive amount wt% |
| Water and its preparation method | TO100 |
| The invention relates to tremella and dendrobium nobile extract | 40-90 |
| Glycerol/1, 3-propanediol | 0.00-10.00 |
| Glycerol polyether-26/panthenol | 0.00-5.00 |
| 1, 2-pentanediol/1, 2-hexanediol | 0.05-2.5 |
| Glucoheptonic acid sodium salt | 0.02-0.10 |
Example 1
The preparation method of the tremella dendrobium extract comprises the following steps:
(1) Weighing tremella 20 g and dendrobium 20 g (tremella: dendrobium=1:1);
(2) Soaking the tremella dendrobium mixture in water at 20-30 ℃ for 0.5-h, and then washing;
(3) Extracting: 2000 mL water is added, namely the feed liquid ratio is 1:50, extracting the mixture at 70 KPa and 115 ℃ to obtain 3 h;
(4) And (3) filtering: filtering the extract with 100 mesh filter cloth; obtaining the tremella dendrobium extract.
Example 2
(1) Weighing tremella 20 g and dendrobium 10 g (tremella: dendrobium=2:1);
(2) Soaking the tremella dendrobium mixture in water at 20-30 ℃ for 0.5-h, and then washing;
(3) Extracting: 2100 and mL water was added, i.e. feed to liquid ratio 1:70, extracting the mixture at 70 KPa and 115 ℃ to obtain 3 h;
(4) And (3) filtering: filtering the extract with 200 mesh filter cloth; obtaining the tremella dendrobium extract.
Example 3
(1) Weighing tremella 20 g and dendrobium 5 g (tremella: dendrobium=4:1);
(2) Soaking the tremella dendrobium mixture in water at 20-30 ℃ for 0.5h, and then washing;
(3) Extracting: 720 mL water is added, namely the feed liquid ratio is 1:30, extracting the mixture at 70 KPa and 115 ℃ to obtain 3 h;
(4) And (3) filtering: filtering the extract with 100 mesh filter cloth; obtaining the tremella dendrobium extract.
Example 4
(1) Weighing tremella 20 g and dendrobium 4 g (tremella: dendrobium=5:1);
(2) Soaking the tremella dendrobium mixture in water at 20-30 ℃ for 1.5-h, and then washing;
(3) Extracting: 1250 and mL water is added, namely the feed liquid ratio is 1:50, extracting the mixture at 130 KPa and 125 ℃ to obtain 4 h;
(4) And (3) filtering: filtering the extract with 100 mesh filter cloth; obtaining the tremella dendrobium extract.
Example 5
(1) Weighing tremella 20 g and dendrobium 20 g (tremella: dendrobium=1:1);
(2) Soaking the tremella dendrobium mixture in water at 20-30 ℃ for 1.5-h, and then washing;
(3) Extracting: 2000 mL water is added, namely the feed liquid ratio is 1:50, extracting the mixture at 50 KPa and 110 ℃ to obtain 1 h;
(4) And (3) filtering: filtering the extract with 100 mesh filter cloth; obtaining the tremella dendrobium extract.
Example 6
(1) Weighing tremella 20 g and dendrobium 20 g (tremella: dendrobium=1:1);
(2) Soaking the tremella dendrobium mixture in water at 20-30 ℃ for 0.5-h, and then washing;
(3) Extracting: 2000 mL water is added, namely the feed liquid ratio is 1:50, extracting the mixture at 40 KPa and 105 ℃ to obtain 3 h;
(4) And (3) filtering: filtering the extract with 100 mesh filter cloth; obtaining the tremella dendrobium extract.
Comparative example 1
(1) Weighing tremella 5 g and dendrobium 20 g (tremella: dendrobium=1:4);
(2) Soaking the tremella dendrobium mixture in water at 20-30 ℃ for 0.5-h, and then washing;
(3) Extracting: 1250 and mL water is added, namely the feed liquid ratio is 1:50, the mixture is stirred at 70 KPa,115 DEG CA kind of electronic deviceExtracting 3 h under the condition;
(4) And (3) filtering: filtering the extract with 100 mesh filter cloth; obtaining the tremella dendrobium extract.
Comparative example 2
(1) Weighing tremella 20 g and dendrobium 2.5 g (tremella: dendrobium=8:1);
(2) Soaking the tremella dendrobium mixture in water at 20-30 ℃ for 0.5-h, and then washing;
(3) Extracting: 1125 of mL water is added, namely the feed liquid ratio is 1:50, extracting the mixture at 70 KPa and 115 ℃ to obtain 3 h;
(4) And (3) filtering: filtering the extract with 100 mesh filter cloth; obtaining the tremella dendrobium extract.
Comparative example 3
The procedure of example 1 was repeated except that no dendrobe was added to obtain a tremella extract.
(1) Weighing tremella 20 and g;
(2) Soaking tremella in water at 20-30 ℃ for 0.5-h, and then washing;
(3) Extracting: 1000 mL water is added, namely the feed liquid ratio is 1:50, extracting the mixture at 70 KPa and 115 ℃ to obtain 3 h;
(4) And (3) filtering: filtering the extract with 100 mesh filter cloth; obtaining tremella extract.
Comparative example 4
The procedure of example 1 was repeated except that tremella was not added, to obtain a dendrobe extract.
(1) Weighing herba Dendrobii 20 g;
(2) Soaking dendrobium in water at 20-30 ℃ for 0.5-h, and then panning;
(3) Extracting: 1000 mL water is added, namely the feed liquid ratio is 1:50, extracting the mixture at 70 KPa and 115 ℃ to obtain 3 h;
(4) And (3) filtering: filtering the extract with 100 mesh filter cloth; obtaining the dendrobium extract.
Comparative example 5
The preparation method of the tremella dendrobium extract by the traditional water extraction method comprises the following steps:
(1) Weighing tremella 20 g and dendrobium 20 g (tremella: dendrobium=1:1);
(2) Soaking the tremella dendrobium mixture in water at 20-30 ℃ for 0.5-h, and then washing;
(3) Extracting: 2000 mL water is added, namely the feed liquid ratio is 1:50, extracting the mixture at the normal pressure of 80 ℃ to obtain 3 h;
(4) And (3) filtering: filtering the extract with 100 mesh filter cloth; obtaining the tremella dendrobium extract by the traditional water extraction method.
Comparative example 6
The preparation method of the dendrobium extract by the traditional water extraction method comprises the following steps:
(1) Weighing herba Dendrobii 20 g;
(2) Soaking dendrobium in water at 20-30 ℃ for 0.5-h, and then panning;
(3) Extracting: 1000 mL water is added, namely the feed liquid ratio is 1:50, extracting the mixture at the normal pressure of 80 ℃ to obtain 3 h;
(4) And (3) filtering: filtering the extract with 100 mesh filter cloth; obtaining the dendrobium extract by the traditional water extraction method.
Efficacy evaluation of tremella and dendrobium nobile extracts
1. Skin feel test of tremella and dendrobium nobile extract
Skin feel test: 30 women were recruited, aged 18-40 years, with dry skin, and 3 areas 1,2, 3 were drawn on the arm and samples 1,2, 3 were smeared, respectively. Scoring the skin feel after trial, wherein the score of each item is 5 points, and the more satisfied the score is, the higher the score is; in addition to sticky feel, the lower the score, the better.
Sample to be tested:
sample 1 the method of example 1 prepares a tremella dendrobium extract;
sample 2 comparative example 3 tremella high temperature high pressure extract;
sample 3 comparative example 5 water extraction of tremella dendrobium extract.
Fig. 1 is a skin feel comparison chart of a tested sample, and from five dimensions, the high-temperature and high-pressure tremella extract of the sample 2 is too thick, has obvious sticky feel, is sticky to feel, has poor skin feel and has stronger film forming feel. Compared with the sample 2 and the sample 3, the tremella dendrobium extractive solution prepared by the method can obviously improve the sticky feeling of tremella, so that the skin feeling is improved to a great extent, and the moistening feeling, the absorption speed and the slippery feeling of hands are improved to different degrees.
Fig. 2 is a diagram of skin-feel radar of different tremella dendrobe ratios (samples prepared in example 1, comparative example 1 and comparative example 2), and skin-feel is different according to different addition ratios. Compared with the comparative example, the tremella dendrobium extract prepared by the embodiment of the invention has obvious advantages in the aspects of absorption speed, slippery feeling on hands, moistening degree and sticky feeling.
The tremella dendrobium nobile extract prepared by the invention has obvious improvement on the skin feel of the obtained extract.
2. Free radical scavenging experiment of tremella and dendrobium extract
The free radical scavenging experimental method is as follows: prepared as 7 mmol.L -1 ABTS stock solution and 140 mmol.L -1 Potassium persulfate stock solution. A certain amount of 7 mmol.L -1 ABTS and 140 mmol.L -1 Potassium persulfate was mixed and allowed to stand at room temperature in the dark for a period of time to form ABTS radical stock solution. Taking a certain amount of ABTS free radical stock solution, diluting with 50% ethanol, and making final test negative control light absorptionThe value was 0.70.+ -. 0.02.
Diluting the tremella dendrobium extract prepared in the embodiment 1 into different concentration gradients, sequentially adding the test solution and the ABTS free radical stock solution, mixing uniformly by vortex, placing the mixture in an enzyme-labeled instrument for light-shielding incubation for a certain time, measuring the absorbance value of the mixture at the wavelength 734 nm by the enzyme-labeled instrument, and calculating the ABTS free radical clearance. As can be seen from fig. 3, the tremella dendrobium extract has high free radical removal rate.
Example 7 (Water aqua mask liquid)
91.98 percent of tremella dendrobium extract (example 1), 1.00 percent of panthenol, 3.00 percent of glycerol, 2.00 percent of 1, 3-propanediol, 0.02 percent of sodium glucoheptonate, 1.00 percent of glycereth-26 and 1.00 percent of octanoyl hydroxamic acid/1, 2-hexanediol/1, 3-propanediol) are sequentially mixed and stirred uniformly to obtain the aqueous facial mask sticking mask liquid.
Example 8 (Water aqua mask liquid)
Mixing 92.47% of tremella herba dendrobii extract (example 1), 0.50% of phenoxyethanol/ethylhexyl glycerol, 3.00% of 1, 3-propanediol, 0.03% of EDTA disodium and 1.00% of panthenol in sequence, and stirring uniformly to obtain the aqueous facial mask sticking film liquid.
Example 9 (Water aqua mask liquid)
92.18% of tremella extract (example 1), 0.80% (glyceryl caprylate, octanoyl hydroxamic acid, 1, 2-pentanediol/1, 2-hexanediol), 3.00% of glycerin, 2.00% of butanediol, 0.02% of Crodaquest A300, 2.00% of EG-1 and the like are sequentially mixed and stirred uniformly to obtain the aqueous facial mask liquid.
Example 10 (Water aqua mask liquid)
Mixing 90.48% of tremella herba dendrobii extract (example 1), 1.00% of panthenol, 3.00% of glycerol, 2.00% of 1, 3-propanediol, 0.02% of sodium glucoheptonate, 1.00% of glycerolyether-26, 2.00% of 1, 2-pentanediol and 0.5% of 1, 2-hexanediol in sequence, and stirring uniformly to obtain the aqueous facial mask liquid.
Example 11 (mask liquid containing 40% Tremella dendrobe extract)
Mixing 40% of tremella herba dendrobii extract (example 1), 2.5% (1, 2-pentanediol/1, 2-hexanediol), 3.00% of glycerin, 2.00% of 1, 3-propanediol, 0.02% of Crodaquest A300, 1.00% of EG-1 and 1.00% of panthenol and the balance of deionized water in sequence, and stirring uniformly to obtain the aqueous facial mask liquid.
Example 12 (mask liquid containing 70% Tremella dendrobe extract)
Mixing 70% of tremella herba dendrobii extract (example 1), 2.5% (1, 2-pentanediol/1, 2-hexanediol), 3.00% of glycerin, 2.00% of 1, 3-propanediol, 0.02% of Crodaquest A300, 1.00% of EG-1 and 1.00% of panthenol and the balance of deionized water in sequence, and stirring uniformly to obtain the aqueous mask liquid.
Example 13 (mask liquid containing 90% extract of Tremella Dendrobium nobile)
Mixing 90% of tremella herba dendrobii extract (example 1), 2.5% (1, 2-pentanediol/1, 2-hexanediol), 3.00% of glycerol, 2.00% of 1, 3-propanediol, 0.02% of Crodaquest A300, 1.00% of EG-1 and 1.00% of panthenol and the balance of deionized water in sequence, and stirring uniformly to obtain the aqueous mask film liquid.
Comparative example 7 (commercial mask lotion)
The full components of the commercially available moisturizing mask are as follows: water, glycerol, 1, 3-propylene glycol, betaine, p-hydroxyacetophenone, sodium citrate, citric acid, hydroxyethyl cellulose, PEG-40 hydrogenated castor oil, sodium alginate, sodium hyaluronate, ascorbyl glucoside, 1, 2-pentanediol, rye (SECALE CEREALE) seed extract, dipeptide diamino Ding Xianbian-yl amide diacetate and essence.
Comparative example 8 (Water extraction Tremella dendrobe mask liquid)
The other parts are the same as in example 10 except that the tremella dendrobium extract of the present invention is replaced with the water extracted tremella dendrobium extract (comparative example 5).
Efficacy evaluation of aqueous mask sticking mask liquid
3. Water supplementing and moisturizing effect test
30 volunteers are selected, the test sample is smeared on the forearm flexor side, and the moisture content of the tested part is measured at each time point such as 15min, 30min, 45min, 1h, 1.5h, 2h and the like before the test.
TABLE 3 influence of 90% Tremella Stem extract (example 1) and mask liquid containing 90% Tremella Stem extract (example 13) on skin Water holding Property
| Product(s) | Initial value | After using for 15min | After 30min of use | After using for 45min | After 1h of use | After 1.5h of use | After 2 hours of use |
| 90% extract of Tremella herba Dendrobii (example 1) | 24.34 | 29.67 | 27.14 | 25.98 | 26.15 | 26.81 | 25.18 |
| Facial mask liquid containing 90% tremella dendrobium extract (example 12) | 22.58 | 33.50 | 30.48 | 30.43 | 32.49 | 32.11 | 31.00 |
As can be seen from table 3 and fig. 4, both the tremella dendrobium extract and the facial mask liquid product containing tremella dendrobium extract can significantly increase the skin moisture content.
4. Skin elasticity test
30 volunteers are selected, a test sample is smeared on the forearm flexor side, and elasticity of tested parts at several time points such as 15min before use, 1h, 2h and the like of the mask liquid containing 90% of the dendrobe tremella extract and 90% of the dendrobe tremella extract is tested.
Table 490 Effect of Tremella Stem extract (example 1) and mask solution containing 90% Tremella Stem extract (example 13) on skin elasticity
| Skin elasticity | Initial value | After using for 15min | After 1h of use | After 2 hours of use |
| 90% extract of Tremella herba Dendrobii (example 1) | 0.816 | 1.055 | 1.110 | 1.089 |
| Facial mask liquid containing 90% tremella and dendrobium extract (example 13) | 0.814 | 1.092 | 1.120 | 1.120 |
As can be seen from table 4 and fig. 5, the skin elasticity can be significantly improved both in the tremella dendrobium extract and the facial mask liquid product containing tremella dendrobium extract.
5. Skin gloss test
30 volunteers are selected, a test sample is smeared on the forearm flexor side, and the glossiness of tested parts at a plurality of time points such as 15min before use, 1h, 2h and the like of the mask liquid containing 90% of the dendrobe tremella extract and 90% of the dendrobe tremella extract is tested.
TABLE 5 influence of 90% Tremella Stem extract (example 1) and mask liquid containing 90% Tremella Stem extract (example 13) on skin gloss
| Skin gloss | Initial value | After using for 15min | After 1h of use | After 2 hours of use |
| 90% extract of Tremella herba Dendrobii (example 1) | 3.85 | 4.14 | 4.02 | 4.49 |
| Facial mask liquid containing 90% tremella dendrobium extract (example 12) | 3.82 | 4.28 | 4.34 | 4.22 |
As can be seen from table 5 and fig. 6, the skin elasticity can be significantly improved both in the tremella dendrobium extract and the facial mask liquid product containing tremella dendrobium extract.
6. Water agent surface film skin feel test
After normal face cleaning, 23 volunteers are selected, the aqueous face mask is applied for 15 minutes, questionnaire survey is filled after cleaning, the total score is 5 minutes, the higher the score is, the higher the degree is, and the primary feeling evaluation and the skin feeling evaluation of the subjects on the aqueous face mask are arranged according to trial feedback.
TABLE 6 evaluation results of preliminary feeling of aqueous mask film
| Project | Average value of | 1 | 2 | 3 | 4 | 5 |
| Degree of mask cloth infiltration | 4.87 | 0 | 0 | 0 | 3(13.04%) | 20(86.96%) |
| Uniformity of liquid on membrane cloth | 4.61 | 0 | 0 | 2(8.7%) | 5(21.74%) | 16(69.57%) |
| Facial mask liquid consistency | 3.48 | 0 | 4(17.39%) | 7(30.43%) | 9(39.13%) | 3(13.04%) |
| Color preference degree of mask liquid | 3.78 | 0 | 3(13.04%) | 5(21.74%) | 9(39.13%) | 6(26.09%) |
| Liquid odor preference of mask | 3.43 | 0 | 4(17.39%) | 8(34.78%) | 8(34.78%) | 3(13.04%) |
As can be seen from table 6 and fig. 7, the degree of wetting of the mask cloth by the subject and the uniformity degree of the liquid on the mask cloth were high.
TABLE 7 evaluation results of skin feel of aqueous surface film
| Question/option | Average score | 1 | 2 | 3 | 4 | 5 |
| Moist feeling | 4.17 | 0 | 0 | 3(13.04%) | 13(56.52%) | 7(30.43%) |
| Moisturizing effect | 4 | 0 | 0 | 4(17.39%) | 15(65.22%) | 4(17.39%) |
| Slip feeling | 3.87 | 0 | 1(4.35%) | 5(21.74%) | 13(56.52%) | 4(17.39%) |
| Absorption rate | 3.74 | 0 | 2(8.7%) | 5(21.74%) | 13(56.52%) | 3(13.04%) |
| Sticky feeling | 2.7 | 2(8.7%) | 8(34.78%) | 8(34.78%) | 5(21.74%) | 0 |
| Integral bodyFeel of sensation | 4.09 | 0 | 0 | 1(4.35%) | 82.61% | 3(13.04%) |
As can be seen from table 7 and fig. 8, the subjects were highly evaluated in terms of the overall moisturizing sensation, moisturizing effect, slip sensation, absorption rate, and overall sensation of the mask.
7. Evaluation of effects such as facial mask cloth fitting degree and comfort level
Three types of commonly used mask cloth are respectively selected, the same amount of mask liquid (25 g) of the commercially available mask is used for soaking the same mask cloth for the same time (30 min) by using water and water to extract the tremella dendrobium mask liquid and the tremella dendrobium mask liquid, then 6 professional cosmetic formulators are used for performing skin sensing evaluation, 5 is divided into an upper limit, the degree of fitting of the mask cloth is increased along with the increase of the score value, the comfort of the mask cloth is increased, the softness of the mask cloth is increased, and the average value for taking out the test is represented by a final result. By combining tables 8-10 and trial figures 9-11, the tremella and dendrobium mask liquid can be intuitively seen to obviously improve the fitting degree of mask cloth and obviously improve the comfort and softness of the mask cloth.
FIGS. 9-11A volunteer used mask liquid sequentially were left one water, left two commercial mask liquid, left three water extracted tremella dendrobe mask liquid (comparative example 8), left four tremella dendrobe mask liquid of the present invention (example 10)
TABLE 8 correspondence between cotton cloth and water, commercially available mask liquid, water extracted Tremella Stem mask liquid (comparative example 8) and Tremella Stem mask liquid of the present invention (example 10)
| Cotton cloth | Water and its preparation method | Commercially available mask liquid | Water extraction tremella and dendrobium mask liquid | The invention relates to tremella and dendrobium mask liquid |
| Degree of film cloth fitting | 2.2 | 3.6 | 3.2 | 4.7 |
| Comfort level of membrane cloth | 2.6 | 3.8 | 3.8 | 4.8 |
| Softness and softness | 2.9 | 3.9 | 3.3 | 4.5 |
Table 9 correspondence of lint and water, commercial mask solution, aqueous extract tremella dendrobe mask solution (comparative example 8) and tremella dendrobe mask solution of the present invention (example 10)
| Lint cloth | Water and its preparation method | Commercially available mask liquid | Water extraction tremella and dendrobium mask liquid | The invention relates to tremella and dendrobium mask liquid |
| Degree of film cloth fitting | 2.8 | 3.4 | 3.1 | 4.8 |
| Comfort level of membrane cloth | 3.2 | 3.5 | 3.3 | 4.4 |
| Softness and softness | 3.5 | 3.8 | 3.8 | 4.7 |
Table 10 correspondence of copper ammonia silk mask cloth and water, commercial mask liquid, water extracted tremella dendrobe mask liquid (comparative example 8) and tremella dendrobe mask liquid of the present invention (example 10)
| Copper ammonia wire | Water and its preparation method | Commercially available mask liquid | Water extraction tremella and dendrobium mask liquid | The invention relates to tremella and dendrobium mask liquid |
| Degree of film cloth fitting | 2.1 | 3.6 | 3.3 | 4.5 |
| Comfort level of membrane cloth | 2.3 | 3.2 | 3.4 | 4.3 |
| Softness and softness | 1.8 | 3.4 | 3.3 | 4.1 |
8. Consistency contrast of mask solution
The lower graph shows the consistency comparison of the four types of mask liquid (generally, the higher the consistency is, the worse the wetting degree of the mask cloth is, and the best the wetting degree of water is). As shown in fig. 12, the consistency of the mask liquid is compared with the following result: the tremella and dendrobium mask liquid is more than the commercial mask liquid and the water extraction tremella and dendrobium mask liquid is more than or equal to water.
9. Influence of tremella and dendrobium mask liquid with different proportions on mask skin feeling
Three tremella dendrobium mask solutions with the tremella dendrobium extract proportion of 40%, 70% and 90% are respectively used for soaking superfine cotton mask cloth, skin sensing evaluation is carried out by 6 professional cosmetic formulators, 5 is divided into upper limits, the moisturizing feeling is increased along with the increase of the score value, the slippery feeling is increased, the absorption speed is accelerated, the sticky feeling is increased, the overall feeling is better, and the average value for sampling is represented as a final result. As shown in Table 11, the facial mask liquid containing 90% of the extract of Dendrobium tremella has outstanding moist feel and slippery feel, and the overall feel is better.
Table 11 effects of mask liquids of different proportions of tremella and dendrobium nobile extracts on mask skin feel
| Superfine cotton | Mask liquid of 40% tremella dendrobe extract (example 11) | Mask liquid of 70% tremella dendrobe extract (example 12) | Facial mask liquid of 90% tremella dendrobe extract (example 13) |
| Moist feeling | 2.3 | 3.4 | 4.6 |
| Slip feeling | 3.2 | 3.8 | 4.7 |
| Absorption rate | 4.1 | 3.8 | 3.5 |
| Sticky feeling | 1.8 | 2.5 | 2.8 |
| Feeling as a whole | 2.9 | 3.4 | 4.2 |
The inventor tests the polysaccharide yield and the molecular weight of the tremella dendrobium extract, and the testing process and the results are as follows:
polysaccharide yield test
The testing method comprises the following steps: polysaccharide determination is carried out by phenol-sulfuric acid method (specifically, reference is made to the content determination of polysaccharide in tremella [ J ]. Heilongjiang medical science, 1999 (06): 32-32.).
Test sample: the tremella dendrobium extract is prepared in the embodiment.
Test results: the polysaccharide content is 1.20 mg/mL-4.24 mg/mL.
| Sample of | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 |
| Polysaccharide content | 4.24mg/mL | 3.09mg/mL | 2.94mg/mL | 1.20mg/mL | 3.20mg/mL | 3.04mg/mL |
Wherein the highest polysaccharide content is that of the tremella dendrobium extract prepared in the embodiment 1, and the polysaccharide content is 4.24mg/mL.
Molecular weight measurement of polysaccharide of tremella dendrobium extract
Molecular weight distribution determination: the detection method adopts high-efficiency gel permeation chromatography (specifically referring to tremella polysaccharide quality control research based on high-efficiency gel permeation chromatography, [ J ] Chinese herbal medicine, 2011, 42 (09): 1732-1735.).
The molecular weight distribution of the tremella dendrobium polysaccharide prepared in the measurement example 1, the tremella dendrobium polysaccharide of the comparison example 4 and the tremella polysaccharide of the comparison example 3 is shown in fig. 13, 14 and 15.
As can be seen from fig. 13, 14 and 15, the molecular weight of the dendrobe polysaccharide is smaller, the molecular weight of the tremella polysaccharide is larger, and compared with the separate dendrobe extract and tremella extract, the molecular weight distribution of the tremella dendrobe polysaccharide prepared in the embodiment 1 of the present invention is greatly changed, and the molecular weight distribution range is from 400 Da to 580 ten thousand Da. The molecular distribution of dendrobium polysaccharide is mainly 300 Da to 260 ten thousand Da.
The experiment shows that under the preparation process conditions, the molecular weight distribution of the tremella dendrobium extract is improved.
Claims (9)
1. The utility model provides a water aqua face pad pasting which characterized in that: the raw materials used in the method comprise the following components in percentage by weight: 82.4 to 99.3 percent of tremella dendrobium extractive solution, 0.00 to 10.00 percent of humectant, 0.05 to 2.5 percent of preservative, 0.02 to 0.10 percent of chelating agent and 0.00 to 5.00 percent of skin feel regulator; the tremella and dendrobium nobile extract is prepared by compounding tremella and dendrobium nobile according to a certain proportion and adopting a high-temperature high-pressure method preparation process;
the preparation method of the tremella dendrobium extractive solution specifically comprises the following steps:
soaking tremella and dendrobium nobile in water in a certain weight ratio, and then washing, and extracting with water to obtain tremella dendrobium nobile extract;
in the extracting step, the extracting pressure is 40-130 KPa; the extraction temperature is 105-125 ℃; the extraction time is 1-4 h;
wherein the weight ratio of the tremella to the dendrobium nobile in the tremella dendrobium nobile extracting solution is 1:1-5:1.
2. The aqueous facial mask of claim 1, wherein: in the step of extracting the tremella dendrobium nobile extract, the extracting pressure is 40-75 KPa; the extraction temperature is 105-115 ℃; the extraction time is 2-3 h.
3. The aqueous facial mask of claim 1, wherein: in the step of extracting the tremella dendrobium nobile extract, the extracting pressure is 70 KPa; the extraction temperature is 115 ℃; the extraction time was 3 h.
4. The aqueous facial mask of claim 1, wherein: in the extraction step of the tremella dendrobium extractive solution, the feed liquid ratio of tremella dendrobium to water is 1:30-1:70.
5. The aqueous facial mask according to any one of claims 1 to 4, wherein: the humectant is a polyol.
6. The aqueous facial mask according to any one of claims 1 to 4, wherein: the humectant is glycerin and/or 1, 3-propylene glycol.
7. The aqueous facial mask according to any one of claims 1 to 4, wherein: the preservative is one or more of conventional preservatives in the field.
8. The aqueous facial mask according to any one of claims 1 to 4, wherein: the chelating agent is one or more of sodium glucoheptonate, disodium EDTA, trisodium EDTA and tetrasodium EDTA.
9. The aqueous facial mask according to any one of claims 1 to 4, wherein: the skin feel regulator is one or more of glycereth-26, panthenol and other skin feel regulators of water aqua.
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| CN104257597A (en) * | 2014-09-17 | 2015-01-07 | 郑州蓬泽生物科技开发研究院 | Dendrobe beauty fluid and preparation method thereof |
| CN105707628A (en) * | 2016-03-11 | 2016-06-29 | 三株福尔制药有限公司 | Probiotic fermentation dendrobium officinale protocorm composition and preparation method thereof |
| CN106265339A (en) * | 2016-09-14 | 2017-01-04 | 叶树林 | A kind of six hours high-efficiency moisturizing compositions and preparation thereof and application |
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| CN104257597A (en) * | 2014-09-17 | 2015-01-07 | 郑州蓬泽生物科技开发研究院 | Dendrobe beauty fluid and preparation method thereof |
| CN105707628A (en) * | 2016-03-11 | 2016-06-29 | 三株福尔制药有限公司 | Probiotic fermentation dendrobium officinale protocorm composition and preparation method thereof |
| CN106265339A (en) * | 2016-09-14 | 2017-01-04 | 叶树林 | A kind of six hours high-efficiency moisturizing compositions and preparation thereof and application |
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